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Ultralow-load hardness tester for use in a scanning electron microscope

H. Bangert、A. Wagendristel1985-08-01Review of Scientific Instruments

A new ultramicrohardness tester for a load range between 2×10−2 and 5×10−5 N is described. The instrument is operated inside a scanning electron microscope. Load is applied and measured by means of electrical signals thus making fully automized experiments possible. Typical examples demonstrate the capability of the d…

Force Microscopy Techniques and ApplicationsElectron and X-Ray Spectroscopy TechniquesIntegrated Circuits and Semiconductor Failure Analysis

Crystallization behavior of poly(3,3‐bisethoxymethyl oxetane) and poly(3,3‐bisazidomethyl oxetane)

K. E. Hardenstine、G. V. S. Henderson、L. H. Sperling 等 5 位作者1985-08-01Journal of Polymer Science Polymer Physics Edition

Abstract Two crystal modifications have been found for poly(3,3‐bisethoxymethyl oxetane) [poly‐ (BEMO)] by wide‐angle x‐ray powder diffraction and differential scanning calorimetry, while only one modification has been found for poly(3,3‐bisazidomethyl oxetane) [poly(BAMO)]. Melting temperatures for the two polymers w…

Polymer crystallization and propertiesPolymer Nanocomposites and Propertiesbiodegradable polymer synthesis and properties

THE MECHANICAL THRESHOLD OF DYNAMICALLY DEFORMED COPPER AND NITRONIC 40

P.S. Follansbee、U.F. Kocks、G. Regazzoni1985-08-01Le Journal de Physique Colloques

Measurements of the mechanical threshold, or threshold stress, are reported on quasi-statically and dynamically deformed copper and Nitronic 40. Results for copper show that the increase of the threshold stress with strain rate is similar to that of the flow stress. In Nitronic 40 the results show that the ratio of th…

High-Velocity Impact and Material Behavior

Cardiac Glycosides from the Roots ofStreblus asper

Vivek Saxena、Sanjay Chaturvedi1985-08-01Planta Medica

A new cardiac glycoside "vijaloside" in addition to well known cardenolide, asperosid (digitoxigenin-2',3'-di- O-methylglucopyranoside) have been isolated and identified from the roots of STREBLUS ASPER. Repeated chromatgraphic manipulations and spectral analysis (IR, (1)H-NMR, (13)C-NMR and Mass), suggested the struc…

Phytochemistry and Biological ActivitiesPhytochemical Studies and BioactivitiesPhytochemistry and Bioactive Compounds

Influence of Citric Acid on the Formation of Short-Range Ordered Aluminosilicates

Katsuhiro Inoue、Pan Huang1985-08-01Clays and Clay Minerals

Abstract Reactions between hydroxy-Al ions and orthosilicic acid as influenced by citric acid were studied at an initial Si concentration of 1.6 × 10 −3 M, Si/Al molar ratios of 0.5 and 1.0, OH/Al molar ratios of 1.0-3.0, and citric acid/Al molar ratios of 0-0.3. In the absence of citric acid and at OH/A1 ratios of 1.…

Mesoporous Materials and CatalysisClay minerals and soil interactionsIron oxide chemistry and applications

The Dielectric and Optical Properties of Technologically Important Mixtures

Amit Garg、V.K. Agarwal、Birendra Bahadur1985-08-01Molecular crystals and liquid crystals

Temperature variation of the dielectric permittivity, refractive indices, birefringence, density and order parameter of nematic liquid crystalline mixtures 1333, RO-TN 605, 2855, E-43 and ZLI-1565 are reported. The dielectric studies are in the frequency range 1 KHz to 3.5 MHz. The dielectric permittivity component pa…

Photonic and Optical DevicesLiquid Crystal Research AdvancementsPlant Reproductive Biology

Consideration on Filamentary Thermal Breakdown by Measuring Pre-Breakdown Current in Solid Dielectrics

Masayuki Hikita、Ippei Kanno、Goro Sawa 等 4 位作者1985-08-01Japanese Journal of Applied Physics

Filamentary thermal breakdown is discussed on the basis of experimental results on the electrical conduction just prior to breakdown in polyimide (PI) and polyethylene (PE) with a dc ramp voltage applied at 90°C. In PI, the pre-breakdown current was almost proportional to the electrode area S till about 100 µs before…

Advanced Sensor and Energy Harvesting MaterialsHigh voltage insulation and dielectric phenomenaDielectric materials and actuators

Some marine diatoms from the Australian region, especially from Port Phillip Bay and Tropical Nort-eastern Australia.

