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Low‐Temperature Preparation of Nanocrystalline Lead Zirconate Titanate and Lead Lanthanum Zirconate Titanate Powders Using Triethanolamine

Rabindra Nath Das、Amita Pathak、Panchanan Pramanik1998-12-01Journal of the American Ceramic Society

Nanocrystalline lead zirconate titanate (PZT) powders, with a Zr:Ti ratio of 60:40, have been prepared from a solution of triethanolamine (TEA) and Ti 4+ , Zr 4+ , and Pb 2+ ions. The metal ions were in solution through complex formation with TEA. The soluble metal‐ion–TEA complex formed the precursor material when it…

Ferroelectric and Piezoelectric MaterialsAdvanced ceramic materials synthesisMicrowave Dielectric Ceramics Synthesis

Heat Treating of Tool Steels

作者信息未提供1998-12-01ASM International eBooks

Abstract All tool steels are heat treated to develop specific combinations of wear resistance, resistance to deformation or breaking under loads, and resistance to softening at elevated temperature. This article describes recommended heat treating practices, such as normalizing, annealing, austenitizing, quenching, pr…

Additive Manufacturing Materials and ProcessesMetal Alloys Wear and PropertiesMaterial Properties and Applications

Design Model for Selective Catalytic Reduction Process: Solution of Convective Diffusion and NO x Reaction

Hsunling Bai、Jong-Wen Chwu1998-12-01Journal of Environmental Engineering

A simple model for the design of selective catalytic reduction (SCR) process is presented. The two-dimensional mass transfer equation shown in Bai and Chwu (1997) is simplified and the analytic solution is obtained. The analytic solution is verified by the solution of the numerical two-dimensional model as well as pub…

Catalytic Processes in Materials ScienceAmmonia Synthesis and Nitrogen ReductionIndustrial Gas Emission Control

Mikrostruktur und Wechselverfomnmgs- verhalten des mechanisch randschichtverfestigten Stahls Ck 45

I. Altenberger、B. Schottes、U. Martin 等 4 位作者1998-12-01HTM Journal of Heat Treatment and Materials

Article Mikrostruktur und Wechselverfomnmgs- verhalten des mechanisch randschichtverfestigten Stahls Ck 45 was published on December 1, 1998 in the journal HTM Journal of Heat Treatment and Materials (volume 53, issue 6).

Metal and Thin Film MechanicsMetal Forming Simulation TechniquesMetal Alloys Wear and Properties

Metallographic Practices Generally Applicable to All Metals

作者信息未提供1998-12-01ASM International eBooks

Abstract This article describes the methods and equipments involved in the preparation of specimens for examination by light optical microscopy, scanning electron microscopy, electron microprobe analysis for microindentation hardness testing, and for quantification of microstructural parameters, either manually or by…

Advanced Surface Polishing TechniquesMetal Alloys Wear and Properties

Scale Formation in a Batch Reactor Under Pressure Acid Leaching of a Limonitic Laterite

P. Perdikis、Vladimiros G. Papangelakis1998-12-01Canadian Metallurgical Quarterly

The formation of scale under sulphuric acid pressure leaching conditions of a limonitic laterite ore was investigated. Experiments were conducted using a batch titanium autoclave in order to study the effects of acidity (0.15–0.40 M), and temperature (250–270°C) on scale formation. It was found that scale increases wi…

Calcium Carbonate Crystallization and InhibitionMinerals Flotation and Separation TechniquesCrystallization and Solubility Studies

Synthesis of poly(thio-1,4-phenylene) by oxidative coupling reaction of diphenyl disulfide with potassium persulfate in strongly acidic solutions

Sunita Omprakash Yemul、Omprakash S. Yemul、S. Ponrathnam 等 5 位作者1998-12-01Macromolecular Rapid Communications

The synthesis of poly(thio- 1,4-phenylene) (PPS) at room temperature by the reaction of diphenyl disulfide with potassium persulfate (K2S2O8) in non-basic solvents, in the presence of trifluoromethanesulfonic acid, is reported. The reaction in chlorinated solvents, such as dichloromethane and tetrachloroethane, result…

