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Das erste Oxogermanat mit „Stuffed Pyrgoms”: CsNa3Li8{Li[GeO4]}4

Ricardo Brandès、R. Hoppe1995-05-01Zeitschrift für anorganische und allgemeine Chemie

Abstract Durch Tempern der binären Oxide CsO 0,52 , NaO 0,45 , LiO 0,5 und GeO 2 im mol. Verhältnis 1,24:1,4:6,7:3,9 (Ni‐Bömbchen; 600°C/89 bzw. 65 d) wurden erstmals Einkristalle von CsNa 3 Li 8 {Li[GeO 4 ]} 4 in Form von schwachgelblichen Prismen sowie blaßgelbem Pulver erhalten: Raumgruppe I 4/ m (I. T. Nr. 87) mit…

Crystal Structures and PropertiesPolyoxometalates: Synthesis and ApplicationsInorganic Chemistry and Materials

Numerical method for the performance of a separate-type transformer connected to battery charger

K. Hirata、Yoshio Mitsutake、Yoshiyuki Ishihara 等 4 位作者1995-05-01IEEE Transactions on Magnetics

The purpose of this paper is to present an easy method for analyzing the operating characteristics of a separate-type transformer connected to an external circuit including elements such as batteries, resistances, and diodes. This method, a combination of two- and three-dimensional finite element methods, has been app…

Advanced DC-DC ConvertersMagnetic Properties and ApplicationsInduction Heating and Inverter Technology

Modeling Fission Product Vapor Transport in the Falcon Facility

I. Shepherd、Yannis Drossinos、Christopher G. Benson1995-05-01Nuclear Technology

An extensive database of aerosol experiments exists and has been used for checking aerosol transport codes. Data for fission product vapor transport are harder to find. Some qualitative data are available, but the Falcon thermal gradient tube tests carried out at AEA Technology’s laboratories in Winfrith, England, mar…

Nuclear reactor physics and engineeringNuclear Materials and PropertiesCyclone Separators and Fluid Dynamics

Sulfidation of Zinc by Traces of Hydrogen Sulfide in Air

Jan Svensson、L.‐G. Johansson1995-05-01Journal of The Electrochemical Society

The effect of in the sub‐parts per million range on the atmospheric corrosion of zinc has been investigated in the laboratory. Each sample was exposed individually to air with careful control of pollutant concentration, relative humidity, and flow conditions. Monitoring of concentration at the outlet of the corrosion…

Corrosion Behavior and Inhibition

Diamond deposition on carbon fibers

S. İsmat Shah、M. M. Waite1995-05-01Journal of Vacuum Science & Technology A Vacuum Surfaces and Films

Diamond films have been deposited on carbon fibers with diameters as small as 5 μm by microwave plasma assisted chemical vapor deposition. An ultrasonic pretreatment of the fibers in a bath containing methanol and diamond paste was required for successful coating of the fibers. In the absence of such treatment, the fi…

Metal and Thin Film MechanicsDiamond and Carbon-based Materials ResearchLubricants and Their Additives

Electromagnetic field analysis of film transformer

Yoichi Midorikawa、Iliana Marinova、S. Hayano 等 4 位作者1995-05-01IEEE Transactions on Magnetics

In this paper, we investigate a thin film transformer for small electronic devices. This transformer is composed of the lamination of thin film conductors. Both the primary and secondary coils of the film transformer are arranged coaxially on one layer and multiply laminated. The operation principle of the transformer…

Magnetic Properties and ApplicationsThermal Analysis in Power TransmissionInduction Heating and Inverter Technology

X-ray photoelectron and infrared spectroscopies of Cu-implanted silica and borosilicate glasses

D. O. Henderson、M. A. George、Y. S. Tung 等 10 位作者1995-05-01Journal of Vacuum Science & Technology A Vacuum Surfaces and Films

Fourier transform infrared (FTIR) spectra and x-ray photoelectron spectra (XPS) were acquired from Cu implanted in fused silica and a borosilicate glass. The FTIR spectra indicate that Cu ion implantation in the silica and borosilicate glasses results in an intensity decrease in the Si–O stretching vibration. The Si–O…

