Materials Literature
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Hydrous titanium dioxide (TiO 2 · n H 2 O) was used to prepare K 2 Ti 2 O 5 single crystals, K 2 Ti 4 O 9 whiskers and K 2 Ti 6 O 13 whiskers at 820°, 940°, and 1110°C, respectively, by calcination. At T < 820°C, dehydration of hydrous titania, decomposition of potassium carbonate, and reaction between titanate and…
Abstract A series of new polybenzimidazopyrrolones (polypyrrolone, PPy) were synthesized by polycondensation of pyridine‐bridged aromatic tetraamines, including 2,6‐bis (3′,4′‐diaminophenyl)‐4‐phenylpyridine and 2,6‐bis(3′,4′‐ diaminophenyl)‐4‐(3″‐trifluoromethyl)phenyl pyridine, with various aromatic dianhydrides. Ex…
Abstract We discuss the use of multivariate design to ensure representativity and balance of the training set data for PLS multivariate modeling. Three application areas are used to illustrate the discussion, namely multivariate calibration in process analytical chemistry, quantitative structure activity relationships…
Tissue engineering may allow for the reconstruction of breast, facial, skin, and other soft tissue defects in the human body. Cell-seeded collagen gels are a logical choice for creating soft tissues because they are biodegradable, mimic the natural tissue, and provide a three-dimensional environment for the cells. The…
Classical molecular dynamics simulations are used to study the structure of densified germanium dioxide (GeO 2 ). It is found that the coordination number of germanium changes with increasing density (pressure) while pressure released systems exhibit only a marked angular change in local structure as compared to the v…
The mechanism of Al ohmic contacts to n-type zinc oxide (ZnO:Al) epitaxial layer was investigated. The formation of an Al-ZnO interfacial phase at room temperature was responsible for the low specific resistivity (8±0.3×10 -4 Ωcm 2 ). The results of Auger electron spectroscopy (AES), X-ray photoelectron spectroscopy (…
Demolition techniques for concrete and masonry structures. Case studies of demolition of structures, including prestressed concrete structures, nuclear power related structure, off-shore structures, chemical plants etc. Reuse, treatment and disposal of demolished concrete, stone and brick. The economics of demolition…
Abstract AgNO3 was reduced by ethylene glycol (EG) in the presence of Pt seeds and polyvinylpyrrolidone (PVP) under microwave heating. In addition to spherical nanoparticles, single-crystalline silver nano-films, rods, and wires were produced. The relative number ratio of nanorods and nanowire to the total silver nano…
Abstract Summary: A comparative study of polyelectrolyte microcapsules templated on melamine formaldehyde (MF) and manganese carbonate (MnCO 3 ) particles was performed using confocal Raman microscopy, scanning electron microscopy and by force measurements with an atomic force microscope. There is no significant diffe…
We have investigated partial discharge (PD) degradation for conventional polyamide-6. without nanoscale fillers (nanofillers) and polyamide-6 nanocomposites with 2 weight (wt) %, 4 wt% and 5 wt% addition. Such materials were subjected to partial discharge under the IEC (b) electrode configuration for evaluation. Compa…
We describe a history-dependent (non-Preisach) hysteresis model based on direct use of experimental first-order reversal curves. We propose that any second or higher order reversal curve can be constructed by using internal segments of the first-order reversal curves, and show that particular transplants (segments wit…
Anisotropic optical coatings offer unique polarizing properties, unmatched by conventional isotropic devices. Here we demonstrate the fabrication of a birefringent omnidirectional reflector, a type of photonic crystal, which exhibits complete reflection of radiation at 1.1 microm for all incidence angles and polarizat…
Abstract Structure and ionic conductivity of Mg-doped La10Si6O27 was investigated on dense ceramic samples prepared from sol–gel derived powders using two step sintering process. The conductivity was increased by the doping (from 22 to 30–39 mS cm−1 at 800 °C) because of expansion of the apatite lattice.
This review focuses on the association between mild renal insufficiency (stage 2 and 3 of chronic kidney disease) and cardiovascular disease and discusses therapeutic options. Although the association of chronic renal insufficiency and cardiovascular risk was first shown in patients with end-stage renal disease, even…
This paper explores the physical meaning of pseudosources of an adjoint system in a continuum design sensitivity analysis (CDSA) when applied to shape optimization in magnetostatics. An efficient and practical way to compute the required gradient information with standard electromagnetic (EM) software packages is sugg…
The Escherichia coli Tat system has unusual capacity of translocating folded proteins across the cytoplasmic membrane. The TatA protein is the most abundant known Tat component and consists of a transmembrane segment followed by an amphipathic helix and a hydrophilic C terminus. To study the operation mechanism of the…
In order to bound failure of austenitic stainless steel storage containers housing Ga-containing compounds, the liquid-metal embrittlement of Type 316L (UNS S31603) stainless steel (SS) by Ga was investigated. Type 316L SS compact tension specimens were exposed to liquid Ga using a depassivation technique to wet the s…
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Abstract The kinetics of esterification of bisphenol‐A based epoxy resin with acrylic acid in presence of triphenylphosphine has been studied. The reaction exhibits a first‐order rate dependence with respect to [Epoxy] and [Catalyst]. A first‐order dependence of rate with respect to [Acid] has been observed during a p…
Abstract A quantitative fabric drape evaluation system that uses image processing technology and simple instruments has been developed. The purpose of this research is to obtain detailed quantitative information on fabric drapability from digital images captured with a commercial digital camera (or a scanner). A two-d…