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Effects of processing parameters on material properties of mechanically processed polyamide

Junjie Pan、William J. Shaw1995-05-02Journal of Applied Polymer Science

Abstract A semicrystalline polyamide polymer was processed using a new technique known as mechanical alloying. The material processed by this technique was first introduced into a high‐energy ball mill and ground over long periods of time, resulting in the production of extremely fine powders. These powders were subse…

Polymer crystallization and propertiesPolymer Nanocomposites and Propertiesbiodegradable polymer synthesis and properties

2‐[p(N‐tert‐butyl‐N‐oxyamino)phenyl]‐4,4,5,5‐tetramethyl‐4,5‐dihydroimidazol‐3‐oxide‐1‐oxyl, a Stable Diradical with a Triplet Ground State

Katsuya Inoue、Hiizu Iwamura1995-05-02Angewandte Chemie International Edition in English

A value of 2.71 μB for the effective magnetic moment between 100 and 300 K is determined for 1. This magnetic moment supports the assumption of a triplet ground state for 1. The bis(nitroxyl) diradical, which melts only at 180 °C with decomposition, could be characterized by X-ray crystallography. It has a distinctly…

Magnetism in coordination complexesLanthanide and Transition Metal ComplexesElectron Spin Resonance Studies

A Nickel(II) Azide Cubane: Characterization of the Magnetic Exchange Interactions Mediated by a Triply Bridging Azide Group Bound End‐On

Malcolm A. Halcrow、John C. Huffman、George Christou1995-05-02Angewandte Chemie International Edition in English

A ferromagnetic exchange interaction that is not influenced by the distortion of the cubane framework of 1 (see picture; only the O atoms of the EtOH and dbm− ligands are shown) and is mediated by the end-on-coordinated μ3-azide bridges has been detected for the first time. Although the unusual [M4(η1-μ3-N3)4] core is…

Metal complexes synthesis and propertiesMagnetism in coordination complexesLanthanide and Transition Metal Complexes

Collagen turnover and its regulation in the normal and hypertrophying heart

Jill E. Bishop、G. Laurent1995-05-02European Heart Journal

Eighteen different collagen types have now been identified, at least five of which are found in the extracellular matrix of the heart. The interstitial collagens, types I and III are the most abundant components. Due to their tensile strength and arrangement in a network, surrounding and inter-connecting myocytes and…

Orthopaedic implants and arthroplastyCardiac Fibrosis and RemodelingCollagen: Extraction and Characterization

Model Reactions for Photosynthesis—Photoinduced Charge and Energy Transfer between Covalently Linked Porphyrin and Quinone Units

H. Kurreck、Martina Huber1995-05-02OpenAlex

Abstract Photosynthesis is one of the fascinating fields of current interdisciplinary research. It seems miraculous that nature, in the process of evolution, has managed to bring about the process of photosynthesis. The first step involves a charge separation at the reaction centers, which proceeds with 100% quantum y…

Photosynthetic Processes and MechanismsPorphyrin and Phthalocyanine ChemistryPhotochemistry and Electron Transfer Studies

Zur Darstellung und Kristallstruktur eines neuen Kupfer-Antimon-Oxomolybdats: CuSbMo2O8 / On the Synthesis and Crystal Structure of a New Copper Antimony Oxomolybdate: CuSbMo2O8

H. Szillat、Hk. Müller‐Buschbaum1995-05-01Zeitschrift für Naturforschung B

Abstract Single crystals of the hitherto unknown compound CuSbMo 2 O 8 were prepared by recrystallization from melts in closed copper tubes and investigated by X-ray diffractometer technique. CuSbMo 2 O 8 crystallizes in a new structure type with monoclinic symmetry, space group C 6 2h - I12/a1, a = 5.554(2), b = 4.91…

Polyoxometalates: Synthesis and ApplicationsChemical Synthesis and CharacterizationInorganic Chemistry and Materials

Thermotropic liquid‐crystalline aromatic polyester‐graft‐poly(2,6‐dimethyl‐1,4‐phenylene oxide) copolymers

Moriyuki Sato、Takashi Mangyo、Ken‐ichi Mukaida1995-05-01Macromolecular Chemistry and Physics

