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New Semiquinone/Catecholate Complexes That Exhibit Valence Tautomerism. Synthesis and Characterization of MnIII(thf)2(3,6-DBSQ)(3,6-DBCat) and Observations on the MnIV(3,6-DBSQ)2(3,6-DBCat)/MnIII(3,6-DBSQ)3 Equilibrium in the Solid State

Attia、Cortlandt G. Pierpont1998-05-15Inorganic Chemistry

Irradiation of a THF solution containing Mn 2 (CO) 10 and 3,6-di- tert -butyl-1,2-benzoquinone (3,6-DBBQ) gave dark green crystals of Mn(thf) 2 (3,6-DBQ) 2 . Structural characterization has shown that the inner coordination geometry about the metal has the axially elongated trans structure that appears characteristica…

Metal complexes synthesis and propertiesLanthanide and Transition Metal ComplexesMagnetism in coordination complexes

Hyperbranched Poly(ε-caprolactone)s

Mikael Trollsås、Björn Atthoff、Hans Claesson 等 4 位作者1998-05-15Macromolecules

Novel hyperbranched poly(ε-caprolactone)s have been synthesized. The versatile synthesis utilizes AB 2 macromonomers and allows the thermo-physical properties of the polymers to be tailored. The ε-caprolactone-based AB 2 macromonomers were synthesized through living ring opening polymerization, using aluminum benzylox…

Dendrimers and Hyperbranched PolymersRNA Interference and Gene DeliveryPolymer Surface Interaction Studies

Self-Consistent Calculations of Block Copolymer Solution Phase Behavior

Ching‐I Huang、Timothy P. Lodge1998-05-15Macromolecules

We present a theoretical study of the influence of solvent on ordered block copolymer solutions. The phase behavior is examined as a function of solvent selectivity, temperature, copolymer concentration, composition, and molecular weight. Phase maps are constructed using self-consistent mean-field (SCMF) theory, via t…

Theoretical and Computational PhysicsRheology and Fluid Dynamics StudiesBlock Copolymer Self-Assembly

Development of ferroelectric mixed states in a random field of static defects

S. Semenovskaya、A. G. Khachaturyan1998-05-15Journal of Applied Physics

A para→ferroelectric stress-free transition in a random field of static defects is studied by the computer simulation method. It is shown that the electrostatic dipole–dipole interaction may produce in the ferroelectric transition the same “martensitelike” effects as the strain-induced interaction in the martensitic t…

Ultrasonics and Acoustic Wave PropagationAcoustic Wave Resonator TechnologiesFerroelectric and Piezoelectric Materials

Exciton fine structure in CdSe nanoclusters

K. T. Leung、Simone Pokrant、K. Birgitta Whaley1998-05-15Physical review. B, Condensed matter

The fine structure in the CdSe nanocrystal absorption spectrum is computed by incorporating two-particle electron-hole interactions and spin-orbit coupling into a tight-binding model, with an expansion in electron-hole single-particle states. The exchange interaction and spin-orbit coupling give rise to dark, low-lyin…

Chalcogenide Semiconductor Thin FilmsQuantum Dots Synthesis And PropertiesPerovskite Materials and Applications

High-Pressure, High-Temperature Synthesis and Characterization of Boron Suboxide (B6O)

H. Hubert、L. A. J. Garvie、Bertrand Devouard 等 6 位作者1998-05-15Chemistry of Materials

Boron suboxide, nominally B 6 O, was synthesized by reducing B 2 O 3 with B up to 10 GPa in a multianvil press at temperatures between 1200 and 1800 °C. The samples were characterized by powder X-ray diffraction, scanning electron microscopy, transmission electron microscopy, and parallel electron energy-loss spectros…

Boron and Carbon Nanomaterials ResearchMXene and MAX Phase MaterialsAdvanced ceramic materials synthesis

High-resolution surface-sensitive C1score-level spectra of clean and hydrogen-terminated diamond (100) and (111) surfaces

R. Graupner、Florian Maier、J. Ristein 等 5 位作者1998-05-15Physical review. B, Condensed matter

The carbon $1s$ core levels of diamond (100) and (111) surfaces were investigated using high-resolution photoelectron spectroscopy. The surfaces were prepared in a hydrogen plasma, which is known to result in atomically flat surfaces. From the signature of the C $1s$ core-level spectra, four different surface terminat…

