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Ein neues Oxocuprat(III): Na3CuO3

Klaus Hestermann、Rudolf Hoppe1969-07-01Zeitschrift für anorganische und allgemeine Chemie

Abstract Neu dargestellt wurde Na 3 CuO 3 durch Erhitzen von Na 2 O 2 /CuO‐Mischungen auf 630°C unter O 2 . Nach Einkristalluntersuchungen kristallisiert Na 3 CuO 3 triklin: a = 18,25 5 ; b = 16,78 5 ; c = 11,12 9 Å; α = 136,2; β = 106,9; γ = 90,6°; Z = 36.

Metal-Organic Frameworks: Synthesis and ApplicationsPolyoxometalates: Synthesis and ApplicationsLayered Double Hydroxides Synthesis and Applications

Studies on Dicumylperoxide Vulcanization of Natural Rubber in Presence of Sulfur and Accelerators

S. P. Manik、Susanta Banerjee1969-07-01Rubber Chemistry and Technology

Abstract The effect of sulfur, MBT, zinc oxide and stearic acid, either singly or in mixtures, on the DCP vulcanization of NR has been studied. In all cases DCP decomposes by a first order law, but the rate constant is higher in presence of MBT. Sulfur and MBT, separately or together reduce the crosslink density, each…

Polymer Nanocomposites and Propertiesbiodegradable polymer synthesis and propertiesSynthesis and properties of polymers

Recrystallization of Thin Gold Films: Influence on Their Electrical Properties

J. P. Chauvineau、Pietro Croce、G. Devant 等 4 位作者1969-07-01Journal of Vacuum Science and Technology

Views Icon Views Article contents Figures & tables Video Audio Supplementary Data Peer Review Share Icon Share Twitter Facebook Reddit LinkedIn Tools Icon Tools Reprints and Permissions Cite Icon Cite Search Site Citation J. P. Chauvineau, P. Croce, G. Devant, M. F. Verhaeghe; Recrystallization of Thin Gold Films: Inf…

Magnetic properties of thin filmsCopper Interconnects and ReliabilityNanoporous metals and alloys

Kinetics of the Transition of Titanium Dioxide Prepared by Sulfate Process and Chloride Process

Akira Suzuki、Ritushi Tukuda1969-07-01Bulletin of the Chemical Society of Japan

Abstract The kinetics of the phase transformation of anatase to rutile was studied by means of X-ray diffraction. Samples of anatase were prepared by sulfate and chloride processes. The kinetic data could well be expressed by the equation α=1−e−btn, where α is the fraction of anatase transformed in time t, and b and n…

TiO2 Photocatalysis and Solar CellsThermal and Kinetic AnalysisChemistry and Chemical Engineering

The electric charging of electron-microscope specimens

Garniss H. Curtis、R.P. Ferrier1969-07-01Journal of Physics D Applied Physics

In electron microscopy, and particularly in small-angle electron diffraction, the electric charging of thin insulating films, which are frequently used to support specimens, has been regarded as a nuisance and techniques have been developed to minimize it. One particular phenomenon, however, has been of scientific int…

Power Transformer Diagnostics and InsulationElectron and X-Ray Spectroscopy TechniquesSurface and Thin Film Phenomena

Conductance, viscosity, density, proton magnetic resonance spectra, and glass transition temperatures of calcium nitrate tetrahydrate-cadmium nitrate tetrahydrate melts. An ideal fused salt system

Cornelius T. Moynihan、C. R. Smalley、C. Austen Angell 等 4 位作者1969-07-01The Journal of Physical Chemistry

ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTConductance, viscosity, density, proton magnetic resonance spectra, and glass transition temperatures of calcium nitrate tetrahydrate-cadmium nitrate tetrahydrate melts. An ideal fused salt systemCornelius T. Moynihan, C. R. Smalley, C. A. Angell, and E. J. SareCite this: J.…

