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Analytical Determination of the {Ln-Aminoxyl Radical} Exchange Interaction Taking into Account Both the Ligand-Field Effect and the Spin-Orbit Coupling of the Lanthanide Ion (Ln=DyIII and HoIII)

Myrtil L. Kahn、R. Ballou、P. Porcher 等 5 位作者2002-01-18Chemistry - A European Journal

Numerous compounds in which a paramagnetic LnIII ion is in an exchange interaction with a second spin carrier, such as a transition metal ion or an organic radical, have been described. However, except for GdIII, very little has been reported about the magnitude of the interactions. Indeed, for these ions both the lig…

Magnetism in coordination complexesLanthanide and Transition Metal ComplexesElectron Spin Resonance Studies

Photochemical Functionalization of Diamond Films

Todd Strother、Tanya Knickerbocker、John N. Russell 等 6 位作者2002-01-18Langmuir

We report a new scheme for attachment of functionalized organic molecules to polycrystalline diamond films. In this scheme, ultraviolet light is used to cause a local reaction between a hydrogen-terminated diamond surface and organic molecules present as a thin overlayer liquid film. Comparison of functionalized alken…

Semiconductor materials and devicesElectronic and Structural Properties of OxidesDiamond and Carbon-based Materials Research

Functionalizing Multiple-Walled Carbon Nanotubes with Aminopolymers

Yi Lin、Apparao M. Rao、Bindu Sadanadan 等 5 位作者2002-01-18The Journal of Physical Chemistry B

Multiple-walled carbon nanotubes (MWNTs) produced using the chemical vapor deposition method were functionalized via attaching aminopolymer poly(propionylethylenimine- co -ethylenimine) to the nanotubes. Two different reaction conditions based on acylating the nanotube-bound carboxylic acids and on directly heating na…

Nanotechnology research and applicationsFullerene Chemistry and ApplicationsCarbon Nanotubes in Composites

Electric Polarization of Heteropolar Nanotubes as a Geometric Phase

E. J. Melé、Petr Král2002-01-18Physical Review Letters

The threefold symmetry of planar boron nitride (BN), the III-V analog to graphene, prohibits an electric polarization in its ground state, but this symmetry is broken when the sheet is wrapped to form a BN nanotube. We show that this leads to an electric polarization along the nanotube axis which is controlled by the…

Graphene research and applicationsBoron and Carbon Nanomaterials ResearchFullerene Chemistry and Applications

Enhancement of Red Emission (4F9/2 → 4I15/2) via Upconversion in Bulk and Nanocrystalline Cubic Y2O3:Er3+

John A. Capobianco、Fiorenzo Vetrone、J. Christopher Boyer 等 5 位作者2002-01-18OpenAlex

In this paper, we investigate as a function of erbium concentration (1, 2, 5, 10 mol %) the upconversion properties of bulk and nanocrystalline Er 3+ doped cubic Y 2 O 3 . After excitation at short wavelength (488 nm) or with upconversion pumping (815 nm), green and red emissions were observed for both nanocrystalline…

Luminescence and Fluorescent MaterialsLuminescence Properties of Advanced MaterialsGlass properties and applications

Methods of Loading and Releasing Low Molecular Weight Cationic Molecules in Weak Polyelectrolyte Multilayer Films

A. J. Chung、Michael F. Rubner2002-01-18OpenAlex

This work studied the loading capabilities and release behavior of poly(acrylic acid) (PAA) and poly(allylamine hydrochloride) (PAH) multilayer films, using methylene blue dye (MB) as an indicator. PAA/PAH multilayers assembled at pH = 2.5/2.5 loaded MB throughout the multilayers due to available binding sites and a p…

Polymer Surface Interaction StudiesDendrimers and Hyperbranched PolymersMarine Biology and Environmental Chemistry

Structural Study of Mesoporous MCM-48 and Carbon Networks Synthesized in the Spaces of MCM-48 by Electron Crystallography

Mizue Kaneda、T. Tsubakiyama、Anna Carlsson 等 8 位作者2002-01-18OpenAlex

Recently, we have developed a new electron crystallography (EC) method for study of three dimensional (3D) structures of silica-mesoporous materials, and the 3D-structural solutions of MCM-48 and SBA-1, -6, and -16 were briefly reported. The method gives a unique structure solution through the Fourier sum of the 3D-st…

