Materials Literature
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In this study, anionic gadofullerene {Gd@C60[C(COOH)2](10)} was used as an in vitro cellular magnetic resonance imaging label. The cellular uptake characteristics of this gadofullerene were significant and nonspecific, and excellent labeling efficiency (98-100%) was achieved without a transfecting agent. The average u…
In this report, we describe a novel solvothermal procedure for the synthesis of nanosized particles of barium titanate (BaTiO 3 ). We have been able to synthesize large amounts of nearly uniform sized BaTiO 3 nanocrystals in the size range of 5−37 nm. The advantages of our technique over other previously reported hydr…
Abstract This paper describes experiments in which mechanisms of crystal growth are inferred from the surface nanotopography of natural and synthetic dolomite using atomic force and scanning electron microscopy. Synthetic dolomite was formed by replacement of calcite at 218°C in Mg–Ca–Cl solutions. The first products…
Magnetic and magnetoelastic properties of a series of Ga-substituted cobalt ferrites, CoGaxFe2−xO4 (x=0.0–0.8), have been investigated. The Curie temperature TC and hysteresis properties were found to vary with gallium content (x), which indicates that exchange and anisotropy energies changed as a result of substituti…
The kinetics of 18O/16O isotopic exchange over CeO2-ZrO2-La2O3 and Pt/CeO2-ZrO2 catalysts have been investigated under the conditions of dynamic adsorption-desorption equilibrium at atmospheric pressure and a temperature range of 650-850 degrees C. The rates of oxygen adsorption-desorption on Pt sites, support surface…
The selective production of long, horizontally aligned carbon nanotubes (>1 mm) or short, randomly oriented carbon nanotubes (<50 μm) was achieved in a chemical vapor deposition process by influencing the catalyst pretreatment and reaction conditions. A detailed investigation was undertaken to elucidate the mechanism…
Polycrystalline BiFeO3 film has been fabricated by a chemical solution deposition on Pt∕Ti∕SiO2∕Si(100) substrates. A ferroelectric hysteresis loop showed a high remanent polarization of 47μC∕cm2 at room temperature. Leakage current density was on the order of 10−1A∕cm2 at 100kV∕cm, indicating the high leakage current…
Alumina thin films were manufactured from aqueous slurries by dip coating. Film thickness as function of substrate withdrawal velocity could be correctly modeled by Landau and Levich's theory. Samples were sintered on a rigid substrate at 1350°C for different isothermal times to achieve relative densities from 84% to…
Several commercial high density ferroelectric random access memory (FeRAM) devices utilize stacks of submicron lead zirconate-titanate (PZT) capacitors. The low-field electrical characteristics of these capacitors display a specific frequency dependence which is best represented by a constant phase element (CPE) in th…
The magnetic, magnetocaloric, and magnetoresistive properties of the polycrystalline compound HoNiAl have been studied. The temperature variations of magnetization and heat capacity show that the compound undergoes two magnetic transitions, one at 14K and the other at 5K. The former is due to the paramagnetic-ferromag…
In the present study, the ballistic resistance of sandwich composite structures for vehicle armor panel applications is investigated. The core material of each sandwich structure is a layer of tiled alumina ceramic, combined with a layer of two-dimensional (2D)/three-dimensional (3D) S-2 glass-based woven composite la…
The Bi 2 Te 3 /Te multiple heterostructure nanowire arrays were successfully synthesized through a simple thermal annealing process of the supersaturated Bi−Te alloy nanowire arrays. On the basis of the systematic investigations of the thermal treatment processes, it is considered that the precipitation confined by po…
The preparation and properties of protective sol–gel coatings on metallic substrates are reviewed. Control of the coating microstructure is critical to obtain the desired properties and this requires optimisation of processing parameters that include sol composition, synthesis and processing conditions, deposition met…
Four new one-dimensional materials and one dimer complex based on the linkage of [Nb6O19] clusters and [CuLx] (L=ethylenediamine (en), NH3, H2O) assemble under ambient conditions. These phases include the following: Rb4[Cu(en)2(H2O)2]3[(Nb6O19H2)2Cu(en)2].24H2O (1), space group P; [Cu(en)2(H2O)2]2[(Nb6O19H2)Cu(en)2].1…
Copolyesters of isosorbide and 1,4‐butane diol were prepared by Ti(OBu)4‐catalyzed transesterifications with dimethyl terephthalate in bulk at temperatures up to 250°C. The content of isosorbide was considerably lower than expected from the feed ratio and the molar masses were low, so that no DSC measurements were con…
Nanotubes are important "building block" materials for nanotechnology, but a synthesis process for short (sub-100-nm) solid-state nanotubes with structural order and monodisperse diameter has remained elusive. To achieve this goal, it is critical to possess a definitive mechanistic framework for control over nanotube…
Abstract Blue phases have two major advantages over commonly used nematic phases:1) the response is much faster, 2) the zero‐electric field state is optically isotropic. We demonstrate the sufficiently large electric field‐induced birefringence and the micro‐second response of the polymer‐stabilized blue phases and th…
Concomitant with the development of metal-based spintronics in the late 1980s and 1990s, important advances were made on the growth of high-quality oxide thin films and heterostructures. While this was at first motivated by the discovery of high-temperature superconductivity in perovskite Cu oxides, this technological…
The radical copolymerization of gum Arabic and polyaniline was done using peroxydisulfate as oxidant and initiator. The produced copolymer was electrically active, water‐soluble and has redox property. The redox behavior of the copolymer was studied using cyclic voltammetry and compared with the pure polyaniline. The…
PURPOSE: To evaluate the biliary enhancement dynamics of the two gadolinium chelates Gd-BOPTA (MultiHance) and Gd-EOB-DTPA (Primovist) in normal healthy subjects. MATERIAL AND METHODS: Ten healthy volunteers were evaluated with both agents by magnetic resonance (MR) imaging at 1.5T using a breath-hold gradient-echo T1…