Materials Literature
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Abstract Epoxides from a variety of unsaturated fatty acids were prepared, and corrosion tests for these products as water‐based cutting fluid additives were performed. The triethanolamine salt of an epoxide of undecylenic acid showed very effective rust‐inhibiting properties in a water‐based cutting fluid.
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTOsmotic swelling of poly(vinyl acetate) gels at the .THETA. temperatureFerenc Horkay, Erik Geissler, Anne Marie Hecht, and Miklos ZrinyiCite this: Macromolecules 1988, 21, 8, 2589–2594Publication Date (Print):August 1, 1988Publication History Published online1 May 2002Publis…
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTMicrodomain characterization of styrene-imidazole copolymersR. C. Sutton, L. Thai, J. M. Hewitt, C. L. Voycheck, and J. S. TanCite this: Macromolecules 1988, 21, 8, 2432–2439Publication Date (Print):August 1, 1988Publication History Published online1 May 2002Published inissu…
Abstract The thermal decomposition of a fibrous talc was studied by transmission electron microscopy (TEM) and selected-area electron diffraction (SAD). Small changes in the lengths of a and b unit-cell parameters were noticeable at 500°C, but the talc laths did not change morphologically until 800°C. At this temperat…
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTA theoretical study of the interaction of acetylene with copper and silver monoionsJosefa Miralles-Sabater, Manuela Merchan, Ignacio Nebot-Gil, and Pedro M. Viruela-MartinCite this: J. Phys. Chem. 1988, 92, 17, 4853–4859Publication Date (Print):August 1, 1988Publication Hist…
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTNew low-temperature synthesis of transition-metal sulfidesMichael J. Martin, Guo Hua Qiang, and Donald M. SchleichCite this: Inorg. Chem. 1988, 27, 16, 2804–2808Publication Date (Print):August 1, 1988Publication History Published online1 May 2002Published inissue 1 August 19…
Abstract Nitridation of polycrystalline titanium was investigated in situ at about 550°C by angle‐resolved x‐ray photoelectron spectroscopy (XPS). The nitrogen pressure was varied from 10 −4 mbar to 1 mbar. The distribution of nitrogen in the titanium and the chemical bonding present were deduced from XPS measurements…
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTCoordination chemistry of new sulfur containing ligands. 28. Syntheses and characterization of two vanadium tris complexes of the 1,2-dithiolene 5,6-dihydro-1,4-dithiin-2,3-dithiolate. Crystal structure of [(C4H9)4N][V(DDDT)3]Jane Hanna Welch, Robert D. Bereman, and Phirtu S…
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTExtended x-ray absorption fine structure study of molybdenum/alumina samples prepared by equilibrium adsorption of ammonium heptamolybdateC. T. J. Mensch, J. A. R. Van Veen, B. Van Wingerden, and M. P. Van DijkCite this: J. Phys. Chem. 1988, 92, 17, 4961–4964Publication Date…
Hardness was measured as a function of temperature (20° to 1000°C) for several Al 2 O 3 ceramics, including single‐crystal sapphire and polycrystalline aluminas containing different amounts of second phase. Hardness decreased steadily with increasing temperature for all materials tested, in accordance with a semiempir…
The behavior of a two-dimensional orientation field has been studied directly in space and time. In a freely suspended thin film of tilted smectic liquid crystal the local projection onto the film plane of the molecular orientation averaged through the film forms a two-dimensional (2D) vector field C^(x,y) with local…
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTRemarkably inert metal alkyl linkages in alkyl dioxo complexes of molybdenum and tungstenPeter Legzdins, Everett C. Phillips, Steven J. Rettig, Luis Sanchez, James Trotter, and Vivien C. YeeCite this: Organometallics 1988, 7, 8, 1877–1878Publication Date (Print):August 1, 19…
Methods are described for the analysis of electron micrographs of regular biological objects. Fourier-based processing of one-dimensionally ordered arrays is described by way of introduction, before analysing two-dimensional crystals in projection with the aim of enhancing signal:noise ratio and thus of feint features…
Abstract The infrared absorption spectra of a palygorskite sample from Cáceres, Spain, showed two previously unreported bands in the OH-stretching region at 3420–3440 and 3220–3230 cm −1 after evacuation at 90°–230°C. These bands, which reached maximum intensity after the sample was heated at 150°C, were assigned to O…
Crystallization of an MgO‐Al 2 O 3 ‐SiO 2 ‐ZrO 2 sintered glass frit was studied. Heat treatment at 850° or 900°C caused initial crystallization of μ‐cordierite and tetragonal ( t ) ZrO 2 . The t ‐ZrO 2 crystallized with an irregular dendritic morphology and could be transformed to monoclinic ( m ) symmetry under cert…
The crystal chemistry of 16 groups of multiple‐chain, sheet, and framework silicates is reviewed. Crystal structure drawings are presented to illustrate crystal chemical features necessary to interpret chemical data for each mineral group. The 16 silicate groups considered in this review are the amphibole; nonclassica…
LCAO-CPA theory is applied to substitutionally disordered ferromagnetic BCC FeCo alloys. Calculations are based on charge and spin self-consistent LCAO parameters determined for the pure component metals within the local spin density functional theory. Effects of charge and spin self-consistency on the alloy magnetisa…
Simultaneous measurements of load, deformation and diameter were performed on stretched collagen fiber bundle from rat tail tendon using a dynamic, electronically controlled stretch system and a novel computer based electroptical set-up. A parallel analysis of glycosaminoglycan (GAG) concentration in the bathing solut…
We present the phase diagram of a binary system of two nematogenic terminal, non-polar compounds in which an induced smectic A phase appears over a large concentration–temperature range. X-ray measurements give evidence that the layer spacing, d, of this induced smectic A phase is clearly larger than the average molec…
The magnetic properties of Fe-Mn-Al alloys in the disordered phase are investigated through the M\"ossbauer technique. The magnetic phase diagram in the bcc structural phase is obtained as a function of the Al concentration ($q$) and Mn concentration ($x$). The site-diluted Ising model proposed in a previous study of…