High-pressure geophysics and materialsDiamond and Carbon-based Materials ResearchAdvanced Chemical Physics Studies

Solvent dependence of the first hyperpolarizability of p-nitroanilines: Differences between nonspecific dipole–dipole interactions and solute–solvent H-bonds

François L. Huyskens、P. Huyskens、André Persoons1998-05-15The Journal of Chemical Physics

In this paper, the influence of solvents on the first hyperpolarizability β of nonlinear optical (NLO) molecules is studied at 25 °C for solutions of p-nitroaniline and N,N-dimethyl paranitroaniline in some 50 solvents belonging to different classes. The hyperpolarizabilities deduced from measured hyper-Rayleigh scatt…

Nonlinear Optical Materials ResearchChemical synthesis and pharmacological studiesPhotochemistry and Electron Transfer Studies

Photoemission and x-ray-absorption study of boron carbide and its surface thermal stability

I. Jiménez、D. G. J. Sutherland、T. van Buuren 等 6 位作者1998-05-15Physical review. B, Condensed matter

We present a photoemission and x-ray-absorption study on boron carbide which identifies the spectroscopic features of this material, discussing them in connection with current structural models. A study on the surface thermal stability is also performed, revealing that despite the high melting point of boron carbide $…

Diamond and Carbon-based Materials ResearchAdvanced ceramic materials synthesisBoron and Carbon Nanomaterials Research

Magnetization Plateaus in NH 4CuCl 3

W. Shiramura、K. Takatsu、Budhy Kurniawan 等 9 位作者1998-05-15Journal of the Physical Society of Japan

The magnetic susceptibility and high-field magnetization process of NH 4 CuCl 3 with double chains of CuCl 3 have been measured using single crystals. No anomaly indicative of the three-dimensional ordering is observed in susceptibility data above 1.7 K. It is found, by magnetization measurement down to 0.5 K, that in…

Solid-state spectroscopy and crystallographyPerovskite Materials and ApplicationsAdvanced Condensed Matter Physics

Ultrafast dynamics of hot electrons and holes in copper: Excitation, energy relaxation, and transport effects

E. Knoesel、A. Hötzel、Martin Wolf1998-05-15Physical review. B, Condensed matter

Time-resolved two-photon photoemission (2PPE) at various photon energies is used to investigate the relaxation dynamics of hot electrons in Cu(111), applying auto- and cross-correlation techniques. The relaxation times vary from 250 fs at 0.1 eV above the Fermi level to 20 fs at 2 eV and show a strong wavelength depen…

Advanced Chemical Physics StudiesSurface and Thin Film PhenomenaElectron and X-Ray Spectroscopy Techniques

Electronic structure ofV2O5: Role of octahedral deformations

Volker Eyert、K.‐H. Höck1998-05-15Physical review. B, Condensed matter

We present results of all-electron electronic-structure calculations for semiconducting vanadium pentoxide. The calculations are based on density-functional theory within the local-density approximation and employ the augmented spherical wave method in its scalar-relativistic implementation. The electronic properties…

Transition Metal Oxide NanomaterialsGa2O3 and related materialsCatalysis and Oxidation Reactions

Influence of temperature on the electromechanical and fatigue behavior of piezoelectric ceramics

Donny Wang、Yevgeniy Fotinich、Greg P. Carman1998-05-15OpenAlex

This paper presents research results on the electro–thermomechanical behavior of piezoelectric ceramics for use in actuator applications with an emphasis on ferroelectric fatigue. The material being investigated is a lead zirconate titanate piezoelectric ceramic with the composition PbZr0.53Ti0.47O3 (PZT-5H). Results…

Numerical methods in engineeringFerroelectric and Piezoelectric MaterialsUltrasonics and Acoustic Wave Propagation

Systematic study of the electronic state in θ-type BEDT-TTF organic conductors by changing the electronic correlation

