Materials Literature
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Abstract This work is an investigation of the influence of β‐cyclodextrin (CD) on the synthesis and characteristics of conducting polyaniline composites (PCDs). In a systematic way, this influence was studied with two different approaches for five PCDs: (1) increasing the initial CD content under identical preparation…
A quantitative investigation of the effect of process parameters such as electrolyte concentration, temperature, anodization duration and anodization potential on the pore pattern (including pore diameter and distribution) in anodic alumina was performed based on aluminum anodization experiments. Using fast Fourier tr…
Abstract Energy‐filtered transmission electron microscopy proves directly that ion irradiation and post‐irradiation annealing of a Si/SiO 2 interface results in the formation of a narrow layer of monodisperse Si nanocrystals in the oxide at a tunnel distance from the interface. Position and size of the Si nanocrystals…
Based on phase separation and intergranular tunneling, a correlated resistor network model is proposed to simulate the percolative magnetotransport in some spontaneously phase-separated perovskite oxides and their artificial granular composites. For the inclusion of spin-dependent transport mechanism in a network with…
The effect of aging temperature on precipitates in AZ80 magnesium alloy was studied by using environmental scanning electron microscope (ESEM) and transmission electron microscope (TEM). The precipitate/matrix orientation relationships (ORs) were measured, the precipitation mechanism was analyzed and the effect of pre…
Reaction in aqueous solution of nickel(II) squarate with isonicotinamide yielded well formed yellow crystals of the title compound, 2C6H6N2O+.C4O4(2-), as a side product. The squarate dianion is bisected by a crystallographic twofold rotation axis, which passes through the centres of two opposite bonds of the ring. Cr…
Controlled growth of CdSe nanoneedles and nanorods was realized in a metal–organic chemical vapour deposition system by employing sputtered Au as a catalyst. The controls over the morphology, density and structure of the nanostructures were realized by varying the growth parameters independently. By varying the growth…
It has long been conjectured that the difficulty of heterogeneously epoxidizing higher alkenes such as propene is due to the presence in the molecule of "allylic" H atoms that are readily stripped off by the oxygenated surface of the metal catalyst resulting in combustion. Here, taking advantage of the intrinsically h…
The method of thin film preparation known as layer-by-layer assembly is of growing interest for current and envisioned developments in bionanotechnology. Here, cysteine-containing 32mer peptides have been designed, synthesized, purified, and used to prepare polypeptide films. A range of methods-quartz crystal microbal…
Self-organized Si-Er heterostructure nanowires showed promising 1.54 microm Er(3+) optical activity. Si nanowires of about 120-nm diameter were grown vertically on Si substrates by the vapor-liquid-solid mechanism in an Si-Er-Cl-H(2) system using an Au catalyst. Meanwhile, a single-crystalline Er(2)Si(2)O(7) shell san…
This paper describes the photosynthesis of gold nanoparticles (GNPs) in the presence of bovine serum albumin (BSA). The concentration of NaAuCl4 and the relative ratio of NaAuCl4 to BSA are important parameters for controlling the size of the GNPs. We prepared GNPs having average diameters ranging from 7 to 50 nm by i…
The phase composition and morphology of black powder samples synthesized by pyrogenation of carbon nanotubes and colloidal Fe(OH) 3 were investigated using x-ray diffraction (XRD) and transmission electron microscopy. A new kind allotrope of carbon, 'new diamond' (n-diamond), was obtained in the final black powder whe…
Thermally induced transmission and reflectivity changes are investigated in thin films formed by Bi nanostructures embedded in amorphous Al 2O3. The Bi nanostructures are formed by coalesced nanoparticles forming a quasi-network close to the percolation threshold. Upon heating above the Bi melting temperature (>574…
This paper deals with the investigations on the nucleation and growth of Zinc Oxide (ZnO) nanostructures in a catalyst free synthesis. The ZnO nanostructures have been formed by evaporation of Zn (99.99%) in O2 and Ar atmosphere in single zone furnace under two temperature regions, region A (approximately 1173-1073 K)…
Abstract The effects of molecular weight (MW) and MW distribution on the maximum tensile properties of polyethylene (PE), achieved by the uniaxial drawing of solution‐grown crystal (SGC) mats, were studied. The linear‐PE samples used had wide ranges of weight‐average ( M w = 1.5–65 × 10 5 ) and number‐average MWs ( M…
The development of the ferroelectric polarization of lead–zirconate–titanate (PZT) bulk ceramics under varying electric fields is examined. Repeated partial switching and backswitching results in a decrease of the switchable polarization, but has no effect on the effective strain. This is attributed to a stabilization…
Abstract Acrylic polymer/silica hybrids were prepared by emulsifier‐free emulsion polymerization and the sol–gel process. Acrylic polymer emulsions containing triethoxysilyl groups were synthesized by emulsifier‐free batch emulsion polymerization. The acrylic polymer/silica hybrid films prepared from the acrylic polym…
We observed thermally induced nanomechanical deflection of a hybrid inorganic nanowire (NW) synthesized by pulsed-laser deposition, the structure of which is a carbon nanotube template sandwiched by aluminum oxide and tungsten oxide thin layers. The hybrid NW was gradually bent at a specimen temperature ranging from r…
Microwave absorption (8 GHz to 12 GHz) studies have been made with carbon nanomaterials for the first time. Carbon nanomaterials are synthesized by the pyrolysis of camphor. It is observed that film of carbon prepared under certain synthetic condition, can absorb microwave of either some specific wavelengths e.g., 9.5…
The alkylation of m-cresol with isopropyl alcohol in the presence of novel superacidic catalysts named as UDCaT-4, UDCaT-5, and UDCaT-6 was investigated. The catalysts are modified versions of zirconia showing high catalytic activity, stability, and reusability in the presence of water as compared to conventional sulf…