Materials Literature
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Theoretical saturation magnetization and magnetocrystalline anisotropy energy (MAE) of τ-phase (face-centered tetragonal) Mn50Al50 alloy were obtained by first principles calculations, and the alloy was fabricated to compare the experimental values with the theoretical predictions. The calculated magnetic moment and M…
We adopt a reverse Monte Carlo refinement approach, using experimental X-ray total scattering data, to develop a structure model for synthetic, hydrated amorphous calcium carbonate (ACC). The ACC is revealed to consist of a porous calcium-rich framework that supports interconnected channels containing water and carbon…
We demonstrate a novel way to actively tune surface plasmons by fabricating plasmonic nanostructures on stretchable elastomeric films. This allows reversible modification of the metal geometry on the nanometer scale. Using 100 nm scale Au nanoparticle dimers whose spacing is stretch-tuned reveals radically different s…
Stimulus-responsive peptide self-assembly provides a powerful method for controlling self-assembly as a function of environment. The development of a reductive trigger for peptide self-assembly and subsequent hydrogelation is described herein. A self-assembling peptide sequence, Ac-C(FKFE)(2)CG-NH(2), was cyclized via…
Flip to be square: Structural, spectroscopic, magnetic, and photomagnetic studies conclusively demonstrate that a tetranuclear cyanometalate {Fe2Co2} complex undergoes reversible thermally and light-induced changes in its optical and magnetic properties. This bistability is induced by an intramolecular electron transf…
We numerically produce fully amorphous assemblies of frictionless spheres in three dimensions and study the jamming transition these packings undergo at large volume fractions. We specify four protocols yielding a critical value for the jamming volume fraction which is sharply defined in the limit of large system size…
In the last few years, great attention has been paid to the preparation of polypropylene (PP) nanocomposites using carbon nanotubes (CNTs) due to the tremendous enhancement of the mechanical, thermal, electrical, optical and structural properties of the pristine material. This is due to the unique combination of struc…
Sulfide-based luminescent materials have attracted a lot of attention for a wide range of photo-, cathodo- and electroluminescent applications. Upon doping with Ce3+ and Eu2+, the luminescence can be varied over the entire visible region by appropriately choosing the composition of the sulfide host. Main application a…
We measure the room-temperature electron and hole field-effect mobilities (micro(FE)) of a series of alkanedithiol-treated PbSe nanocrystal (NC) films as a function of NC size and the length of the alkane chain. We find that carrier mobilities decrease exponentially with increasing ligand length according to the scali…
A variety of new multisegmented nanowires based on magnetic metals and conjugated polymers, polypyrrole (PPy) and poly(3,4-ethylenedioxythiophene) (PEDOT), were synthesized by an all-electrochemical template method for precise control over segment lengths. To overcome the major problem occurring when performing direct…
Silver/polylactide nanocomposites (Ag/PLA-NCs) were synthesized via chemical reduction method in diphase solvent. Silver nitrate and sodium borohydride were used as a silver precursor and reducing agent in the polylactide (PLA). The properties of Ag/PLA-NCs were studied as a function of the weight percentages of silve…
D-Tyrosyl-tRNA(Tyr) deacylase (DTD) is an editing enzyme that removes D-amino acids from mischarged tRNAs. The crystal structure of Plasmodium falciparum DTD (PfDTD) was determined using the iodide-SAD phasing method. Iodide-derivatized PfDTD crystals were obtained using the quick cryo-soaking procedure in which nativ…
Quasi‐static Weibull strength‐size scaling of hot‐pressed silicon carbide is described. Two surface conditions (uniaxial ground and uniaxial ground followed by grit blasting) were explored. Strength test coupons sampled effective areas from the very small (4 × 10 −3 mm 2 ) to the very large (4 × 10 4 mm 2 ). Equibiaxi…
Hysteresis observed in the resistive semiconductor-to-metal phase transition in VO2causes problems in bolometric readout, and thus is an obstacle in utilizing this strong phase transition in bolometric sensor applications. It is possible to avoid the unwanted hysteresis when operating in limited temperature ranges wit…
Three-dimensional superstructures of unique self-assemblies generated by exploring the conformational flexibility of various dipyrromethenes through creation of hydrogen-bonds with metal-halide anions are reported and the conformational diversity is thoroughly described in the solid and solution states by X-ray diffra…
The problem of image segmentation is considered. Popular thresholding methods are reviewed and tested on images presenting yarn of different hairiness. Results of image segmentation provided by the regarded thresholding approaches are presented, compared and analyzed. Especially their capabilities of extracting single…
Slow and fast growth textured polycrystalline rods of Fe82Ga18 have been annealed at 300 and 600 °C under 50 MPa of tensile stress for 20 min. The rods showed a built-in positive internal stress of ∼20 MPa (300 °C annealing) to ∼30 MPa (600 °C annealing), corresponding to an induced uniaxial anisotropy energy from −4…
An organic–inorganic hybrid compound (C5H9N3)ZnCl4 · H2O was synthesized by slow evaporation and characterized by single-crystal X-ray diffraction, differential scanning calorimetry, thermogravimetry, temperature-dependent X-ray powder diffraction, infrared spectroscopy, and some preliminary theoretical calculations o…
Magnetic poly(methyl methacrylate) nanocomposites were prepared using oleic acid coated cobalt ferrite and magnetite nanoparticles. Both nanofillers had a similar effect in shifting the glass transition temperature from that of the neat polymer. The cobalt ferrite nanocomposite had magnetic hysteresis at 2 and 300 K a…
A series of arylacetylene resins with siloxane units were synthesized by the condensation reactions of m-diethynylbenzene magnesium reagents with various <TEX>$\alpha,\omega$</TEX>-bis(chloro)dimethylsiloxanes. These resins are liquids and are miscible with common organic solvents at room temperature. The structures o…