Materials Literature
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The annealing and fading characteristics of CaF2:Tm (TLD-300) have been investigated. The best annealing temperature and time are given. The thermal treatment after exposure and before read out has also been studied. This work also reports the results of studies on fading in dark and light conditions. The stability of…
Abstract Infrared spectroscopy (4000–50 cm −1 ) was used to characterize the two crystalline modifications of poly(p‐phenylene terephthalamide). Polarized studies revealed that hydrogen bonds are oriented primarily perpendicular to the film plane in both forms. We also found that the crystalline modification coagulate…
Magnetometer surveys above gas pipelines show stress induced magnetic anomalies at pipe bends. This suggests a potential technique for the noninvasive monitoring of stress in buried pipelines, etc. Laboratory measurements of the magnetic field changes due to the elastic bending of 110 mm diameter pipe are presented. T…
Abstract A method has been developed for extracting the clay fraction from soil samples and using it for soil color comparisons. A syringe press has been constructed to aid the procedure.
For the complete nuclear fuel cycle, the development of a process for the co-conversion of Pu-U nitrate mixed solutions to mixed oxide powder has been performed along the line of non-proliferation policy of nuclear materials. A new co-conversion process using a microwave heating method has been developed and successfu…
Abstract Reactions of Ni(CH3)2(bpy) (1), Ni(C2H5)2(bpy) (2) (bpy=2,2′-bipyridine), trans-Ni(CH3)2(triethylphosphine)2 (3), Ni(CH3)2(1,2-bis(diphenylphosphino)ethane) (4), and Ni(CH3)2(1,3-bis(diphenylphosphino)propane) (5) with alkyl or aryl halides, R′COY (Y=Cl, Br, OC6H5, OCOC6H5), and CS2 have been investigated. Th…
Heat conduction is considered in a semi-infinite solid subjected to a high step change in surface heat flux, such that melting occurs. A time-dependent relaxation model for the energy flux is assumed, leading to a non-Fourier, non-linear equation for the thermal field, which is solved under suitable conditions on the…
The dynamic structure factors of crystals with sublattices which are mutually incommensurate are examined. The sublattices may be individually ordered, but incommensurate, or only one may be ordered with an interpenetrating fluid of the second atomic species. At high frequencies there are two propagating longitudinal-…
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTCrystal and molecular structures of 2,11-dithia- and 1,3,10,12-tetrathia[3.3](2,6)-pyridinophanesGeorge R. Newkome, Sebastiano Pappalardo, and Frank R. FronczekCite this: J. Am. Chem. Soc. 1983, 105, 15, 5152–5153Publication Date (Print):July 1, 1983Publication History Publi…
Abstract Blepharida sacra (Weise) is one of many species of flea beetles that have remarkable jumping abilities. The energy for its prodigious leaps is evidently stored in a central scroll‐shaped organ inside the hind femur of this insect—the metafemoral spring. X‐ray diffraction, scanning electron microscope, and ana…
Summary On-going field scaling tests have provided a unique opportunity to study how strontium sulfate and calcium sulfate scales are formed in an oil-producing well. Results indicate that development of nucleation sites on tubing surfaces is the most critical step. Scale profiles within a wellbore are determined main…
Glycolysis of rigid polyurethane foams is an efficient process for chemical recycling of waste products into raw materials. Secondary reactions leading, to some extent, to formation of amines are also involved in the process. The choice of catalyst is an important factor in selecting the type of reaction as well as th…
A new Monte Carlo simulation including generation of secondary electrons has been performed to study ultimate resolution in electron beam lithography. With respect to the simulations of inelastic scattering process of the primary electrons we used Gryzinski’s excitation function for single electron excitation processe…
We found that silver, either as silver metal or silver chloride, exerted toxic effects on the smooth muscle of isolated cannulated hamster cheek pouch arterioles. Silver initially stimulated the smooth muscle, producing a marked vasoconstriction. The vessels then dilated back to control diameters. Once the arterioles…
In the Staphylococcus aureus strain harbouring the plasmid RPAL, the resistance to aminoglycoside antibiotics results from two inactivating reactions catalyzed by a 6'-N-aminoglycoside acetyltransferase and a 2"-O-amino-glycoside phosphotransferase. These enzymes are copurified with a constant ratio between the two ac…
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTSwelling of model poly(dimethylsiloxane) networksR. W. Brotzman Jr. and B. E. EichingerCite this: Macromolecules 1983, 16, 7, 1131–1136Publication Date (Print):July 1, 1983Publication History Published online1 May 2002Published inissue 1 July 1983https://pubs.acs.org/doi/10.…
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTPotential dependence of surface-enhanced Raman scattering from citrate on colloidal silverC. G. Blatchford, O. Siiman, and Milton KerkerCite this: J. Phys. Chem. 1983, 87, 14, 2503–2508Publication Date (Print):July 1, 1983Publication History Published online1 May 2002Publish…
Abstract The resistance and resistivity of Ketjenblack EC/silicone rubber compounds were studied as function of strain in constant strain rate experiments. Both strain and rate of strain affect the electrical resistivity of the compounds. Such effects are carbon black concentration dependent. Ketjenblack EC, a low str…
Films selected for anticipated reaction with atomic oxygen, namely carbon, silver, and osmium, were exposed during the Shuttle STS‐4 mission. A silver film 225 ± 5 nm thick was converted to a transparent blue‐green interference film 355 ± 5 nm thick. Both carbon and osmium films 10‐30 nm thick apparently formed volati…
In an effort to advance our understanding of the principles governing the structures of and the hydrogen bonding in alkylammonium hexachlorostannates(IV), (R n NH 4−n ) 2 SnCl 6 , we have determined the room-temperature crystal structures of (Me 2 NH 2 ) 2 SnCl 6 and (Me 3 NH) 2 SnCl 6 (variants of the antifluorite st…