Materials Literature
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A single crystal of a birefringent Cr-bearing majorite, Mg 3 Mg 0.34 Si 0.34 Al 0.18 Cr 0.14 ) 2 Si 3 O 12, was synthesized at 20 OPa and 2000 °C using “6-8” type uniaxial split-sphere apparatus. This garnet is tetragonal with the unit-cell parameters a ≈ c and deviates slightly from cubic symmetry. The structure refi…
This review comprises an up‐to‐date literature survey on the topic of food contact can coatings. Special consideration is given to the choice of can coating. To avoid reactions between the food and the metal of the can, the interior metal surface is treated with lacquers which act as a barrier. This ensures that the r…
Superplasticity can be generally achieved by grain boundary sliding (GBS). The GBS in polycrystalline materials sometimes accompanies with intergranular fracture because of stress concentrations at triple points and/or GB irregularities. To develop the superplastic flow, it is necessary to suppress the intergranular c…
A series of copolyesters were prepared by the incorporation of p-hydroxybenzoic acid (HBA), hydroquinone (HQ), and terephthalic acid (TA) into poly(ethylene terephthalate) (PET). On the basis of viscosity measurements, high molar mass copolyesters were obtained in the syntheses, and 1H-NMR analyses indicated the total…
Abstract Polyesteramides were prepared by reactive extrusion by a condensation reaction of a fatty dicarboxylic acid [Unichema Pripop (1009) (C36)] or a carboxyl terminated polyamide 12 (CTPA 12) and a dioxazoline coupling agent [(1,3‐Phenylene)‐bis(2‐Oxazoline), (OO)]. The Residence Time Distribution (RTD) was measur…
Platelike particles of SrFe12O19 with epitaxially grown Fe3O4 overlayer were prepared by a wet method. The experimental results have shown that modified sample has an exchange coupling between epitaxial layer and Sr-ferrite core. As Fe2+ quantity added, coercive force decreased and saturation magnetization increased,…
Abstract An experimental study was conducted in a 0.43‐m‐ID packed column to determine the axial mixing properties of air and water under single‐phase flow conditions. The packings used were 25.4‐mm ceramic Raschig rings, one modern random packing, 25.4‐mm metal Pall rings; two structured packings, Sulzer BX and Flexi…
Abstract Phase separation of poly(2‐chlorostyrene)/poly(vinyl methyl ether) (P2CS/PVME) blends driven by a temperature gradient was investigated by phase‐contrast optical microscopy combined with digital image analysis. The samples were set in a temperature gradient in such a way that the two ends of the gradient cove…
The nature of minerals in the B horizons of alpine forest soils in subtropical and tropical areas remains to be identified. The objective of this study was to investigate the distribution of Fe-oxides and hydroxy-interlayered vermiculite (HIV) in typical alpine forest soils of Taiwan. Five pedons at roughly 2000 m ele…
The synthesis of tetraphenylporphyrin, H2[TPP], and para-substituted tetraphenylporphyrins, H2[(p-X)4TPP], where X = CN, CH3, and OCH3, is easily accomplished using microscale glassware. The compounds are synthesized from inexpensive starting reagents.
The effect of antioxidant on the reaction mechanism of chemical crosslinking of polyethylene with dicumyl peroxide (DCP) at high temperatures was investigated by electron spin resonance (ESR). The crosslinking reactions were induced by the alkyl radicals in polyethylene (PE) formed by the thermal decomposition of DCP…
The crystal structures of 2,6-naphthalenedicarboxylic acid (NDA) and dimethyl 2,6-naphthalenedicarboxylate (NDC) have been solved ab initio using a combination of X-ray powder diffraction and computational chemistry techniques. These two crystal structures, and that of 2,6-dimethylnaphthalene (DMN), have been refined…
High power laser shocks with a 0.6 ns pulse duration have been used to study the debonding of coatings electrolytically deposited on the opposite face of the substrate than the one shocked. Experiments have been carried out on various substrate/coating systems such as stainless steel/copper or nickel and hastelloy X/p…
IMP-specific, High Km 5'-nucleotidase (EC 3.1.3.5) is an ubiquitous enzyme, the activity of which is highly regulated by substrate, ATP, and inorganic phosphate. The cDNA encoding this enzyme has recently been cloned and found to contain a unique stretch of nine glutamic and four aspartic acid residues at the C-termin…
Solid solution of manganese in yttria‐stabilized zirconia (YSZ) may occur in the electrolyte of solid oxide fuel cells. Possible changes in valence, coordination, and site occupancy of Mn in YSZ are of interest. Also, subsequent structural modification of the cubic YSZ, as well as the possible ordering of vacancies, h…
Finite domains of a Langmuir monolayer in a phase with tilted molecules can be modeled by a simple elastic free energy of an $\mathrm{XY}$ order parameter with isotropic and anisotropic line tension terms. The domains can and often do contain nontrivial textures, which in turn influence the shape of the domains. Herei…
Reaction of A2CO3 (A = K, Rb) with Sn and Se in an H2O/CH3OH mixture at 115–130°C affords the isotypic selenidostannates(IV) A6Sn4Se11 _. xH2O (A = K, x = 8) 1 and 2 whose discrete [Sn4Se11]6– anions each contain two corner-bridged ditetrahedral [Sn2Se6]4– species. Similar reaction conditions with A = Cs afford Cs2Sn2…
Summary Barium sulfate scale deposition in the near wellbore, perforations, or production tubing has severely affected well productivity in many North Sea Fields. This is due to the co-mingling of the sulfate-rich seawater used for reservoir sweep with formation water containing high concentrations of barium ions. Mit…
Mean standard errors in atomic displacement parameters (ADPs) resulting from protein crystal structure determinations are estimated by comparing the ADPs of protein-chain pairs of identical sequence within the same crystal or within different crystals displaying the same or different space groups. The estimated ADP st…
According to IEC 34-2 and the harmonised European standards derived from it, the additional losses in electrical machines are taken into account by an estimated 0.5% P1 in the indirect determination of efficiency. In the USA, extensive measurements are made to this effect (IEEE/NEMA), whereas in Japan the additional l…