Polyoxometalates: Synthesis and ApplicationsMesoporous Materials and CatalysisZeolite Catalysis and Synthesis

Recent Advances in Synthesis and Applications of Transition Metal Containing Mesoporous Molecular Sieves

Xun He、David M. Antonelli2002-01-18OpenAlex

Work in mesoporous silica-based materials began in the early 1990s with work by Mobil. These materials had pore sizes from 20-500 A and surface areas of up to 1500 m(2) g(-1) and were synthesized by a novel liquid crystal templating approach. Researchers subsequently extended this strategy to the synthesis of mesoporo…

Catalytic Processes in Materials ScienceCatalysis and Oxidation ReactionsMesoporous Materials and Catalysis

Tuning the Electrical Conductivity and Self-Assembly of Regioregular Polythiophene by Block Copolymerization: Nanowire Morphologies in New Di- and Triblock Copolymers We gratefully acknowledge support from the NSF (CHE-9807707).

Jinsong Liu、Elena E. Sheina、Tomasz Kowalewski 等 4 位作者2002-01-18OpenAlex

Simply changing the solvent or evaporation conditions enables the physical properties of polythiophene block copolymers and polyurethane elastomers to be controlled. The copolymers all have high conductivities as well as excellent film-forming and good mechanical properties, and well-defined nanowires that reach lengt…

Organic Electronics and PhotovoltaicsConducting polymers and applicationsPolymer composites and self-healing

Synthesis and characterization of stable aqueous dispersions of silver nanoparticles through the Tollens processElectronic supplementary information (ESI) available: photographs of silver mirror, and of stable dispersions of silver nanoparticles from mixing diluted silvering solutions under sonication at various times. See http://www.rsc.org/suppdata/jm/b1/b107469e/

Yadong Yin、Zhiyuan Li、Ziyi Zhong 等 6 位作者2002-01-18OpenAlex

This paper describes a simple and convenient procedure based on the Tollens process for the preparation of silver nanoparticles with a relatively narrow distribution in size. The starting reagents were similar to those commonly used in the electroless deposition of silver. Only under appropriate conditions, mixing of…

Nanoparticles: synthesis and applicationsGold and Silver Nanoparticles Synthesis and ApplicationsElectrochemical Analysis and Applications

Negative Role of Surface Plasmons in the Transmission of Metallic Gratings with Very Narrow Slits

Qing Cao、Philippe Lalanne2002-01-18OpenAlex

It is generally admitted that the extraordinary transmission of metallic grating with very narrow slits is mainly due to the excitation of surface plasmons on the upper and lower interfaces of the grating. We show that the surface plasmon contribution is not the prime effect and that waveguide mode resonance and diffr…

Plasmonic and Surface Plasmon ResearchOptical Coatings and GratingsPhotonic Crystals and Applications

Solid Wettability from Surface Energy Components: Relevance to Pickering Emulsions

Bernard P. Binks、John H. Clint2002-01-18OpenAlex

A theoretical treatment is developed for the wetting of a solid particle at an oil−water interface in terms of the components of the surface energies of all three phases. Calculated oil−water contact angles for a solid of given hydrophobicity with a range of oils of different polarity show good agreement with experime…

Pickering emulsions and particle stabilizationProteins in Food SystemsSurfactants and Colloidal Systems

Spider Silk Fibers Spun from Soluble Recombinant Silk Produced in Mammalian Cells

Anthoula Lazaris、Steven Arcidiacono、Yue Huang 等 9 位作者2002-01-18OpenAlex

Spider silks are protein-based "biopolymer" filaments or threads secreted by specialized epithelial cells as concentrated soluble precursors of highly repetitive primary sequences. Spider dragline silk is a flexible, lightweight fiber of extraordinary strength and toughness comparable to that of synthetic high-perform…

Silkworms and Sericulture ResearchInvertebrate Immune Response MechanismsSilk-based biomaterials and applications

A second-generation reactive empirical bond order (REBO) potential energy expression for hydrocarbons