Hatsumi Mori、Shōji Tanaka、Takehiko Mori1998-05-15OpenAlex

The behavior of the phase transitions is mapped out as a function of the dihedral angle (\ensuremath{\theta}) or the transfer integral $(t)$ between donor columns for \ensuremath{\theta}-type BEDT-TTF [BEDT-TTF: bis(ethylenedithio)tetrathiafulvalene, abbreviated as ET] salts involving the series $\ensuremath{\theta}\e…

Organic and Molecular Conductors ResearchMagnetism in coordination complexesMolecular Junctions and Nanostructures

Ferromagnetism in LaFeO 3 -LaCrO 3 Superlattices

K. Ueda、Hitoshi Tabata、Tomoji Kawai1998-05-15OpenAlex

Ferromagnetic spin order has been realized in the LaCrO3-LaFeO3 superlattices. Ferromagnetic coupling between Fe3+ and Cr3+ through oxygen has long been expected on the basis of Anderson, Goodenough, and Kanamori rules. Despite many studies of Fe-O-Cr-based compounds, random positioning of Fe3+ and Cr3+ ions has frust…

Advanced Condensed Matter PhysicsMagnetic and transport properties of perovskites and related materialsMultiferroics and related materials

Impurity Scattering in Carbon Nanotubes – Absence of Back Scattering –

Tsuneya Ando、Takeshi Nakanishi1998-05-15OpenAlex

The effective potential of an impurity in a k · p scheme is derived in two-dimensional graphite sheet. When the potential range is smaller than the lattice constant, it has an off-diagonal matrix element between K and K ′ points comparable to the diagonal element. With the increase of the range, this off-diagonal elem…

Graphene research and applicationsCarbon Nanotubes in CompositesThermal properties of materials

Porous Shape Persistent Fluorescent Polymer Films: An Approach to TNT Sensory Materials

Jye‐Shane Yang、Timothy M. Swager1998-05-15OpenAlex

ADVERTISEMENT RETURN TO ISSUEPREVCommunicationNEXTPorous Shape Persistent Fluorescent Polymer Films: An Approach to TNT Sensory MaterialsJye-Shane Yang and Timothy M. SwagerView Author Information Department of Chemistry Massachusetts Institution of Technology 77 Massachusetts Ave., Cambridge, Massachusetts 02139 Cite…

Luminescence and Fluorescent MaterialsOrganic Electronics and PhotovoltaicsPhotochemistry and Electron Transfer Studies

On the optical band gap of zinc oxide

V. Srikant、David R. Clarke1998-05-15OpenAlex

Three different values (3.1, 3.2, and 3.3 eV) have been reported for the optical band gap of zinc oxide single crystals at room temperature. By comparing the optical properties of ZnO crystals using a variety of optical techniques it is concluded that the room temperature band gap is 3.3 eV and that the other values a…

Ga2O3 and related materialsZnO doping and propertiesGas Sensing Nanomaterials and Sensors

Mimicking Cytochrome P-450 2B4 and Aromatase: Aromatization of a Substrate Analogue by a Peroxo Fe(III) Porphyrin Complex

Diana L. Wertz、Marlene F. Sisemore、Matthias Selke 等 5 位作者1998-05-14Journal of the American Chemical Society

ADVERTISEMENT RETURN TO ISSUEPREVCommunicationNEXTMimicking Cytochrome P-450 2B4 and Aromatase: Aromatization of a Substrate Analogue by a Peroxo Fe(III) Porphyrin ComplexDiana L. Wertz, Marlene F. Sisemore, Matthias Selke, Jennifer Driscoll, and Joan Selverstone ValentineView Author Information Department of Chemistr…

Porphyrin and Phthalocyanine ChemistryPorphyrin Metabolism and DisordersPhotosynthetic Processes and Mechanisms

Magnon modes and magnon-vortex scattering in two-dimensional easy-plane ferromagnets

B. A. Ivanov、H. J. Schnitzer、F. G. Mertens 等 4 位作者1998-05-14arXiv

We calculate the magnon modes in the presence of a vortex in a circular system, combining analytical calculations in the continuum limit with a numerical diagonalization of the discrete system. The magnon modes are expressed by the S-matrix for magnon-vortex scattering, as a function of the parameters and the size of…

Materials Science