Materials Literature
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A multiple-elastic shell model is applied to systematically study free vibration of multiwall carbon nanotubes (MWNTs). Using Flugge [Stresses in Shells (Springer, Berlin, 1960)] equations of elastic shells, vibrational frequencies and associated modes are calculated for MWNTs of innermost radii 5 and 0.65 nm, respect…
This paper reports on the synthesis, X-ray structure, magnetic properties, and DFT calculations of [[HC(CMeNAr)2]Mn]2 (Ar = 2,6-iPr2C6H3) (2), the first complex with three-coordinate manganese(I). Reduction of the iodide [[HC(CMeNAr)2]Mn(mu-I)]2 (1) with Na/K in toluene afforded 2 as dark-red crystals. The molecule of…
Chiral poly(3-(3,7-dimethyloctyloxy)thiophene)s were prepared using three different methodologies, rendering polymers with different degrees of regioregularity. In a first attempt, 3-alkoxythiophene was polymerized using FeCl 3, resulting in a highly regioirregular poly(3-alkoxythiophene). Second, the GRIM methodology…
Diffusion exchange of dextran with molecular weights 4.4 and 77 kDa through polyelectrolyte multilayer (PEM) hollow capsules consisting of four bilayers of polystyrene sulfonate/polydiallyldimethylammonium chloride has been investigated using two-dimensional nuclear-magnetic-resonance methods: diffusion-diffusion exch…
Biotinylated immunoliposomes were prepared by a non-covalent (biotin-streptavidin) coupling procedure and conjugated to the OX26 monoclonal antibody directed against the rat transferrin receptor. In vitro, these biotinylated immunoliposomes were used to by-pass P-glycoprotein in multidrug-resistant RBE4 brain capillar…
Gold nanoparticle (NP) mono- and multilayers were constructed on gold surfaces using coordination chemistry. Hydrophilic Au NPs (6.4 nm average core diameter), capped with a monolayer of 6-mercaptohexanol, were modified by partial substitution of bishydroxamic acid disulfide ligand molecules into their capping layer.…
We present the first synthesis of double coaxial carbon nanotubes with nitrogen-doped and boron-doped multiwalls by the template technique with two-step chemical vapor deposition. X-ray photoelectron spectra confirm the coaxial formation of different-doped structures. The electrical conductance and oxygen chemisorptio…
Hydrothermally stable and structrurally ordered mesoporous and microporous aluminosilicates with different pore sizes have been synthesized to immobilize cytochrome c (cyt c): MAS-9 (pore size 90 A), MCM-48-S (27 A), MCM-41-S (25 A), and Y zeolites (7.4 A). The amount of cyt c adsorption could be increased by the intr…
The metal-support interaction of a dispersed Pt atom on H-ZSM-5 zeolite has been investigated by using an embedded cluster and cluster models with the density functional theory/B3LYP functional method. We found that the Pt atom interacts with a Brønsted proton and a nearby framework oxygen. Interaction with the framew…
Two discretizations, linear and nonlinear, of basic notions of the complex analysis are considered. The underlying lattice is an arbitrary quasicrystallic rhombic tiling of a plane. The linear theory is based on the discrete Cauchy-Riemann equations, the nonlinear one is based on the notion of circle patterns. We clar…
Magnetic tunnel junctions (MTJs) with a Co2FeAl Heusler alloy electrode are fabricated by the deposition of the film using an ultrahigh vacuum sputtering system followed by photolithography and Ar ion etching. A tunnel magnetoresistance (TMR) of 47% at room temperature (RT) are obtained in a stack of Co2FeAl∕Al–Ox∕Co7…
Abstract In the present study, we investigate pseudoelastic pull – pull cycling of ultra-fine-grained (40 nm) Ni-rich (50.9 at.% Ni) NiTi shape-memory wires at temperatures ranging from 301 to 323 K. Strain-controlled experiments were performed using incremental strain steps and different constant maximum strains. Pul…
The objective of this work was to develop a PSPICE-compatible equivalent circuit of a thermoelectric cooler (TEC). Equivalent circuits are convenient tools for power electronics engineers since they help in presenting a problem in electronic circuit terms and can assist in the design of power stages and the control ci…
ABSTRACT ASTM A‐36 medium carbon steel, 110 copper, 3003‐H14 aluminum, polyvinylchloride (PVC) type 1 and 304 stainless steel coupons were immersed in electrolyzed (EO) water, chlorine water, modified EO water and deionized water for a period of 8 days, and the properties of these types of water, weights and surface r…
This paper presents a discussion of the concept of threshold for trapped space charge accumulation in solid dielectrics submitted to a DC field. The starting point is the fact that it is often possible to define a critical field separating an ohmic type of conduction from a nonlinear regime in the current-voltage char…
A second-order finite-element adaptive strategy with error control for one-dimensional grating problems is developed. The unbounded computational domain is truncated to a bounded one by a perfectly-matched-layer (PML) technique. The PML parameters, such as the thickness of the layer and the medium properties, are dete…
In this study, the microstructure and phase transformation behaviour of Ti–50.8 at.% Ni alloy severely deformed using equal channel angular extrusion (ECAE) were investigated. The aim of the study was to reveal the effect of severe plastic deformation on the interplay between plastic deformation via dislocation slip a…
Magnetization reversal in exchange-spring magnet films has been investigated by a first-order reversal curve (FORC) technique and vector magnetometry. In Fe/epitaxial-SmCo films, the reversal proceeds by a reversible rotation of the Fe soft layer, followed by an irreversible switching of the SmCo hard layer. The switc…
EFICIENT USAGE OF SOFT MATERIALS UNDER IMPACT LOADING CONDITIONS REQUIRES ACCURATE AND RELIABLE DESCRIPTIONS OF THE HIGH-RATE MECHANICAL RESPONSES OF SUCH MATERIALS, WHICH MOTIVATES RECENT DEVELOPMENT OF VALID AND E±CIENT DYNAMIC EXPERIMENTAL TECHNIQUES. SPLIT HOPKINSON PRESSURE BAR (SHPB) HAS BEEN EXTENSIVELY USED TO…
Patterning of semiconductor surfaces is an area of intense interest, not only for technological applications, such as molecular electronics, sensing, cellular recognition, and others, but also for fundamental understanding of surface reactivity, general control over surface properties, and development of new surface r…