Stosch HA Von1985-08-01Brunonia

Ten taxa of marine diatoms from SE. or NE. Australia are described or redescribed, and their characters are supplemented by fine-structural and developmental data. One genus (Pseudoguinardia von Stosch), one species (Pseudoguinardia recta von Stosch), and two varieties (Odontella retiformis var. trigona von Stosch and…

Marine Biology and Ecology ResearchDiatoms and Algae ResearchIsotope Analysis in Ecology

Strength Recovery in Degraded Yttria‐Doped Tetragonal Zirconia Polycrystals

Roger L. K. Matsumoto1985-08-01Journal of the American Ceramic Society

The low‐temperature tetragonal‐monoclinic phase transformation in yttria‐doped tetragonal zirconia polycrystalline ceramics which results in strength degradation was found to be reversible. The retransformed ceramic has properties equivalent to those of the as‐sintered ceramic.

Advanced ceramic materials synthesisAdvanced materials and compositesNuclear materials and radiation effects

Rough‐surface crystallization: Some applications to poly(ethylene oxide)

D. M. Sadler1985-08-01Journal of Polymer Science Polymer Physics Edition

Abstract A model incorporating a rough (disordered) crystal growth surface is capable of treating many of the observations and measurements on the crystal growth of short chains of poly(ethylene oxide) from the melt. A simple preliminary treatment if presented which aims primarily to analyze the growth rate data withi…

Polymer crystallization and propertiesRheology and Fluid Dynamics StudiesCrystallization and Solubility Studies

Syntheses of MSn(OH)6 by coprecipitation and of MSnO3 by thermal decomposition (M = Mg, Co, Zn, Mn, Cd, Ca, Sr, Ba)

M. Inagaki、Tadafumi Kuroishi、Y. Yamashita 等 4 位作者1985-08-01Zeitschrift für anorganische und allgemeine Chemie

Abstract MSn(OH) 6 (M = Mg, Co, Zn, Mn, Cd, Ca, Sr, and Ba) and their solid solutions were synthesized by coprecipitation from aqueous solutions of Na 2 Sn(OH) 6 complex and MCl 2 . MSnO 3 and their solid solutions were prepared by thermal decomposition of these MSn(OH) 6 precipitates. Coprecipitation procedures were…

ZnO doping and propertiesNuclear materials and radiation effectsElectronic and Structural Properties of Oxides

Aliphatische Flüssigkristalle, 2. Einige nematische Derivate des all‐trans‐Perhydrophenanthrens

Wolfgang Sucrow、Hermann Minas、H. Stegemeyer 等 6 位作者1985-08-01Chemische Berichte

Abstract Die stereoselektive Synthese der all‐ trans ‐7‐Alkylperhydro‐2‐phenanthrenole 15a – f in 11 Stufen und 28 flüssigkristalline Ester 16 von 15a – f werden beschrieben, daneben einige weitere Derivate der 7‐Alkylperhydro‐2‐phenanthrenole. Vom Ester 16ec wurde eine Röntgenstrukturanalyse durchgeführt.

Liquid Crystal Research AdvancementsMolecular spectroscopy and chiralityAxial and Atropisomeric Chirality Synthesis

Glutathione-independent isomerization of maleylpyruvate by Bacillus megaterium and other gram-positive bacteria

S R Hagedorn、G. Bradley、P. J. Chapman1985-08-01Journal of Bacteriology

Maleylpyruvate, the ring fission product of gentisic acid, was found to be isomerized to fumarylpyruvate without a requirement for glutathione by an enzyme activity found in cell extracts of m-hydroxybenzoate-grown Bacillus megaterium 410. The isomerization reaction was detected as a shift in the absorbance maximum fr…

Enzyme Structure and FunctionPolyamine Metabolism and ApplicationsAldose Reductase and Taurine

The Properties of Electrochromic Film Electrodes of Lanthanide Diphthalocyanines in Ethylene Glycol

Gillian Collins、David J. Schiffrin1985-08-01Journal of The Electrochemical Society