Glass properties and applicationsSolid-state spectroscopy and crystallography

The Variable Corrosion Resistance of 18Cr-8Ni Stainless Steels: Behavior of Commercial Alloys

B. E. Wilde、N. D. Greene1969-07-01CORROSION

The electrochemical and corrosion characteristics of Types 383, 304, and 316 stainless steel in 1N¯ H2SO4 were determined using precision potentiostatic polarization and conventional coupon exposure/weight change techniques. Factors increasing the magnitude of the critical anodic current density, Ic, are shown to have…

Corrosion Behavior and InhibitionHydrogen embrittlement and corrosion behaviors in metalsWelding Techniques and Residual Stresses

Thermal Coefficient of Refractive Index of Optical Glasses*

Tryggve Bååk1969-07-01Journal of the Optical Society of America

The thermal coefficients of refractive index have been determined for 23 commercial glasses. The interferometric procedure consisted of determining both the change of optical path of each glass with a change of temperature at a given wavelength and set coefficient of linear thermal expansion of the glass for the same…

Glass properties and applicationsSurface Roughness and Optical MeasurementsOptical and Acousto-Optic Technologies

Thermal Behavior of Pyrite and Its Relation to Carbon and Sulfur Oxidation in Clays

J. R. Schorr、J. O. Everhart1969-07-01Journal of the American Ceramic Society

The thermal behavior of pyrite in air was studied. A one‐step mechanism for the oxidation of pyrite to hematite exists and accounts for previously reported weight‐loss, DTA, and gas train data which implied a two‐step mechanism. Proper control of the oxidation temperature is very important in completing the pyrite oxi…

Concrete and Cement Materials ResearchClay minerals and soil interactionsMine drainage and remediation techniques

Enzymatic Synthesis of Cytidine Diphosphate 3,6-Dideoxyhexoses

H. Pape、Jack L. Strominger1969-07-01Journal of Biological Chemistry

Abstract Two protein fractions, designated E1 and E3, which are required for the TPNH-dependent reduction of cytidine diphosphate 4-keto-6-deoxy-d-glucose to an intermediate (presumed to be CDP-4-keto-3,6-dideoxy-d-glucose) have been partially purified from extracts of Pasteurella pseudotuberculosis 25 VO and Salmonel…

Fungal and yeast genetics researchEnzyme Structure and FunctionPolyamine Metabolism and Applications

Group theory and magnetic phenomena in solids

A. P. Cracknell1969-07-01Reports on Progress in Physics

In a brief introductory section the derivation of the Shubnikov groups and their importance in the description of the symmetries of magnetic crystals is described. The derivation of the black and white Bravais lattices and of the Shubnikov point groups and space groups is described and there is a brief discussion of s…

Magnetic properties of thin filmsTheoretical and Computational PhysicsMagnetism in coordination complexes

Structure of Pressure-Induced Fibrous Sulfur

Morten Lind、S. Geller1969-07-01The Journal of Chemical Physics

The arrangement of the sulfur helices in the pressure-induced fibrous form of sulfur has been determined from three-dimensional x-ray diffractometer data. The crystals show orthorhombic diffraction symmetry, but analysis of their structure has shown that the most probable space group is P2 and that the orthorhombic sy…

Solid-state spectroscopy and crystallography

The application of stereographic techniques to the scanning electron microscope

Gregory Lane1969-07-01Journal of Physics E Scientific Instruments

A stereographic technique has been developed for the accurate determination of the dimensions of features on scanning electron micrographs. More general methods than those used previously are shown to be necessary largely because of the wide range of operating angles available in the scanning electron microscope. An e…

Advancements in Photolithography TechniquesNuclear Physics and ApplicationsElectron and X-Ray Spectroscopy Techniques

Studies of Epitaxial Growth of Metallic and Nonmetallic Films by Means of High-Resolution Ciné and Still-Electron Microscopy

