Materials Literature
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A novel approach toward the synthesis of hollow silver nanoparticle (NP) cages built with building blocks of silver NPs by layer-by-layer (LbL) assembly is demonstrated. The size of the NP cage depends on the size of template used for the LbL assembly. The microcages showed a uniform distribution of spherical silver n…
The analytical performance of high-resolution scanning electron microscopy/energy dispersive X-ray spectroscopy (SEM/EDX) for accurate determination of the size, size distribution, qualitative elemental analysis of nanoparticles (NPs) was systematically investigated. It is demonstrated how powerful high-resolution SEM…
In this paper, we report on the precise determination of the orientation of NV centers by imaging with a radially polarized beam. Vectorial Debye theory is applied to the field in the focus of radially polarized beams to generate emission profiles of two orthogonal optical dipoles. By comparing features of the measure…
The cubic ReO 3 -type material ScF 3 exhibits strong isotropic negative thermal expansion (NTE) over a wide temperature range while remaining cubic. Control of its thermal expansion was investigated by forming Sc 1- x Ti x F 3 solid solutions, which were characterized by synchrotron powder diffraction at ambient press…
Structural phase transitions driven by oxygen-vacancy ordering can drastically affect the properties of transition metal oxides. The focused electron beam of a transmission electron microscope (TEM) can be used to control structural phase transitions in epitaxial La2/3Sr1/3MnO3. The ability to induce and characterize…
Cellulose acetate (CA), polyethylene oxide (PEO) copolymer blend was prepared using γ-rays as initiator. PEO as an additive was added with different concentrations (0 – 5%) based on cellulose acetate. As the PEO is water soluble, some portions of them were extracted into aqueous solution. To overcome this, the PEO add…
In this paper, we discuss a phenomenological approach for the numerical modeling of static hysteresis of grain oriented (GO) steels at macro-magnetic scale. The modeling is inspired to a generalization in 2-d of the Preisach model (this generalization can be easily extended in 3-d, but it is not necessary here), and t…
Electromigration (EM) has become a major power grid reliability problem in VLSI. In this paper, we first demonstrate that EM reliability analysis of a power grid can be converted to analyzing EM reliability of the grid vias. We develop a model for calculating EM lifetime of via-arrays and observe that making power gri…
The hydrogen storage capacity of nanoporous carbons can be enhanced through metal doping, for instance doping with palladium. However, there are two problems that may limit the positive effect of metal doping on the reversible storage capacity. First, clustering of the metal atoms decreases its effectiveness, which is…
An experimental technique for in situ and real-time monitoring of mechanochemical reactions in a shaker ball mill was recently described, which utilises highly penetrating X-ray radiation available at the ID15B beamline of the European Synchrotron Radiation Facility. Herein, we describe the first attempts to perform s…
Hyptis suaveolens leaf extract (HSLE) as corrosion inhibitor in 1 M H 2 SO 4 was evaluated using mass loss measurement as well as potentiodynamic polarization and electrochemical impedance spectroscopy measurements. The extract was found to efficiently inhibit the corrosion process in 1 M H 2 SO 4 and inhibition effic…
The design of stacks of layered materials in which adjacent layers interact by van der Waals forces[1] has enabled the combination of various two-dimensional crystals with different electrical, optical and mechanical properties, and the emergence of novel physical phenomena and device functionality[2-8]. Here we repor…
We report preparation of large area quasi-one-dimensional (1D) monolayer graphene superlattices on a prototypical high-index surface Cu(410)-O and characterization by Raman spectroscopy, Auger electron spectroscopy, low-energy electron diffraction, scanning tunneling microscopy, and scanning tunneling spectroscopy. Th…
To understand from first principles how spin and charge fluctuations affect quasiparticle excitations, start with simple alkali metals, not high-Tc superconductors. Spin fluctuations alone cannot account for the experimentally observed reduction in occupied bandwidth.
Plastic thermo-electrochemical cells (thermocells) involving aqueous potassium ferricyanide/ferrocyanide electrolyte have been investigated as an alternative to conventional thermoelectrics for thermal energy harvesting. Plastic thermocells that consist of all pliable materials such as polyethylene terephthalate (PET)…
The spin-dependent electronic structures of aluminum-(Al) doped zigzag silicene nanoribbons (ZSiNRs) are investigated by first-principles calculations. When ZSiNRs are substitutionally doped by a single Al atom on different sites in every three primitive cells, they become half-metallic in some cases, a property that…
We investigate spatial adiabatic passage processes for sound waves propagation in sonic crystals, consisting of steel cylinders embedded in a water host medium, that present two linear defects. This work constitutes an extension of the well-known quantum optical rapid adiabatic passage technique to the field of sound…
The electronic properties of graphene nano-flakes (GNFs) with different edge passivation are investigated by using density functional theory. Passivation with F and H atoms is considered: C(N(c)) X(N(x)) (X = F or H). We studied GNFs with 10 < Nc < 56 and limit ourselves to the lowest energy configurations. We found t…
The rich phase diagram of the two dimensional electron gas (2DEG) at the \STO/\LAO interface is probed using Hall and longitudinal resistivity. Thanks to a special bridge design we are able to tune through the superconducting transition temperature T$_c$ and to mute superconductivity by either adding or removing carri…
We point out the erroneous reasoning and disprove the conclusions contained in a recent preprint by A. H. Bougourzi (arxiv:1402.3855v1) concerning the spin structure factor of the Heisenberg model at zero field in the thermodynamic limit, as calculated using the vertex operator approach.