Materials Literature
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Sulphoaluminate-alite cement (SAAC) was successfully prepared from high alumina fly ash. XRD analysis indicated that the optimal mineralogical phase of cement clinker was obtained under condition of MG=1.05, MS =0.95 at 1300oC, and C4A3 S reached the strongest intensity and is 58.73% in the phase of calcined clinckers…
Abstract Using an oxidative coupling polymerization of the macromonomers of oligoaniline and p ‐phenylenediamine, we have prepared an electroactive hyperbranched polyamide, exhibiting an exciting molecular structure, and interesting spectroscopic and electrochemical properties. The molecular structure of the electroac…
Tungsten oxides are of interest as an oxidant for metals in metastable intermolecular composites (MICs), a reactive nanoscale powder useful for such applications as electric matches and gun primers. Smaller particles typically lead to fast reaction rates in this class of energetic material, and we have synthesized nan…
Ultra-low carbon steel (ferritic steel), commercial purity aluminum and high purity copper were heavily deformed by the accumulative roll bonding (ARB) process, and the microstructural evolution during the ARB was analyzed. Significant grain refinement by grain subdivision mechanism was confirmed in all three kinds of…
Barium strontium titanate (Ba0.5Sr0.5TiO3 or BST) films were grown on SiO2∕Si substrate by means of a reactive pulsed laser deposition technique. The microstructural and surface morphology of BST films were characterized by x-ray diffraction, scanning electron microscopy, and atomic force microscopy. Films deposited a…
Abstract Soluble poly(imide‐siloxane)s were obtained by carefully designing the synthesis and introducing poly(ethylene glycol) (PEG) units, thereby making the system amphiphilic in nature. The solubility of the synthesized PEG containing poly(mide‐siloxane)s (PPIS) in various solvents was tested and their thermal pro…
Effects of pretreatment on the nuclei formation of ultrananocrystalline diamond (UNCD) on Si substrates were studied. Either precoating a thin layer of titanium (∼400nm) or ultrasonication pretreatment using diamond and titanium mixed powder (D&T process) enhances the nucleation process on Si substrates markedly,…
Polycrystalline Ba1−xSrxTiO3 (BST) thin films with three different compositions have been deposited by radio-frequency magnetron sputtering technique on platinum coated silicon substrates. Samples with buffer and barrier layers for different film thicknesses and processing temperatures have been studied. Crystallite s…
We report experiments on a ferroelectric membrane and droplets with tunable surface properties. In smectic membranes the configuration of the c -director field near inclusions may be rearranged drastically with temperature. The transformation of the c -director field results from the competition between the elastic an…
Poly(3-hydroxybutyrate-co-3-hydroxyvalerate) (PHBV) was used to fabricate micro- and nano-fibrous, non-woven mats by electrospinning for potential tissue engineering applications. The morphology and size of electrospun fibers were assessed systematically by varying the processing parameters. It was found that the diam…
We propose a phenomenological intrinsic finite-size effect model for single domain, mechanically free, and surface charge compensated PbTiO3 (PT) nanocrystals with no depolarization fields, undergoing a first-order tetragonal→cubic ferrodistortive phase transition. We then derive a Landau-Devonshire type free-energy f…
Sn 1 − x Mn x O 2 nanocrystalline powders were synthesized by a wet chemical method (x⩽0.08). X-ray diffraction reveals that single-phase rutile Sn1−xMnxO2 was obtained for x up to about 0.06. Evolution of cell parameters, x-ray photoelectron spectroscopy measurements, thermogravimetric analysis, and quantitative eval…
This work reports the influence of oxidation on the superplasticity of commercially pure titanium at high temperatures. Uniaxial tensile tests were conducted at temperatures in the range 600-800°C with an initial strain rate of 10s-1 to 10s-3. This study shows that oxidization at the surface of the alloy causes oxide…
The required complex of properties of modern pipe steels, including improved weldability and cold resistance, can be achieved due to formation of fine-grained ferrite-bainite microstructure of steel. Effect of various designs of additional alloying of steel on phase transformations with use of deformation CCT diagrams…
Authors have reported theses concerning the cast defect for publication in journal of Japanese Foundry Engineering Society and AFS Transactions. This is a review of these reports. There are various factors in the casting defect that occurs in the article of casting metal, and specific of the generation factor is diffi…
Many steels tubes used in the Oil Industry are constantly exposed to hydrogen sulphide (H2S) which can lead to the diffusion of hydrogen into the steel, potentially provoking hydrogen embrittlement and/or stress corrosion cracking. Additionally the critical region in pipelines is usually considered to be the welded jo…
Alloys based on FePd in the vicinity of the equiatomic composition are good model systems to study the microstructrual and phase transformation behavior of the class of technologically interesting ferromagnetic L10-intermetallics that includes also FePt and CoPt. Here, thermo-mechanical processing, involving cold-work…
Three main hypotheses of hydrogen embrittlement (HE) of austenitic steels are discussed based on the studies of the interatomic interactions, hydrogen-induced phase transformations and dislocations properties. Measurements of electron spin resonance and ab initio calculations of the electron structure witness that the…
Up to now, Solid Oxide Fuel Cell (SOFC) materials and processing does not meet the cost goals for commercialization. This resulted in a worldwide increase in R&D activities dealing with advanced materials and effective manufacturing methods. The present paper describes efforts to process novel SOFC materials as we…
Effect of isothermal aging on martensitic transformation temperatures, mechanical properties and microstructure was investigated for a Ni-rich Ti-Zr-Ni shape memory alloy at temperatures ranging from 673 K to 773 K. The aging behaviour was two stage process: the first stage associated with an increase in the Vickers h…