Materials Literature
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Doping with donor and acceptor impurities is an effective way to control light emission originated from quantum-size effect in Si nanocrystals. Combined measurements of photoluminescence intensity and kinetics give valuable information on mechanisms of the doping influence. Phosphorus, boron, and nitrogen were introdu…
Abstract A study is presented on the morphological effects caused by the nanoclay organic modifier and the nanoclay concentration. This was made under previously determined compatibility conditions of heterophasic polypropylene copolymers (PP‐EP)/poly(ethylene vinyl acetate) (EVA)/organoclay nanocomposites. The nanoco…
We study thermoelectric power under strong magnetic field (TPM) in carbon nanotubes (CNTs) and quantum wires (QWs) of nonlinear optical, optoelectronic, and related materials. The corresponding results for QWs of III-V, ternary, and quaternary compounds form a special case of our generalized analysis. The TPM has also…
Bilayered ferroelectric thin films consisting of Pb(Zr0.52Ti0.48)O3 (PZT) and (Bi3.15Nd0.85)Ti3O12 (BNT) layers have been successfully fabricated via a synthesis route of combining sol-gel and rf sputtering. Both ferroelectric layers are well retained in both PZT/BNT and BNT/PZT bilayered films as suggested by x-ray d…
To obtain high transmittance and low resistivity ZnO transparent conductive thin films, a series of ZnO ceramic targets (ZnO:Al, ZnO:(Al, Dy), ZnO:(Al, Gd), ZnO:(Al, Zr), ZnO:(Al, Nb), and ZnO:(Al, W)) were fabricated and used to deposit thin films onto glass substrates by radio frequency (RF) magnetron sputtering. X-…
Abstract This work presents a novel study on electrochemical codeposition of Mg–Li alloys on molybdenum in KCl–LiCl (50:50 wt %) melts containing different concentrations MgCl2 at 943 K. Cyclic voltammograms showed that the underpotential deposition (UPD) of lithium on pre-deposited magnesium leads to the formation of…
In the Cu-Fe-sulphide mining district of Servette-Chuc (Saint-Marcel, Aosta Valley, Italy), a streambed called Eve Verda and covered with a colloidal blue-green precipitate has been known since the 18th century. X-ray and chemical analyses reveal that the precipitate is a mixture of a nanocrystalline Cu-Al-sulphate hy…
Surface-enhanced Raman spectroscopy is used to investigate the kinetics of adsorption of the cationic surfactant cetylpyridinium chloride (CPC) to hydrophobic surfaces from water. A hydrophobic surface, with stable and reproducible SERS activity, is produced by binding gold colloids to an amine-terminated glass slide…
Mixed oxide photocatalysts, ZnO-Zn2SnO4 (ZnO-ZTO) nanowires with different sizes were prepared by a simple thermal evaporation method. The ZnO-ZTO nanowires were characterized with a scanning electron microscope, X-ray diffraction, high-resolution transmission electron microscopy, energy-dispersive spectrometer, and X…
Molybdenum (Mo) adsorption was investigated on five soils from the Gauro and Roccamonfina volcanoes of Campania, a southern Italian volcanic region. The soils were characterized by different degrees of development. Molybdenum adsorption exhibited a maximum near pH 4–5 and decreased with increasing pH above 5. The cons…
PURPOSE: To design nanoparticles containing accessible gadolinium atoms (Gd-NPs) as a contrast agent for magnetic resonance imaging of tumors. METHODS: Nanoparticles containing phospholipid-chelates (phosphoethanolamine diethylenetriaminepentaacetate) and DSPE-PEG (MW5000) were prepared from Brij 78 and stearyl alcoho…
Ceramic coatings containing ZrO2 were prepared in situ on LY12 aluminum alloy by microarc oxidation (MAO) in the mixed solution of zirconate and phosphate solution. The phase composition and morphology of the coatings were studied by XRD and SEM, respectively. The growing mechanism of ceramic coatings was discussed in…
The pathway for synthesis of the peptidoglycan precursor UDP-N-acetylmuramyl pentapeptide is essential in Gram-positive and Gram-negative bacteria. This pathway has been exploited in the recent past to identify potential new antibiotics as inhibitors of one or more of the Mur enzymes. In the present study, a high-thro…
Nephrogenic systemic fibrosis (NSF) is a newly recognized systemic disorder characterized by widespread tissue fibrosis in patients with impaired renal function. Recent reports suggest that NSF is associated with exposure to gadolinium-based contrast agents used in magnetic resonance imaging. NSF can be very debilitat…
A newly developed hyphenated technique is presented combining an existing rheometer and differential scanning calorimeter into a single experimental setup. Through the development of a fixation accessory for differential scanning calorimeter (DSC) crucibles and a novel rotor, the simultaneous measurement is performed…
One of the most challenging activities for magnesium industry is to increase productivity by introducing cost-effective processes. While die-cast magnesium alloys are in worldwide use, even in the demanding sector of automotive industry, where cost is the major asset, wrought magnesium alloys still not widely availabl…
Epoxy resins were cured by an amine telechelic poly(tetramethylene oxide) (PTMO). The telechelic amine was synthesized from hydroxy telechelic PTMO and was characterized. The kinetics of curing of epoxy monomer by the polyether amine was studied in detail by differential scanning calorimetry (DSC) and rheology to opti…
Quartz crystals collected in druses, including one annealed at 400°C, from a fracture in the hanging-wall sandstone at the McArthur River uranium deposit in the Paleoproterozoic Athabasca basin, northern Saskatchewan, have been investigated by single-crystal X-band electron paramagnetic resonance (EPR) spectroscopy at…
Mesoporous silicas with controllable pore size are providing important platforms finding a multitude of applications such as in catalysis, separations, and as nanoreactors for molecular transformations. In this study, we probe the influence of a coattached hydrogen donor molecule, fluorene, on the free-radical pyrolys…
Abstract Summary: Their biodegradable properties make polyhydroxyalkanoates (PHAs) ideal candidates for innovative applications. Many studies have been primarily oriented to poly(3‐hydroxybutyrate) (PHB) and poly(3‐hydroxybutyrate‐co‐3‐valerate) (PHBV) and afterwards to blends of PHAs with synthetic biodegradable poly…