Materials Literature
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Fundamental information concerning the mechanism of electron transfer from reduced heteropolytungstates (POM(red)) to O2, and the effect of donor-ion charge on reduction of O2 to superoxide anion (O2.-), is obtained using an isostructural series of 1e--reduced donors: alpha-X(n+)W12O40(9-n)-, X(n+) = Al3+, Si4+, P5+.…
In this study, a new Fourier transform infrared (FTIR) spectroscopy method for measuring lactide concentration in a polylactide (PLA) matrix is presented. The lactide ring breathing mode peak at 935 cm -1 is rationed against the asymmetric bending mode of methyl groups at 1454 cm -1; because the methyl group is presen…
Abstract The determination of kaolinite order-disorder by X-ray diffraction is problematic due to overlapping peaks from associated kaolin minerals and X-ray amorphous phases. This paper presents a new index (Aparicio-Gala´n-Ferrell index — AGFI), measured on 02 l and 11 l reflections after decomposing individual peak…
Hugoniot measurements on the highly dense, pure B4C polycrystal were performed by the inclined-mirror method to study the elastoplastic transition and to search phase transition. In inclined-mirror streak photographs, the smoothly jagged structure was observed at the free-surface shape in the plastic region. The Hugon…
Shape Memory Alloy (SMA) actuators, which have the ability to return to a predetermined shape when heated, have many potential applications such as aeronautics, surgical tools, robotics and so on. Although the conventional PID controller can be used with slow response systems, there has been limited success in precise…
This paper illustrates the use of electric field computation to optimize the design of gas filled high voltage composite bushings. The United States Navy employs these bushings in high power very low frequency/low frequency transmitting stations. Commercially available 2D and 3D computational packages based on the bou…
Potential of mean force (PMF) profiles of a single Na+ or K+ ion passing through a cyclic peptide nanotube, cyclo[-(D-Ala-Glu-D-Ala-Gln)2-], in water are calculated to provide insight into ion transport and to understand the conductance difference between these two ions. The PMF profiles are obtained by performing ste…
Do polypeptide chains ever behave like a random coil? In this report we demonstrate that glycine, the residue with the fewest backbone restrictions, exhibits a strong preference for an extended conformation in solution when polymerized in short segments of polyglycine. A model peptide system comprised of two unique tr…
An immunochromatography (ICG) strip test for rapid detection of atrazine in water samples was developed. A monoclonal antibody (MAb) specific to atrazine was produced from the cloned hybridoma cell (AT-1-M3) and used to develop a direct competitive enzyme-linked immunosorbent assay (DC-ELISA) and ICG strip. MAb conjug…
A series of poly(vinylphenol- b -vinylpyridine) (PVPh- b -P4VP) block copolymers were prepared through anionic polymerizations of 4- tert -butoxystyrene with 4-vinylpyridine followed by subsequent selective hydrolysis of the 4- tert -butoxystyrene protective groups. Infrared spectrum analysis suggests that this block…
Structure-sensitive properties of minor hysteresis loops have been compared with Vickers hardness and ductile-brittle transition temperature (DBTT) obtained by Charpy impact test for cold rolled low carbon steel. Minor loops were measured with increasing magnetic field amplitude, step by step, and were analyzed in con…
Copper hydroxy salts with a layer-type structure and general composition Cu2(OH)3X (X = NO3-, CH3COO- and ClO4-) were synthesized by co-precipitation (nitrate and acetate salts) and ion exchange (perchlorate salt) methods. The isolated polycrystalline solids were characterized by X-ray diffractometry, thermogravimetri…
The effects of space charges on hysteresis loops and field distributions in ferroelectrics have been investigated numerically using the phenomenological Landau-Ginzburg-Devonshire theory. Cases with the ferroelectric fully and partially depleted have been considered. In general, increasing the number of charged impuri…
Abstract Summary: Using a “never‐dried” procedure (according to Figure 4) shaped bacterial nanocellulose (BC, 1% cellulose, 99% water) has been modified by the formation of BC‐polymer composites. For this purpose, acrylate and methacrylate monomers and methacrylate crosslinkers were photopolymerized inside an ethanol‐…
A new trimethyltetrathiafulvalene (Me3TTF) derivative Me3TTF-CH=CH-py bearing a pyridyl was synthesized and coordinated to a cobalt(II) benzoate dimer, having paddlewheel core structure, leading to a complex formulated as Co2(PhCOO)4(Me3TTF-CH=CH-py)2. Single-crystal X-ray diffraction studies of the complex performed…
Brindley et al. (1951) reported the earliest efforts to obtain international collaboration on nomenclature and classification of clay minerals, initiated at the International Soil Congress in Amsterdam in 1950. Since then, national clay groups were formed, and they proposed various changes in nomenclature at group mee…
Luminescence and phosphorescence properties are investigated in two series of strontium aluminates, Sr4Al14O25:Eu2+ and SrAl2O4:Eu2+, codoped with rare earth (lanthanoid, Ln) ions. Persistent phosphorescence is observed for the phosphors codoped with Pr, Nd, Dy, Ho, and Er. In the phosphorescence process of these phos…
AlD3 AlD3 was synthesized by ball milling of 3LiAlD4 + AlCl3. Planetary ball milling at room temperature resulted in a mixture of AlD3 (alpha and alpha') and Al in addition to LiCl, whereas cryomilling at 77 K resulted in only AlD3 and LiCl. The AlD3 obtained was a mixture of about 2/3alpha and 1/3alpha'. Alpha' was d…
. –The evolution of biological materials is a critical, yet poorly understood, component in the generation of biodiversity. For example, the diversification of spiders is correlated with evolutionary changes in the way they use silk, and the material properties of these fibers, such as strength, toughness, extensibili…
The electronic structure of ferromagnetic 3d-transition metals in the vicinity of the Fermi level is dominated by the spin-polarized d bands. Experimentally, this energy region can be probed in detail by means of angle-resolved ultraviolet photoemission and inverse photoemission. In several earlier studies the measure…