Abstract Dicarboxy‐terminated poly(2,6‐dimethyl‐1,4‐phenylene oxide) (PPO) macromonomers were prepared and subjected to the preparation of tailor‐made aromatic thermotropic liquid‐crystalline (LC) polyester‐ graft ‐PPO copolymers. The macromonomers were obtained by hydrolysis of dimethyl carboxylate‐terminated PPO mac…

Liquid Crystal Research AdvancementsAdvanced Polymer Synthesis and CharacterizationSynthesis and properties of polymers

Das erste Oxogermanat mit „Stuffed Pyrgoms”: CsNa3Li8{Li[GeO4]}4

Ricardo Brandès、R. Hoppe1995-05-01Zeitschrift für anorganische und allgemeine Chemie

Abstract Durch Tempern der binären Oxide CsO 0,52 , NaO 0,45 , LiO 0,5 und GeO 2 im mol. Verhältnis 1,24:1,4:6,7:3,9 (Ni‐Bömbchen; 600°C/89 bzw. 65 d) wurden erstmals Einkristalle von CsNa 3 Li 8 {Li[GeO 4 ]} 4 in Form von schwachgelblichen Prismen sowie blaßgelbem Pulver erhalten: Raumgruppe I 4/ m (I. T. Nr. 87) mit…

Crystal Structures and PropertiesPolyoxometalates: Synthesis and ApplicationsInorganic Chemistry and Materials

Numerical method for the performance of a separate-type transformer connected to battery charger

K. Hirata、Yoshio Mitsutake、Yoshiyuki Ishihara 等 4 位作者1995-05-01IEEE Transactions on Magnetics

The purpose of this paper is to present an easy method for analyzing the operating characteristics of a separate-type transformer connected to an external circuit including elements such as batteries, resistances, and diodes. This method, a combination of two- and three-dimensional finite element methods, has been app…

Advanced DC-DC ConvertersMagnetic Properties and ApplicationsInduction Heating and Inverter Technology

Modeling Fission Product Vapor Transport in the Falcon Facility

I. Shepherd、Yannis Drossinos、Christopher G. Benson1995-05-01Nuclear Technology

An extensive database of aerosol experiments exists and has been used for checking aerosol transport codes. Data for fission product vapor transport are harder to find. Some qualitative data are available, but the Falcon thermal gradient tube tests carried out at AEA Technology’s laboratories in Winfrith, England, mar…

Nuclear reactor physics and engineeringNuclear Materials and PropertiesCyclone Separators and Fluid Dynamics

Sulfidation of Zinc by Traces of Hydrogen Sulfide in Air

Jan Svensson、L.‐G. Johansson1995-05-01Journal of The Electrochemical Society

The effect of in the sub‐parts per million range on the atmospheric corrosion of zinc has been investigated in the laboratory. Each sample was exposed individually to air with careful control of pollutant concentration, relative humidity, and flow conditions. Monitoring of concentration at the outlet of the corrosion…

Corrosion Behavior and Inhibition

Diamond deposition on carbon fibers

S. İsmat Shah、M. M. Waite1995-05-01Journal of Vacuum Science & Technology A Vacuum Surfaces and Films

Diamond films have been deposited on carbon fibers with diameters as small as 5 μm by microwave plasma assisted chemical vapor deposition. An ultrasonic pretreatment of the fibers in a bath containing methanol and diamond paste was required for successful coating of the fibers. In the absence of such treatment, the fi…

Metal and Thin Film MechanicsDiamond and Carbon-based Materials ResearchLubricants and Their Additives

Electromagnetic field analysis of film transformer

Yoichi Midorikawa、Iliana Marinova、S. Hayano 等 4 位作者1995-05-01IEEE Transactions on Magnetics

In this paper, we investigate a thin film transformer for small electronic devices. This transformer is composed of the lamination of thin film conductors. Both the primary and secondary coils of the film transformer are arranged coaxially on one layer and multiply laminated. The operation principle of the transformer…

Magnetic Properties and ApplicationsThermal Analysis in Power TransmissionInduction Heating and Inverter Technology

