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An apparent double glass transition in semicrystalline polymers

Raymond F. Boyer1973-12-01Journal of Macromolecular Science Part B

Thermal expansion and/or specific heat and/or dynamic mechanical loss data reveal the presence of two glass-like transitions in bulk crystallized polyethylene, polypropylene, polybutene-1, polypentene-1, cis-and trans-polyisoprene (natural), poly-4-methylpentene-1, isotactic polystyrene, poly(vinyl alcohol), nylon 6,…

Polymer crystallization and propertiesMaterial Dynamics and PropertiesPolymer Nanocomposites and Properties

High-field magnetization and coercivity of amorphous rare-earth-Fe2 alloys

Arthur E. Clark1973-12-01Applied Physics Letters

High-field magnetization studies were made from 4 °K to room temperature on rapidly sputtered TbFe2, DyFe2, and SmFe2. At 4.2 °K the magnetic moment resembles that of polycrystal samples, whereas at room temperature it is substantially lower. Huge coercive forces (20–30 kOe) were observed at 4.2 °K. Partial crystalliz…

Metallic Glasses and Amorphous AlloysMagnetic Properties and ApplicationsMagnetic Properties of Alloys

Hydrogen reduction of the chlorides of cobalt and nickel

Tyson Rigg1973-12-01The Canadian Journal of Chemical Engineering

Abstract Experimental results on the reduction of compacted pellets of the chlorides of cobalt and nickel are reported. The kinetics of the processes are considered in the light of the chloride vaporization mechanism previously proposed to account for the reduction of ferrous and chromous chlorides. Although all these…

Crystallization and Solubility Studies

Oxidation of Poco AXF-Q1 Graphite in Air

John A. Segletes1973-12-01Journal of Spacecraft and Rockets

Covers advancements in spacecraft and tactical and strategic missile systems, including subsystem design and application, mission design and analysis, materials and structures, developments in space sciences, space processing and manufacturing, space operations, and applications of space technologies to other fields.

Fiber-reinforced polymer compositesSpacecraft Design and TechnologyGraphite, nuclear technology, radiation studies

Étude vibrationnelle de complexes du magnesium. Spectroscopie Raman de Mg(NH3)6Cl2et Mg(ND3)6Cl2

R. Plus1973-12-01Journal of Raman Spectroscopy

Abstract L'auteur a pu obtenir les fréquences des vibrations actives en diffusion Raman du chlorure de magnésium hexa‐amminé hydrogéné et deutérié à l'état cristallisé. Toutes les vibrations attendues ont pu être observées pour la première fois pour un composé de ce type (vibrations internes et vibrations externes). L…

Crystal structures of chemical compoundsSolid-state spectroscopy and crystallographyMolecular Spectroscopy and Structure

Sulfonic acid metabolism in the diatom <italic>Navicula pelliculosa</italic>

William F. Busby、A.A. Benson1973-12-01Plant and Cell Physiology

Sulfate uptake and the cellular levels of three sulfonic acids, cysteinolic acid, sulfopropanediol, and the plant sulfolipid, were followed using 35S-sulfate labeled cells of the diatom Navicula pelliculosa in silicate starvation synchrony, sulfur deficiency, and chase experiments. Sulfate uptake was nearly completely…

Groundwater and Isotope GeochemistryDiatoms and Algae ResearchEnvironmental Chemistry and Analysis

X-Ray Induced Electron Emission II

J. N. Bradford1973-12-01IEEE Transactions on Nuclear Science

The x-ray induced photoemission measurements made at AFCRL have been used as a basis for comparison to the computed results of the POEM Monte Carlo electron transport code. The results show spectral shapes which closely resemble the experimental data and absolute yield values which agree within 15-27%. The measurement…

Advancements in Photolithography TechniquesX-ray Spectroscopy and Fluorescence AnalysisElectron and X-Ray Spectroscopy Techniques

Advances in Polyurethane Coatings (1969 to Early 1972)

Wen‐Hsuan Chang、Rogers L. Scriven、John Peffer 等 4 位作者1973-12-01Product R&D

ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTAdvances in Polyurethane Coatings (1969 to Early 1972)Wen-Hsuan Chang, Rogers L. Scriven, John R. Peffer, and Samuel Porter Jr.Cite this: Ind. Eng. Chem. Prod. Res. Dev. 1973, 12, 4, 278–288Publication Date (Print):December 1, 1973Publication History Published online1 May 20…

Polymer composites and self-healing

The Chemical Behavior of Low Valence Sulfur Compounds. VIII. The Oxidation of Sodium Thiosulfate with Ozone

Masahiro Takizawa、Akitsugu Okuwaki、Taijiro Okabe1973-12-01Bulletin of the Chemical Society of Japan

Abstract The oxidation of sodium thiosulfate with ozone in an aqueous solution was investigated as a part of a series of studies on the chemical behavior of such low-valence sulfur compounds as thiosulfate and sulfite. The ozone oxidation was carried out by blowing a mixed gas of ozone and oxygen continuously into a 0…

Thermal and Kinetic Analysis

The electric field and geometrical factor of an annular curved plate electrostatic analyzer

H. Moestue1973-12-01Review of Scientific Instruments

Response and geometrical factor of a charged particle energy spectrometer are presented. Both a theoretical and an experimental approach are used. A set of two annular curved deflection plates constitutes the energy analyzer of the spectrometer. The analyzer has the features of large geometrical factor, high angular a…

