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Kinetic parameters in polymer degradation by dynamic thermogravimetric analysis

Leo Reich、H. T. Lee、D. W. Levi1965-01-01Journal of Applied Polymer Science

A new and relatively convenient procedure for obtaining kinetic parameters in the degradation of high polymers is described and the necessary experimental procedure is outlined. Results for the degradation of Teflon are compared with several previously reported methods and the agreement is found to be good. Some advan…

Polymer Science and PVCPolymer crystallization and propertiesThermal and Kinetic Analysis

Über Wismutnitrate. IV. Darstellung und Eigenschaften von Bi(NO3)3 · 5 H2O

G. Gattow、G. Kiel1965-01-01Zeitschrift für anorganische und allgemeine Chemie

Abstract Für das neutrale Salz, dessen Eigenschaften mitgeteilt werden, konnte die Zusammensetzung Bi(NO 3 ) 3 · H 2 O gesichert werden. Das thermische Verhalten des Bi(NO 3 ) 3 · 5 H 2 O wurde mittels isobarem Abbau, Aufheizversuchen und Differentialthermoanalyse untersucht und die Zersetzungsprodukte mit Hilfe von c…

Solid-state spectroscopy and crystallographyThermal and Kinetic AnalysisOrganometallic Compounds Synthesis and Characterization

Study on Solidification and Segregation of Stirred Ingot

Tadayoshi Takahashi、Iwao Hagiwara1965-01-01Journal of the Japan Institute of Metals and Materials

On the segregation of a steel or alloy ingot, the effect of stirring during the process of solidification appears to be an important factor to clarify the segregation phenomenon. In the present investigation on Al-Cu alloy, stirring was carried out by means of the method hydro-dynamically known as Taylor’s vortex flow…

Metallurgy and Material Science

Osmium Tetroxide Fixation of Rubber Latices

Koichi KATO1965-01-01Journal of Electron Microscopy

Journal Article Osmium Tetroxide Fixation of Rubber Latices Get access Koichi KATO Koichi KATO Central Research Laboratories, Toyo Rayon Company, Ltd.Otsu, Shiga-ken Japan Search for other works by this author on: Oxford Academic PubMed Google Scholar Journal of Electron Microscopy, Volume 14, Issue 3, 1965, Pages 219…

Electron and X-Ray Spectroscopy TechniquesAdvanced Materials Characterization TechniquesAnodic Oxide Films and Nanostructures

Thermal Conductivity of Sintered UO, and Al 2 O 3 at High Temperatures

T. Nishijima、Toshiyuki KAWADA、Akira Ishihata1965-01-01Journal of the American Ceramic Society

The thermal conductivities of sintered Al 2 O 3 and UO 2 were measured in the ranges 400° to 1700°C and 300° to 2100°C respectively. The conductivity values for Al 2 O 3 agreed with those reported previously at all temperatures investigated. The conductivity of UO, decreased with increasing temperature to a minimum of…

Nuclear reactor physics and engineeringNuclear Materials and PropertiesNuclear and radioactivity studies

726. The stability constants of magnesium citrate complexes

S S Tate、A. K. Grzybowski、S. P. Datta1965-01-01Journal of the Chemical Society (Resumed)

S. S. Tate, A. K. Grzybowski and S. P. Datta, J. Chem. Soc., 1965, 3905 DOI: 10.1039/JR9650003905

Magnetism in coordination complexesLanthanide and Transition Metal ComplexesMetal complexes synthesis and properties

Contribution à l'étude de la constante diélectrique de la cuprite. I. Détermination de la constante diélectrique par des méthodes optiques

C. Noguet、C. Schwab、C.T. Sennett 等 5 位作者1965-01-01Journal de physique

La constante diélectrique ε de Cu2O a été mesurée par une méthode optique et pour des nombres d'onde variant de 4 000 à 50 cm —1. La valeur de ε extrapolée donne : εstat = 7,5 ± 0,2. La courbe de dispersion peut-être représentée par une formule du type [FORMULE]faisant intervenir les deux fréquences actives dans l'inf…

Metallurgical Processes and ThermodynamicsX-ray Diffraction in CrystallographyCopper-based nanomaterials and applications

Electron Microscopic Observation of the Sporangial Structure of a Strain of Actinoplanes

Hubert A. Lechevalier、Pauline E. Holbert1965-01-01Journal of Bacteriology

Lechevalier, Hubert (Rutgers, The State University, New Brunswick, N.J.), and Pauline E. Holbert. Electron microscopic observation of the sporangial structure of a strain of Actinoplanes. J. Bacteriol. 89:217-222. 1965.-Actinoplanes sp. P 128 has polarly flagellated sporangiospores. The numerous flagella, formed by th…

Mesoporous Materials and CatalysisGenomics and Phylogenetic StudiesDiatoms and Algae Research