Advanced ceramic materials synthesisGlass properties and applicationsPigment Synthesis and Properties

Texture analysis of chemical vapor deposited diamond films on silicon by the component method

K. Helming、Sebastian Geier、M. Schreck 等 6 位作者1995-05-01Journal of Applied Physics

Oriented diamond films have been grown on Si(001) and Si(111) substrates by microwave plasma chemical vapor deposition. X-ray diffractometry has been employed for pole figure measurements which have been evaluated by the component method. This technique can be applied to multiphase materials with overlapping pole figu…

Metal and Thin Film MechanicsSemiconductor materials and devicesDiamond and Carbon-based Materials Research

Objective evaluation of a stabilized garment parts handle

Jelka Geršak、Andreja Saric1995-05-01International Journal of Clothing Science and Technology

Presents the objective evaluation of a stabilized garment parts handle, based on determination of mechanical and physical properties of fabrics using the Kawabata Evaluation System. Parameters that influence the handle are shown on the basis of 16 parameters of mechanical and physical properties of shell fabric, inter…

Additive Manufacturing and 3D Printing TechnologiesTextile materials and evaluationsErgonomics and Musculoskeletal Disorders

Interfacial analyses of copper corrosion by acrylic and methacrylic acids using XPS, auger and grazing angle FTIR spectroscopy

D. Billy Yang、David Wolf1995-05-01Surface and Interface Analysis

Abstract We have observed that methacrylic acid (MA) is far more corrosive than acrylic acid (AA) on copper surfaces when copper was exposed to the vapor of these two acids at ambient temperature and environment. With the aid of modern surface‐sensitive instrumentation, which included grazing angle Fourier transform i…

Corrosion Behavior and InhibitionElectron and X-Ray Spectroscopy TechniquesNon-Destructive Testing Techniques

Mechanisms of radiation damages formation in gadolinium gallium garnet (GGG) single crystals

A. Matkovskii、D. Y. Sugar、S. Ubizskii 等 4 位作者1995-05-01Radiation effects and defects in solids

The influence of γ-, electrons and reactor neutrons irradiation on the optical and electrophysical properties of Gd3 Ga5 O12 single crystals is investigated. Experimental data and theoretical estimations of radiation defect concentration are compared.

Luminescence Properties of Advanced MaterialsPhotorefractive and Nonlinear OpticsNuclear materials and radiation effects

Influence of surface treatments of hot‐dip galvanized steels on their acid–base properties and on their reactions with some organic compounds

F. Gaillard、E. Peillex、M. Romand 等 5 位作者1995-05-01Surface and Interface Analysis

Abstract The surface of hot‐dip galvanized steels is a complex system highly dependent upon the composition of the galvanization bath and upon surface treatments such as degreasing, alkaline etching and chromate conversion. In this study, industrial zinc‐coated samples are subjected to degreasing, alkaline etching and…

Corrosion Behavior and InhibitionHigh voltage insulation and dielectric phenomenaMaterial Properties and Processing

Nature of the first diffraction peak in glassy selenium

F. J. Bermejo、M. Garcı́a-Hernández、F. J. Mompeán 等 5 位作者1995-05-01Physical review. B, Condensed matter

The physical significance of the first diffraction peak in glassy Se is discussed in the light of recent experimental results regarding the temperature dependence of the parameters characterizing the first peaks in the elastic S(Q,\ensuremath{\omega}=0) and static S(Q) structure factors. The rather different behavior…

Glass properties and applicationsPhase-change materials and chalcogenidesSolid-state spectroscopy and crystallography

Living Cationic Polymerization of β-(Vinyloxy)ethyl Cinnamate

Nan‐Xing Hu、Guojun Liu1995-05-01Journal of Macromolecular Science Part A

Trifluoroacetic acid and ZnCl2 have been used as the initiating system for the living cationic polymerization of β-(vinyloxy)ethyl cinnamate (VEC). In contrast to a previous initiating system [EtAlCl2 and 1-(isobutoxy)ethyl acetate], the use of the new system led to excellent agreement between the molar masses of PVEC…