The electrochromic properties of film electrodes of lutetium, erbium, gadolinium, and ytterbium diphthalocyanines in contact with ethylene glycol solutions have been studied. The stability of the electrochromic film under electrochemical cycling in this medium is at least three orders of magnitude better than that in…

Porphyrin and Phthalocyanine ChemistryElectrochemical Analysis and ApplicationsAnalytical Chemistry and Sensors

Adiabatic photodehydroxylation of 9-phenylxanthen-9-ol. Observation of carbocation fluorescence in neutral aqueous solution

Peter Wan、Keith Yates、Mary K. Boyd1985-08-01The Journal of Organic Chemistry

ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTAdiabatic photodehydroxylation of 9-phenylxanthen-9-ol. Observation of carbocation fluorescence in neutral aqueous solutionPeter Wan, Keith Yates, and Mary K. BoydCite this: J. Org. Chem. 1985, 50, 16, 2881–2886Publication Date (Print):August 1, 1985Publication History Publi…

Porphyrin and Phthalocyanine ChemistryAnalytical Chemistry and ChromatographyPhotochemistry and Electron Transfer Studies

Lattice thermal conductivity of small grain size PbSnTe and PbGeTe thermoelectric material

D.M. Rowe、C. M. Bhandari1985-08-01Applied Physics Letters

The effect of phonon grain-boundary scattering on the lattice thermal conductivity λL of PbSnTe and PbGeTe has been investigated theoretically as a function of grain size and doping. It is concluded that for optimally doped thermoelectric material with a mean grain size of 0.5 μm, the reductions in λL of PbSnTe and Pb…

Advanced Thermoelectric Materials and DevicesThermal properties of materialsThermal Radiation and Cooling Technologies

EXTRACTABLE Fe, Al, Si AND C IN B HORIZONS OF PODZOLIC AND BRUNISOLIC SOILS FROM ONTARIO

L. J. Evans、Ward Wilson1985-08-01Canadian Journal of Soil Science

To investigate the content of amorphous forms of Fe, Al and Si in podzolic soils, the B horizons from 54 Humo-Ferric Podzols and 24 Eluviated Dystric Brunisols were sampled in northern Ontario. Dithionite-citrate-bicarbonate (DCB) Fe d and Al d , acid NH 4 -oxalate Fe o , Al o and Si o , Na-pyrophosphate Fe p , Al p a…

Soil and Unsaturated FlowClay minerals and soil interactionsIron oxide chemistry and applications

Structural and electronic properties of six-coordinate manganese(III) porphyrin cations. Crystal and molecular structure of bis(N,N-dimethylformamide)(tetraphenylporphinato)manganese(III) perchlorate, [MnIII TPP(DMF)2]+ClO4-

Craig L. Hill、Michael M. Williamson1985-08-01Inorganic Chemistry

ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTStructural and electronic properties of six-coordinate manganese(III) porphyrin cations. Crystal and molecular structure of bis(N,N-dimethylformamide)(tetraphenylporphinato)manganese(III) perchlorate, [MnIII TPP(DMF)2]+ClO4-Craig L. Hill and Michael M. WilliamsonCite this: I…

Metal complexes synthesis and propertiesMagnetism in coordination complexesPorphyrin and Phthalocyanine Chemistry

Electrochemical investigation of electrochromism in transparent conductive oxides

Stuart F. Cogan、Elizabeth J. Anderson、Timothy D. Plante 等 4 位作者1985-08-01Applied Optics

Get PDF Email Share Share with Facebook Tweet This Post on reddit Share with LinkedIn Add to CiteULike Add to Mendeley Add to BibSonomy Get Citation Copy Citation Text Stuart F. Cogan, Elizabeth J. Anderson, Timothy D. Plante, and R. David Rauh, "Electrochemical investigation of electrochromism in transparent conducti…

Advanced Memory and Neural ComputingTransition Metal Oxide NanomaterialsAnalytical Chemistry and Sensors

Model calculation of the thermal conductivity of polymer crystals

C. L. Choy、S. P. Wong、K. Young1985-08-01Journal of Polymer Science Polymer Physics Edition

Abstract A linear lattice model without adjustable parameters provides an accurate description of the magnitude and temperature dependence of the thermal conductivity of K c of polyethylene crystals parallel (∥) and perpendicular (⟂) to the chain direction. The model shows that heat is transported principally by phono…

Polymer crystallization and propertiesThermal properties of materialsComposite Material Mechanics