Materials Literature
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An empirical equation form, approximating the apparent dependence of the strength of brittle polycrystalline specimens on the combined effect of porosity and grain size, has been developed from concepts and data in the literature. The form is shown to be applicable to data for thoria and chromium carbide specimens.
The total photoelectric cross sections of copper, molybdenum, silver, tantalum, and gold have been measured at 662 kev. A highly collimated beam of gammas from a Cs-137 source impinged upon a thin disk of a target material. Photoelectrons from a target were detected by a plastic scintillator subtending very nearly $4\…
Ferroelectric ${(\mathrm{glycine})}_{3}$\ifmmode\cdot\else\textperiodcentered\fi{}${\mathrm{H}}_{2}$S${\mathrm{O}}_{4}$ crystallizes at room temperature in the monoclinic system with $a={9.41}_{7}$ A, $b={12.64}_{3}$ A, $c={5.73}_{5}$ A, $\ensuremath{\beta}=110\ifmmode^\circ\else\textdegree\fi{}{23}^{\ensuremath{'}}$;…
Montmorillonite, illite, chlorite, and kaolinite in the playas of southern California are traceable directly to the source areas surrounding the basins. No evidence found in this investigation suggests that these clay minerals are unstable in the sodic or calcic saline lake environment, but this conclusion may not be…
Proto-enstatite, at room temperature, is orthorhombie with 8 units of MgSiO3 in a cell of dimensions a ----9.25, b ----8.74, c = 5.32 A, pseudo space group Pbcn. The atomic coordinates of the pseudo space group were determined from X-ray powder data. The SiO3 chain is fully extended. One of the Mg atoms has an irregul…
A new modification of boron, resulting from the pyrolytic decomposition of BI z on a heated surface (800 C. to 1100 C.), has been found to have a simple rhombohedral structure, with a 0 = 5.057 /~ and c~ = 58.06 , space group R3m, Z ----12. The atomic parameters have been obtained from a single crystal using the prece…
The structure was determined and refined by use of Pa t te rson and Fourier projections on the three faces of the uni t cell. The seven shortest Zr-O separations in the coordination polyhedron around each zirconium range from 2.04 to 2.26 A; since the next nearest Zr-O separat ion is 3.77 ~ , the coordination number o…
Abstract The influence of zinc oxide and stearic acid on the structures of vulcanizates was traced in stocks with mercaptobenzothiazole by means of the kinetics of swelling. It was found that zinc oxide in the presence of stearic acid has a marked influence on the rate and degree of crosslinked network formation in vu…
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTReaction of Hydrazine Hydrate and Phenylhydrazine with MalononitrileTADASHI SATOCite this: J. Org. Chem. 1959, 24, 7, 963–966Publication Date (Print):July 1, 1959Publication History Published online1 May 2002Published inissue 1 July 1959https://pubs.acs.org/doi/10.1021/jo010…
Abstract The thermal‐oxidative degradation of films of poly(ethyl acrylate) about 35 μ thick were studied in the temperature range of 80 to 120°C. The degradation was followed by determining intrinsic viscosity changes, absorption of oxygen, and production of titratable acidity in the polymer. From viscosity results a…
Results of measurements of retraction as a function of twist are given for yarns produced by continuous twisting processes, as opposed to the twisting of a fixed length. These are compared with Tattersall's2 earlier work and also with the predictions of Treloar's1 theory. When continuous twisting methods are used, the…
(1959). The saturation magnetostriction of ferromagnetics. Advances in Physics: Vol. 8, No. 31, pp. 252-291.
Abstract The potentials at which iron is converted into anhydrous cubic oxide in certain inhibitive solutions have been measured and it has been shown that these potentials are more negative than the potentials acquired by unpolarised specimens immersed in the solutions for 3 days. It is suggested that when iron, carr…
Abstract Effects of gamma radiation on the properties, such as melt viscosity, elastic modulus above the melting point, creep fracture time above the melting point, density, and the degree of crystallinity by x‐ray diffraction, of polytetrafluoroethylene resin were studied. When exposed to the radiation from a Co 60 g…
Abstract Using a torsion pendulum, measurements have been made of the dynamic modulus of rigidity of wool fibers during the process of sorbing or desorbing water (from the vapor phase). Anomalous behavior is observed, with low values of rigidity which cannot be accounted for in terms of equilibrium data. It appears th…
Abstract Crystallization kinetics of Hercules polypropylenes were studied between 133 and 155 ° C. using dilatometers. The crystallization rates of these samples became too rapid below 133 ° C. for accurate dilatometric measurements. One sample (A) was a commercial sample containing stabilizer and 9% extractable polym…
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTSystematics in the Chemistry of the Boron HydridesR. W. Parry and L. J. EdwardsCite this: J. Am. Chem. Soc. 1959, 81, 14, 3554–3560Publication Date (Print):July 1, 1959Publication History Published online1 May 2002Published inissue 1 July 1959https://doi.org/10.1021/ja01523a…
The rate of isothe rm al bulk crystalli zation of poly (e hloro trifluoroethylene) , 2'm = 221 C, was measured from 170 0 to 200 0 C. The intrinsic bulk cr ystallization, which acc uraLe ly ~o llow e d a n n= 2 la\,:, was. shown t o be a res ult of the i~lj ect ion of primary nu clei spora di cally III Lime, with on e…
Abstract The problem of the mechanism of macromolecule orientation occurring in the formation of fibers from polymer melts has been qualitatively analyzed. As a result of birefringence, x‐ray, and spinning stress investigations carried out on polycapronamide fibers, the main parameters determining orientation have bee…
Abstract Vinyl-(I), allyl-(II), and 3-butenyl-trimethylsilane(III) were polymerized at 70°C in n-heptane with the heterogeneous catalyst of Ziegler’s type. The monomer I gave only a small yield of polymer, while the monomers II and III gave moderate amounts of polymers. The amorphous and crystalline polymers of these…