Advanced Polymer Synthesis and Characterizationbiodegradable polymer synthesis and propertiesPhotopolymerization techniques and applications

Antiferroelectric liquid crystals derived from a new optically active (R)-3-ethylmercapto-2-methylpropionic acid

S.‐L. Wu、Feng Huang、B.‐J. UANG 等 5 位作者1995-05-01Liquid Crystals

A new optically active (R)-3-ethylmercapto-2-methylpropionic acid has been synthesized using D(-)—2,10-camphorsultam as a chiral auxiliary. The optical purity of the acid obtained was greater than 98 per cent. Its derivatives, (R)-4-(3-ethylmercapto-2-methylpropionyl)phenyl 4′-alkoxybiphenyl-4-carboxylates (EMMPPmBC;…

Liquid Crystal Research AdvancementsSurfactants and Colloidal SystemsMolecular spectroscopy and chirality

Pore size control of porous silica by sol-gel process

Sasa Wang、Hongling Liu、Liangying Zhang 等 4 位作者1995-05-01Ferroelectrics Letters Section

Porous silica glass was prepared by sol-gel process from tetraethoxysilane (TEOS). The effects of solvents (water, ethanol), drying condition, heat treatment temperature on specific surface area and pore size distribution of porous silica were investigated. Gelation process accelerates with an increase of H2O content,…

Photonic Crystals and ApplicationsMesoporous Materials and CatalysisAerogels and thermal insulation

Thermodynamics and Hysteresis for Hydrogen Solution and Hydride Formation in Pd-Ni Alloys

Ted B. Flanagan、H. Noh1995-05-01Zeitschrift für Naturforschung A

Pd and its fee substitutional alloys which form hydride phases exhibit hysteresis. If Pd-Ni alloys have been hydrided and then dehydrided a number of times at a moderate temperature, the hysteresis is reduced. The reduction of hysteresis increases with increase of X Ni to 0.15 and, if the X Ni = 0.15 alloy is hydrided…

Fusion materials and technologiesHydrogen Storage and MaterialsThermodynamic and Structural Properties of Metals and Alloys

Elastic Recoil Detection Analysis for Hydrogen near the Surface of Chemical-Vapor-Deposited Diamond

Hiromasa Yagi、Kazuo TANIDA、Kazuhito Nishimura 等 6 位作者1995-05-01Japanese Journal of Applied Physics

Elastic recoil detection analysis (ERDA) was performed to determine hydrogen concentration profiles near the (100) surfaces of epitaxially grown diamond films. Microwave plasma chemical vapor deposition (CVD) was used for the growth. At the end of the growth, the substrates were treated with and without exposure to H…

Diamond and Carbon-based Materials ResearchSpectroscopy and Laser ApplicationsIon-surface interactions and analysis

Effects of electron irradiation of rutile

Edgar C. Buck1995-05-01Radiation effects and defects in solids

The dislocation loops in rutile produced after irradiation by 0.4-1 MeV electrons at various temperatures have been analyzed. Loops formed during electron irradiation at 400°-500°C were pure edge interstitial of the type <100>{100} and were unfaulted. After leaving rutile specimens irradiated at high temperature for a…

Ion-surface interactions and analysisNuclear materials and radiation effectsElectronic and Structural Properties of Oxides

Visible luminescence from single crystal-silicon quantum wells

Peter N. Saeta、Alan Gallagher1995-05-01Journal of Applied Physics

Single crystal-silicon quantum wells with SiO2 barriers have been grown from SIMOX silicon-on-insulator substrates. Photoluminescence in the red and near-infrared is observed for average well width &amp;lt;8 nm, with peak signal for 2-nm average width. The luminescence spectrum is independent of well width for SiO2 ba…

Semiconductor materials and devicesSilicon Nanostructures and PhotoluminescenceNanowire Synthesis and Applications