Materials Literature
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High frequency cyclic voltages on a specimen surface have been studied pictorially, in the scanning electron microscope, by applying the principle of the sampling oscilloscope. The electron beam in the microscope column is pulsed, and the phase varied with respect to that of the waveform on the specimen. With 10 ns el…
It is shown how the method of measuring fabric drape by supporting a circular specimen of fabric between smaller horizontal circular plates has been modified to allow a more sensitive test to be made on very stiff and very limp fabrics. The use of diverging light instead of parallel light is described, and the correct…
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTPreexponential factors for solid-state thermal decompositionHerman F. CordesCite this: J. Phys. Chem. 1968, 72, 6, 2185–2189Publication Date (Print):June 1, 1968Publication History Published online1 May 2002Published inissue 1 June 1968https://doi.org/10.1021/j100852a052RIGH…
The optical absorption and fluorescence spectra of two spinels, ZnAl2O4:Cr3+ and MgAl2O4:Cr3+ have been measured at various temperatures between 2°K and room temperature. The data have been fitted to a crystal-field theory which includes spin-orbit coupling and the trigonal field of the D3d site. The parameters for a…
The thermal behavior of amorphous hydrated zirconium oxide and its coprecipitates with other oxides was studied. Solid solution with a limit of solubility seems to exist in the amorphous coprecipitates. A relation with the high‐temperature solid solution was established. The structure of the amorphous zirconia was stu…
Abstract Vermiculites and smectites in soils and sediments are frequently partially interlayered or “chloritized”. Dioctahedral expansible layer silicates are those most frequently interlayered, and hydroxy-Al appears to be the principal component of the non-exchangeable interlayer material. The most favorable soil co…
An electrostatic lens system which compensates for chromatic aberration has been tested in an electron spectrometer. The results indicate that this lens is suitable for comparisons of peak intensities in electron-impact spectra. Relative intensities in vibrational progressions that belong to a single electronic transi…
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In a limited temperature range above the clearing point of crystal suspensions, submicroscopic entities representing unmeasurably small portions of the original crystal population may survive whose existence is revealed by crystals nucleated on subsequent cooling [1]. Factors influencing the number of these nuclei and…
For an arbitrary electron configuration l1n1l2n2l3n3⋯, analytical expressions are derived for the energy-matrix coefficients of the electrostatic-interaction parameters Fk(li,lj) and Gk(li,lj) and of the spin–orbit parameters ζ(li). A computer program is described which calculates decimal values of these coefficients…
Ferroelectric Ba0.27Sr0.75Nb2O5.78, with Tc = 348° ± 15°K, is a tungsten bronze-type structure crystallizing in the tetragonal system, with lattice constants a = 12.43024 ± 0.00002 and c = 3.91341 ± 0.00001 Å at 298°K, space group P4bm, and five formulas in the unit cell. The integrated intensities of 6781 structure f…
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTRegulation of glutamine synthetase. XII. Electron microscopy of the enzyme from Escherichia coliR. C. Valentine, B. M. Shapiro, and E. R. StadtmanCite this: Biochemistry 1968, 7, 6, 2143–2152Publication Date (Print):June 1, 1968Publication History Published online1 May 2002P…