X-ray photoelectron and infrared spectroscopies of Cu-implanted silica and borosilicate glasses

D. O. Henderson、M. A. George、Y. S. Tung 等 10 位作者1995-05-01Journal of Vacuum Science & Technology A Vacuum Surfaces and Films

Fourier transform infrared (FTIR) spectra and x-ray photoelectron spectra (XPS) were acquired from Cu implanted in fused silica and a borosilicate glass. The FTIR spectra indicate that Cu ion implantation in the silica and borosilicate glasses results in an intensity decrease in the Si–O stretching vibration. The Si–O…

Advanced ceramic materials synthesisGlass properties and applicationsPigment Synthesis and Properties

Texture analysis of chemical vapor deposited diamond films on silicon by the component method

K. Helming、Sebastian Geier、M. Schreck 等 6 位作者1995-05-01Journal of Applied Physics

Oriented diamond films have been grown on Si(001) and Si(111) substrates by microwave plasma chemical vapor deposition. X-ray diffractometry has been employed for pole figure measurements which have been evaluated by the component method. This technique can be applied to multiphase materials with overlapping pole figu…

Metal and Thin Film MechanicsSemiconductor materials and devicesDiamond and Carbon-based Materials Research

Objective evaluation of a stabilized garment parts handle

Jelka Geršak、Andreja Saric1995-05-01International Journal of Clothing Science and Technology

Presents the objective evaluation of a stabilized garment parts handle, based on determination of mechanical and physical properties of fabrics using the Kawabata Evaluation System. Parameters that influence the handle are shown on the basis of 16 parameters of mechanical and physical properties of shell fabric, inter…

Additive Manufacturing and 3D Printing TechnologiesTextile materials and evaluationsErgonomics and Musculoskeletal Disorders

Interfacial analyses of copper corrosion by acrylic and methacrylic acids using XPS, auger and grazing angle FTIR spectroscopy

D. Billy Yang、David Wolf1995-05-01Surface and Interface Analysis

Abstract We have observed that methacrylic acid (MA) is far more corrosive than acrylic acid (AA) on copper surfaces when copper was exposed to the vapor of these two acids at ambient temperature and environment. With the aid of modern surface‐sensitive instrumentation, which included grazing angle Fourier transform i…

Corrosion Behavior and InhibitionElectron and X-Ray Spectroscopy TechniquesNon-Destructive Testing Techniques

Mechanisms of radiation damages formation in gadolinium gallium garnet (GGG) single crystals

A. Matkovskii、D. Y. Sugar、S. Ubizskii 等 4 位作者1995-05-01Radiation effects and defects in solids

The influence of γ-, electrons and reactor neutrons irradiation on the optical and electrophysical properties of Gd3 Ga5 O12 single crystals is investigated. Experimental data and theoretical estimations of radiation defect concentration are compared.

Luminescence Properties of Advanced MaterialsPhotorefractive and Nonlinear OpticsNuclear materials and radiation effects

Influence of surface treatments of hot‐dip galvanized steels on their acid–base properties and on their reactions with some organic compounds

F. Gaillard、E. Peillex、M. Romand 等 5 位作者1995-05-01Surface and Interface Analysis

Abstract The surface of hot‐dip galvanized steels is a complex system highly dependent upon the composition of the galvanization bath and upon surface treatments such as degreasing, alkaline etching and chromate conversion. In this study, industrial zinc‐coated samples are subjected to degreasing, alkaline etching and…

Corrosion Behavior and InhibitionHigh voltage insulation and dielectric phenomenaMaterial Properties and Processing

Nature of the first diffraction peak in glassy selenium

F. J. Bermejo、M. Garcı́a-Hernández、F. J. Mompeán 等 5 位作者1995-05-01Physical review. B, Condensed matter

The physical significance of the first diffraction peak in glassy Se is discussed in the light of recent experimental results regarding the temperature dependence of the parameters characterizing the first peaks in the elastic S(Q,\ensuremath{\omega}=0) and static S(Q) structure factors. The rather different behavior…

Glass properties and applicationsPhase-change materials and chalcogenidesSolid-state spectroscopy and crystallography