Donald W. Brenner、Olga Shenderova、Judith A. Harrison 等 6 位作者2002-01-18OpenAlex

A second-generation potential energy function for solid carbon and hydrocarbon molecules that is based on an empirical bond order formalism is presented. This potential allows for covalent bond breaking and forming with associated changes in atomic hybridization within a classical potential, producing a powerful metho…

High-pressure geophysics and materialsForce Microscopy Techniques and ApplicationsDiamond and Carbon-based Materials Research

From bifluorenylidene dianion to dibenzo[g,p]chrysene dianion: sensitivity of anisotropy changes to bonding structure

Roy Shenhar、Ronald Beust、Stefan Hagen 等 7 位作者2002-01-17Journal of the Chemical Society Perkin Transactions 2

Five polycyclic aromatic hydrocarbons of the C26 series having similar bonding structure yield dianions upon reduction with lithium metal. Anisotropy changes, revealed from an advanced charge distribution analysis performed on these dianions, show a correlation to the bonding structure of the dianions. Electron counti…

Porphyrin and Phthalocyanine ChemistrySynthesis and Properties of Aromatic CompoundsPhotochemistry and Electron Transfer Studies

Structural Analysis of Copolymers of Syndiotactic Polypropylene with 13C-Enriched Ethylene

Claudio De Rosa、Finizia Auriemma、Giovanni Talarico 等 6 位作者2002-01-17Macromolecules

A structural analysis of copolymers of syndiotactic polypropylene with small amounts of 13 C-enriched ethylene, in the range 0.4−2.6 mol %, is reported. X-ray diffraction and solid-state 13 C NMR CPMAS data indicate that the as-prepared copolymer samples are crystallized in the conformationally disordered modification…

Organometallic Complex Synthesis and CatalysisFiber-reinforced polymer compositesPolymer crystallization and properties

The annular tautomerism of 4(5)-phenylimidazole

Rosa M. Claramunt、Dolores Santa María、Lourdes Infantes 等 5 位作者2002-01-17Journal of the Chemical Society Perkin Transactions 2

A new polymorph of 4-phenylimidazole 1a has been characterised by X-ray crystallography. Both polymorphs present a secondary structure of chains, and the observed differences in the topology of their crystal packing are related to the conformational differences in the primary and secondary structural levels. NMR exper…

Synthesis and Characterization of Heterocyclic CompoundsSynthesis and Reactivity of HeterocyclesPorphyrin and Phthalocyanine Chemistry

Electroabsorption Spectroscopic Studies of Dipolar Ruthenium(II) Complexes Possessing Large Quadratic Nonlinear Optical Responses

Benjamin J. Coe、J. Arthur Harris、Bruce S. Brunschwig2002-01-17The Journal of Physical Chemistry A

A series of 20 ruthenium(II) complex salts, known to exhibit large molecular static first hyperpolarizabilities β 0 [HRS] from hyper-Rayleigh scattering measurements on acetonitrile solutions at 298 K (Coe, B. J.; et al. Inorg. Chem . 1997, 36, 3284; 1998, 37, 3391; J. Chem. Soc., Dalton Trans . 1999, 3617), have been…

Nonlinear Optical Materials ResearchSolid-state spectroscopy and crystallographyPhotochemistry and Electron Transfer Studies

Photoinitiated Polymerization of Styrene from Self-Assembled Monolayers on Gold

Rolf Schmidt、Tongfeng Zhao、John-Bruce Green 等 4 位作者2002-01-17Langmuir

We report the synthesis of grafted polystyrene (PS) films on gold via a surface-initiated polymerization strategy. The polymerization proceeded by a “grafted-from” strategy in which the polystyrene grew by free-radical polymerization from a surface-bound photoinitiator. These experiments exploited the spontaneous form…

Molecular Junctions and NanostructuresMarine Biology and Environmental ChemistryPolymer Surface Interaction Studies

Mechanism of Formation of a Productive Molten Globule Form of Barstar

Bhadresh R. Rami、Jayant B. Udgaonkar2002-01-17Biochemistry

Structural analysis of the initial steps in protein folding is difficult because of the swiftness with which these steps occur. Hence, the link between initial polypeptide chain collapse and formation of secondary and other specific structures remains poorly understood. Here, an equilibrium model has been developed fo…

Enzyme Structure and FunctionProtein Structure and DynamicsProtein purification and stability