Chemical Synthesis and ReactionsSynthesis and properties of polymersSynthesis and Characterization of Heterocyclic Compounds

Processing of Titanium and Titanium Alloys

Rodney R. Boyer1998-12-01ASM International eBooks

Abstract Titanium metal passes through three major steps during processing from ore to finished product: reduction of titanium ore to sponge (porous form), melting of sponge and scrap to form ingot, and remelting and casting into finished shape. This article describes primary fabrication, including all operations that…

Metal Forming Simulation TechniquesMetallurgy and Material FormingTitanium Alloys Microstructure and Properties

Photo-oxidative degradation of some water-soluble polymers in the presence of accelerating agents

H. Kaczmarek、A. Kamińska、M. Światek 等 4 位作者1998-12-01Die Angewandte Makromolekulare Chemie

The unsolved problem of plastic waste utilization has led to a great interest in the development of studies of accelerated degradation of polymers. In this work the course of photo-oxidative degradation of some water soluble polymers such as poly(acrylic acid) (PAA), poly(methacrylic acid) (PMA) and poly(vinylpyrrolid…

Microplastics and Plastic PollutionPhotopolymerization techniques and applicationsPolymer Science and PVC

Electrosynthesis of Sodium Hydrosulfite: III. Porous Cathode Materials and Process Model

Leonard L. Scott、Jack Winnick、Paul A. Kohl 等 4 位作者1998-12-01Journal of The Electrochemical Society

The electrolytic manufacture of sodium hydrosulfite is affected by feedstock composition, electrode morphology, and electrode material. Here we show that porous graphite cathodes can provide the highest one‐pass conversion of sodium bisulfite to hydrosulfite, without contamination by sodium thiosulfate. For example, a…

Advanced Photocatalysis TechniquesAdvanced oxidation water treatmentCovalent Organic Framework Applications

Fundamental properties and application of Zn1−XMgXS:Mn thin film electroluminescent devices

Mikihiro Noma、Kouichi Tanaka、Akiyoshi Mikami 等 4 位作者1998-12-01Journal of Applied Physics

By Mg doping of ZnS, the lattice constants and the band gap of Zn1−XMgXS host material were increased. The emission spectrum of Mn in Zn1−XMgXS shifted to shorter wavelengths than that of ZnS:Mn. The electroluminescent (EL) devices fabricated with the source of X=0.32 show 552 nm peak yellowish–green emission. Deposit…

Quantum Dots Synthesis And PropertiesOrganic Light-Emitting Diodes ResearchNanocluster Synthesis and Applications

Pulsed Laser Deposition of VO 2 Single Crystal Thin Films on Sapphire Substrates

Peiran Zhu、S. Yamamoto、A. Miyashita 等 4 位作者1998-12-01Chinese Physics Letters

Thin films of VO 2 single-crystalline on (0001) sapphire substrates have been prepared by visible pulsed laser ablation technique. The crystal quality and properties of the films are evaluated through electrical resistance measurement, x-ray diffraction (XRD), and Rutherford-backscattering spectroscopy/channeling (RBS…

Gas Sensing Nanomaterials and SensorsTransition Metal Oxide NanomaterialsGa2O3 and related materials

Introduction and Overview of Titanium and Titanium Alloys

Rodney R. Boyer1998-12-01ASM International eBooks

Abstract Titanium and its alloys are used in various applications owing to its high strength, stiffness, good toughness, low density, and good corrosion resistance. This article discusses the applications of titanium and titanium alloys in gas turbine engine components, aerospace pressure vessels, optic-system support…

Titanium Alloys Microstructure and PropertiesMaterial Properties and ApplicationsEngineering and Environmental Studies

Electromigration study of Al/low dielectric constant polymer and Al/SiO2 dioxide line structures

Pei-hua Wang、Paul S. Ho、J. G. Pellerin 等 4 位作者1998-12-01Journal of Applied Physics

