Materials Literature
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The first protonation site of [V10O28]6– differs both from the second protonation site and from the site of preferential interaction with aqueous manganese(II) ion. It is probably an out-of-plane apex, and not a bridging oxygen as has recently been proposed. The 51V n.m.r. linewidths are almost independent of direct p…
From X-ray experiments performed on oriented samples of (R-)-chloro-2-propyl-p-hexyloxybenzylidene-p'-aminocinnamate (HOBACPC) by means of an electric field, we have identified two new ordered smectic phases which appear at lower temperature than the ferroelectric Sm C* phase. These two phases are characterized by a p…
The Mossbauer spectra of BCC Fe-V alloys in the concentration range 40-80 at.% V have been obtained for both the ordered and disordered states. No broadening of the absorption line has been detected in an 80 at.% V alloy even at liquid He temperature indicating that the alloy is nonmagnetic. Broadening of absorption l…
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTBlock Copolymer Micelles in Dilute SolutionTadao Kotaka, Takeshi Tanaka, Mitsuhiro Hattori, and Hiroshi InagakiCite this: Macromolecules 1978, 11, 1, 138–145Publication Date (Print):January 1, 1978Publication History Published online1 May 2002Published inissue 1 January 1978…
The calculation of dynamical elastic diffuse electron scattering from a crystal containing a point defect or dislocation may require prohibitively large amounts of computing time. Two approximations are described which greatly reduce the computer time required for these calculations, and so allow the simulation of ele…
Ab initio self-consistent-field molecular-orbital calculations were performed on octahedral Fe${\mathrm{F}}_{6}$ and Fe${(\mathrm{CN})}_{6}$ clusters using extensive basis sets of Gaussian-type functions. Two distances relevant for ferrous and ferric compounds are considered. In this paper, we report the part of our r…
A rotating-analyzer technique for measuring the optical birefringence in liquid crystals is described. This apparatus is continuously readable and has excellent sensitivity. For a sample 50 μm thick, the apparatus has a resolution in the change of birefringence of 4 × 10−6, corresponding to a temperature change of 1 m…
Abstract The effect of shear on polymer crystallization kinetics has been studied for three materials at several shear rates and degrees of supercooling. Two poly(ethylene oxide) samples, with molecular weights of 72, 200 and 12, 600, and a poly(e‐caprolactone) material, with a molecular weight of 9, 400, were investi…
Phase relation studies of Si 3 N 1 , SiO 2 , and MgO have established three important subsolidus tie lines, viz. Si 3 N 4 ‐MgO, Si 3 N 4 ‐Mg 2 SiO 4 , and Si 2 N 2 O‐Mg 2 SiO 4 for nonoxidizing fabrication conditions. Strength measurements at 1400°C show that optimum strengths are obtained for compositions approaching…
Mixtures of terminal polar with terminal non-polar nematic liquid crystals usually produce induced smectic phases (ISP). This is shown by the investigation of a great number of systems using the contact method.In general, SA phases are induced. By means of X-ray investigations SB and SE phases were also established. N…
Multiphase caulytic packed-bed reactors are used in chtmid, petrocbemid, as well as in the petroleum Lndustrg for contactirrg gaseau and liquid reactaxzzs with 2 solid ucalyst. Xydrodesulfurszltion of petroleum fractions, liquid-phase catalytic hydrocracking, and brrryaadiol synthesis fmm forrmldehyde and acetylene (o…
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTEffect of Molecular Weight on Excimer Formation of Polystyrenes in SolutionTadahiro Ishii, Takashi Handa, and Satoru MatsunagaCite this: Macromolecules 1978, 11, 1, 40–46Publication Date (Print):January 1, 1978Publication History Published online1 May 2002Published inissue 1…
The compound erroneously reported as NN-bis(chloromethyldimethylsilyl)acetamide has been proven by single-crystal X-ray analysis to be (O–Si)-chloro-[(N-chlorodimethylsilylacetamido)methyl]dimethylsilane.
Abstract Manganese and cobalt ferrites were prepared by the air oxidation of aqueous suspension of Fe(OH)2 and either Mn(OH)2 or Co(OH)2 at 50–80 °C. In alkaline suspensions, all the metal ions are transformed into spinel ferrites, MxFe3−xO4 (M=Mn or Co), by a suitable combination of the oxidation temperature and the…
Use of tannic acid (TA), in sequence with ferric chloride, uranyl acetate or gold chloride resulted in staining of selective but sometimes different sites in paraffin sections. TA-uranyl acetate of TA-ferric chloride stained sites rich in complex carbohydrates, wherease TA-gold chloride stained the collagen of various…
The effect of aging on the temperature dependence of permittivity ( K ) and tan δ as a function of frequency was examined for both ferroelectric and antiferroelectric PLZT compositions. All compositions aged near their transition temperatures exhibited a marked decrease in dispersion between the aging temperature and…
The forced Rayleigh light scattering technique has been applied to measurements of thermal diffusivity in liquid crystalline phases. In the nematic phase of p-methoxy benzylidene p-n-butyl aniline (MBBA), our results are in good agreement with the data obtained by classical methods. The thermal diffusivity anisotropy…
(1978). Physiological indicators of nutrient deficiency in algae. SIL Communications, 1953-1996: Vol. 21, No. 1, pp. 34-41.
Liquid Crystalline Phenyl‐trans‐4‐n‐alkylcyclohexanecarboxylates The syntheses of p‐substituted phenyl‐trans‐4‐n‐alkylcyclohexanecarboxylates 1 – 12 and cyclohexyl‐p‐n‐alkylbenzoates 15 – 17 and their mesomorphic properties are described. p‐n‐Alkoxyphenyl‐trans‐4‐n‐alkylcyclohexanecarboxylates 1 – 8 exhibit larger the…
Three test methods for determining degree of sensitization in austenitic stainless steels have been investigated. The results clearly show that all three test methods are capable of detecting moderate-to-severe degrees of sensitization, but the electrochemical potentiokinetic reactivation technique is the most sensiti…