Atomic and Molecular PhysicsNuclear Physics and ApplicationsElectron and X-Ray Spectroscopy Techniques

Mass spectrographic determination of hydrogen thermally evolved from uranium and uranium alloys

G.L. Powell、J.B. Condon1973-12-01Analytical Chemistry

ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTMass spectrographic determination of hydrogen thermally evolved from uranium and uranium alloysG. L. Powell and J. B. CondonCite this: Anal. Chem. 1973, 45, 14, 2349–2354Publication Date (Print):December 1, 1973Publication History Published online1 May 2002Published inissue…

Fusion materials and technologiesRadioactive element chemistry and processingNuclear Materials and Properties

Etude de la montée des dislocations au moyen d'expériences de flu age par diffusion dans le magnésium

G. Edelin、Jean Poirier1973-12-01Philosophical magazine

On a effectué des expériences de fluage à, haute température sur des monocristaux de magnésium sollicités en compression suivant l'axe c. L'examen des échantillons déformés en microscopie électronique révèle que la déformation du cristal est due à, la montée pure de dislocations de vecteur de Burgers c situées dans le…

Microstructure and mechanical properties

Lattice expansions of two boron carbides between 12 and 940°C

H. L. Yakel1973-12-01Journal of Applied Crystallography

High-temperature X-ray diffraction methods have been used to determine unit-cell parameters of two boron carbide compositions from 12° to about 940°C. One composition was at the carbon-rich end of the phase field (i.e. B4C), the second at the boron-rich end (5 at. % C by chemical analysis). The lattice expansion of bo…

Rare-earth and actinide compoundsIntermetallics and Advanced Alloy PropertiesBoron and Carbon Nanomaterials Research

Even-tempered atomic orbitals. IV. Atomic orbital bases with pseudoscaling capability for molecular calculations

Richard D. Bardo、Klaus Ruedenberg1973-12-01The Journal of Chemical Physics

Even-tempered atomic orbital bases are formulated which have the property that atomic orbital scaling can be closely simulated through variation of linear expansion coefficients. This ``adaptation to pseudoscaling'' involves two types of adjustments: (1) Optimal orbital exponents and basis sizes are determined for the…

Thermal and Kinetic AnalysisX-ray Diffraction in CrystallographyChemical Thermodynamics and Molecular Structure

Structural and magnetic characterization of .mu.-hydroxobis[pentaamminechromium(III)] chloride monohydrate, the acid rhodo chloride complex

Jack T. Veal、David Y. Jeter、Judith C. Hempel 等 6 位作者1973-12-01Inorganic Chemistry

ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTStructural and magnetic characterization of .mu.-hydroxobis[pentaamminechromium(III)] chloride monohydrate, the acid rhodo chloride complexJack T. Veal, David Y. Jeter, Judith C. Hempel, Richard P. Eckberg, William E. Hatfield, and Derek J. HodgsonCite this: Inorg. Chem. 197…

Magnetism in coordination complexes

The spatial variation of localized power loss in two practical transformer T-joints

A.J. Moses、B.W.J. Thomas1973-12-01IEEE Transactions on Magnetics

The power loss and flux distribution in two commercial T-joints have been compared. The simple 45°-90° T-joint and the slightly more complex 45° offset T-joint were chosen for the investigation, as they are the most common joints currently used in power transformers. The localized and overall power loss of each joint…

Power Quality and HarmonicsMagnetic Properties and ApplicationsMagneto-Optical Properties and Applications

Thermoelectric power of thin copper films

W. F. Leonard、Ho-Yuan Yu1973-12-01Journal of Applied Physics

The thermoelectric power and resistivity of annealed copper films have been measured. From the thermoelectric power values at the minimum in resistivity and the corresponding temperature coefficient of resistance, the calculated values of the energy dependence of the mean free path of conduction electrons and the Ferm…

Electronic Packaging and Soldering TechnologiesCopper Interconnects and ReliabilitySurface and Thin Film Phenomena

Two-phase data for the join monticellite (CaMgSiO4)-forsterite (Mg2SiO4): Experimental results and numerical analysis

Richard R.P. Warner、W. C. Luth1973-12-01American Mineralogist

Subsolidus equilibria along the CaMgSiO.-Mg,SiOn olivine join are governed by partial immiscibility between the end-member phases. The solvi bounding the two-phase region are determined over the temperature range 800-1300'C at 2, 5, and 10 kbar. Within the limits of experimental error, the two-phase data are symmetric…

Clay minerals and soil interactionsCrystallization and Solubility StudiesChemical and Physical Properties in Aqueous Solutions

Relation between physical and chemical processes on semiconductor surfaces

A. Many1973-12-01C R C Critical Reviews in Solid State Sciences

(1973). Relation between physical and chemical processes on semiconductor surfaces. C R C Critical Reviews in Solid State Sciences: Vol. 4, No. 1-4, pp. 515-539.

Advanced Semiconductor Detectors and MaterialsElectron and X-Ray Spectroscopy TechniquesElectronic and Structural Properties of Oxides

Crystallization of amorphous selenium films. I. Morphology and kinetics

K. S. Kim、David Turnbull1973-12-01Journal of Applied Physics

We report a study of the morphology and kinetics of crystallization of films of a-Se vapor deposited on mica substrates. Morphological examination was facilitated by the complete dissolution of the amorphous component of the films by CS2, while the crystalline component was left essentially intact. Crystallization beg…

Material Dynamics and PropertiesPhase-change materials and chalcogenidesBee Products Chemical Analysis