Decorative and Protective Finishes Produced on Aluminium

Hard Anodizing、B. A. Scott1965-01-01Transactions of the IMF

SummaryThe effects of anodizing aluminium of commercial purity (99%) in sulphuric acid at temperatures of -5° to +15°C and current densities of 20 to 80 A/ft2 for 20 to 80 minutes have been studied, with particular reference to appearance and resistance to abrasion. It has been shown that uniform self-coloured films r…

Anodic Oxide Films and NanostructuresAluminum Alloy Microstructure PropertiesCorrosion Behavior and Inhibition

Étude cristallographique de nouveaux sulfures de terres rares et de métaux alcalins M = Li, K

R. Ballestracci1965-01-01Bulletin de la Société française de Minéralogie et de Cristallographie

On décrit de nouveaux sulfures de terres rares et de métaux alcalins (Li, K). Les composés TLiS₂ (T = Pr à Y) ont une structure cubique du type NaCl, les atomes T et Li étant désordonnés ; pour les terres rares de rayons plus petits (Ho, Er, Yb), les atomes T et Li s'ordonnent et il apparaît une déformation rhomboédri…

Iron-based superconductors researchCrystal Structures and PropertiesInorganic Fluorides and Related Compounds

Diffraction des rayons X et des électrons par les molécules

C. Tavard、Marcel Rouault、Monique Roux1965-01-01Journal de Chimie Physique

L’aspect des phénomènes de diffraction des rayons X et des électrons par les molécules gazeuses est bien connu ; on sait en effet que les enregistrements photographiques de ces phénomènes permettent d’observer un ensemble d’anneaux concentriques, dont le centre coïncide avec la trace du faisceau direct.

Porphyrin and Phthalocyanine ChemistryPhotochemistry and Electron Transfer Studies

Alternating and rotational power loss at 50 c/s in 3% silicon-iron sheets

C.R. Boon、J.E. Thompson1965-01-01Proceedings of the Institution of Electrical Engineers

Alternating and rotational power losses at 50c/s have been measured at various flux densities for hot-rolled and cold-rolled 3% silicon iron in 0.013 in laminations, using an improved thermocouple method. The aim of the work was twofold:(a) to provide design data for the engineer on the magnitude of the power loss in…

Microstructure and Mechanical Properties of SteelsElectric Motor Design and AnalysisMagnetic Properties and Applications

Steam and heat setting of nylon 6 fiber. II. Effects of heat setting of nylon 6 fiber on dyeability and fine structure

Motohiro Tsuruta、Akio Koshimo1965-01-01Journal of Applied Polymer Science

Drawn and undrawn nylon 6 fibers subjected to dry heat setting or steam setting were dyed with an acid dyestuff and a direct dyestuff. The dye uptake of these fibers was determined, and the rate of diffusion of a disperse dyestuff was evaluated by the method of Kramer. For the drawn nylon 6, the dye uptake and the dif…

Dyeing and Modifying Textile FibersPolymer crystallization and propertiesPhotopolymerization techniques and applications

Calculation of the magnetic field of rotating machines. Part 4: Approximate determination of the field and the losses associated with eddy currents in conducting surfaces

R.L. Stoll、P. Hammond1965-01-01Proceedings of the Institution of Electrical Engineers

The paper discusses the relationship between the eddy currents flowing inside a conducting material and the magnetic field outside. The particular problem of a current sheet carrying a sinusoidally distributed current parallel to a conducting magnetic slab is examined in detail. It is shown that this mathematical mode…

Magnetic Properties and ApplicationsMaterial Properties and Failure MechanismsNon-Destructive Testing Techniques

Growth of BaTiO3 Crystals from TiO2-Rich Melt

Hiromu Sasaki1965-01-01Japanese Journal of Applied Physics

Single crystals of BaTiO 3 were grown from the TiO 2 -rich side of the BaO-TiO 2 system. They were chunky crystal with mainly {111} form. However, these chunky crystals are obtained only under a reduced atmospheric pressure. An oxygen defect seems to have an effect on the crystal morphology. Curie point of the present…

Ferroelectric and Piezoelectric Materials

The Reaction of Hydrogen with Graphite at 1200° to 1650°C

Earl A. Gulbransen、Kenneth F. Andrew、Fred A. Brassart1965-01-01Journal of The Electrochemical Society

The reaction was studied at 19 Torr pressure under static and flow conditions. Rates of reaction up to were measured at 1650°C and 19 Torr. The rates of reaction were nearly independent of flow and pressure. The kinetic data could be fitted to an Arrhenius‐type equation , where . Mass spectrometer studies of the react…

Graphite, nuclear technology, radiation studiesNuclear Physics and ApplicationsAdvanced Chemical Physics Studies

Heats of formation of the ?-brasses

Raymond L. Orr、B.B. Argent1965-01-01Transactions of the Faraday Society

R. L. Orr and B. B. Argent, Trans. Faraday Soc., 1965, 61, 2126 DOI: 10.1039/TF9656102126

Metallurgy and Material Science