Electromigration reliability is a key concern for implementation of low dielectric constant (low κ) materials for on-chip interconnects. To address this problem, we have carried out a comparative study of electromigration performance for Al(0.5 wt% Cu) line structures formed with tetraethylorthosilicate (TEOS)-based S…

Corrosion Behavior and InhibitionElectronic Packaging and Soldering TechnologiesCopper Interconnects and Reliability

Hysteresis modeling

E. Della Torre1998-12-01COMPEL The International Journal for Computation and Mathematics in Electrical and Electronic Engineering

In the modeling of transducers, especially magnetic transducers, hysteresis may affect performance. Hysteresis models have been improved greatly and are capable of modeling a large variety of rate‐independent phenomena, and are capable of describing minor loops. Of these, the most useful are: the Preisach model, the p…

Electric Motor Design and AnalysisMagnetic Properties and ApplicationsPiezoelectric Actuators and Control

On Nonessential Descriptions of Crystal Multilattices

J. L. Ericksen1998-12-01Mathematics and Mechanics of Solids

In considering crystal symmetries, crystallographers tend to think in terms of particular configurations. In using nonlinear continuum theory to analyze such things as phase transitions and twinning, one needs to consider a variety of configurations having different symmetries. Correlating these leads to some unanswer…

Crystallization and Solubility StudiesQuasicrystal Structures and Properties

Effects of the Encapsulation of Alkali Ions into Iron(III) Complexes with a Macrocyclic Ring on Magnetic Properties

Yonezo Maeda、Masaki Suzuki、S. Hirose 等 6 位作者1998-12-01Bulletin of the Chemical Society of Japan

Abstract New spin-crossover iron(III) complexes [FeM(salten)L]X with an alkali ion in a macrocycle have been prepared, and the magnetic properties of the complexes in the solid and in acetonitrile solution have been examined, where M is Li+, Na+, K+, or Rb+, H2salten is 4-aza-heptamethylene-1,7-bis(salicylideneiminate…

Magnetism in coordination complexesLanthanide and Transition Metal ComplexesMetal-Catalyzed Oxygenation Mechanisms

Synthesis and Properties of Chiral Dopants Synthesized on the Base of 2-methylbutanol and e-menthol

A. G. Kozachenko、V. G. Nazarenko、В. М. Сорокін 等 6 位作者1998-12-01Molecular crystals and liquid crystals science technology. Section A, Molecular crystals and liquid crystals/Molecular crystals and liquid crystals science and technology. Section A, Molecular crystals and liquid crystals

Chiral dopants are optically active substances used in liquid crystal systems. We have investigated the helical twisting power and its temperature dependences for the systematic rows of optically active organic compounds synthesized on the base of 2-methylbutanol and e-menthol. The compounds differ by molecular, chemi…

Liquid Crystal Research AdvancementsAnalytical Chemistry and ChromatographyMolecular spectroscopy and chirality

Crystal structures of sapphirine and surinamite analogues in the MgO-Ga2O3-GeO2 system

J. Barbier1998-12-01European Journal of Mineralogy

Single crystals of the sapphirine and surinamite analogues in the MgO - Ga2O 3 - GeO 2 system have been grown from potassium molybdate fluxes. Their crystal structures and cation distributions have been determined by X-ray diffraction. Sapphirine, Mg (sub 8.9) Ga (sub 14.2) Ge (sub 4.9) O 40 , crystallizes in the P1 s…

Layered Double Hydroxides Synthesis and ApplicationsMicrowave Dielectric Ceramics SynthesisMagnesium Oxide Properties and Applications

Structural instability of the diamond C(111) surface induced by hydrogen chemisorption

Chun Su、J.-C. Lin1998-12-01The Journal of Chemical Physics

The low energy electron diffraction technique was used to study the hydrogen chemisorption induced structural instability on the diamond C(111) surface. From the quantitative analysis of diffraction spots intensity on the as-dosed, partially desorbed, and annealed hydrogenated C(111) surfaces, the correlation between…

Advanced Chemical Physics StudiesHigh-pressure geophysics and materialsDiamond and Carbon-based Materials Research