Goro Honjo、Katsumichi Yagi1969-07-01Journal of Vacuum Science and Technology

Views Icon Views Article contents Figures & tables Video Audio Supplementary Data Peer Review Share Icon Share Twitter Facebook Reddit LinkedIn Tools Icon Tools Reprints and Permissions Cite Icon Cite Search Site Citation Goro Honjo, Katsumichi Yagi; Studies of Epitaxial Growth of Metallic and Nonmetallic Films by Mea…

Advanced Electron Microscopy Techniques and ApplicationsElectron and X-Ray Spectroscopy TechniquesAdvanced Materials Characterization Techniques

CHANGES IN FINE STRUCTURE DURING SILK PROTEIN PRODUCTION IN THE AMPULLATE GLAND OF THE SPIDER ARANEUS SERICATUS

Allen L. Bell、David B. Peakall1969-07-01The Journal of Cell Biology

The ampullate silk gland of the spider, Araneus sericatus, produces the silk fiber for the scaffolding of the web. The fine structure of the various parts of the gland is described. The distal portion of the duct consist of a tube of epithelial cells which appear to secrete a substance which forms the tunica intima of…

Insect and Arachnid Ecology and BehaviorSilk-based biomaterials and applicationsDate Palm Research Studies

Imogolite: a unique aluminosilicate

James Russell、W. J. McHardy、A. R. Fraser1969-07-01Clay Minerals

The fibrous aluminosilicate imogolite has been studied by electronoptical and infrared absorption methods. Electron diffraction patterns are interpreted in terms of repeat units of 8·4 Å parallel and 23 Å perpendicular to the fibre axis. These spacings can not be reconciled with a continuous silicate chain structure a…

Soil and Unsaturated FlowClay minerals and soil interactionsIron oxide chemistry and applications

The photo‐oxidation of polypropylene: Some effects of molecular order

Y. Kato、D. J. Carlsson、D. M. Wiles1969-07-01Journal of Applied Polymer Science

Abstract Fractional crystallization was used to separate a commercial, predominatly isotactice, unstabilized polypropylene into fractions of relatively low and relatively high atacticity, but of similar molecular weight. IR spectroscopy was used to follow the photo‐oxidations of films formed from these fractions durin…

Polymer crystallization and propertiesMicroplastics and Plastic PollutionPolymer Science and PVC

Porosity of MgF2 Films—Evaluation Based on Changes in Refractive Index Due to Adsorption of Vapors

Koreo Kinosita、Mineo Nishibori1969-07-01Journal of Vacuum Science and Technology

The refractive index nf of evaporated MgF2 films changes almost reversibly with the relative vapor pressure p/po of water in the ambient atmosphere. If q is the porosity, or the fractional volume of the pores in the film, and ns and np are the mean indices of the skeleton of the film and the pore space respectively, i…

Advanced Fiber Optic SensorsHigh voltage insulation and dielectric phenomenaOptical Coatings and Gratings

Preservation of electron microscope image contrast after inelastic scattering

S. L. Cundy、A. Howie、U. Valdrè1969-07-01Philosophical magazine

Observations of the effect of thermal diffuse scattering, single electron excitations and plasmon excitation on the quality of electron microscope images of crystals are presented and discussed. Preservation of image contrast after thermal diffuse scattering seems to be poor in practice but only a small fraction of th…

Advanced Electron Microscopy Techniques and ApplicationsElectron and X-Ray Spectroscopy TechniquesX-ray Diffraction in Crystallography

The thermoelectric powers of transition metals at high temperature

Mikhail Vedernikov1969-07-01Advances In Physics

This paper is concerned with a survey of the experimental data for the thermoelectric power† The thermoelectric power is hereinafter referred to as TEP of transition metals and with their discussion. For the first time a critical review of the main data, which are given in the literature and proved to be rather incomp…

Advanced Thermoelectric Materials and DevicesAdvanced Thermodynamics and Statistical MechanicsThermodynamic and Structural Properties of Metals and Alloys