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Determination of the Magnetic Axes of Cobalt(II) and Nickel(II) Azurins from 1H NMR Data: Influence of the Metal and Axial Ligands on the Origin of Magnetic Anisotropy in Blue Copper Proteins

Antonio Donaire、Jesús Salgado、José‐María Moratal1998-05-22Biochemistry

The orientation and the axial, Deltachiax, and rhombic, Deltachirh, components of the magnetic susceptibility tensor anisotropy for the cobalt(II) and nickel(II) derivatives of azurin from Pseudomonas aeruginosa have been determined from 1H NMR data. For both derivatives, the axial geometry of the system determines th…

Enzyme Structure and FunctionProtein Structure and DynamicsMetal-Catalyzed Oxygenation Mechanisms

A density functional study of the electronic structure of sodalite

Kendall T. Thomson、Renata M. Wentzcovitch1998-05-22The Journal of Chemical Physics

We have conducted a first principles density functional theory (DFT) calculation to explore the electronic structure of sodalite at various stages of Al-substitution. By calculating the electronic structure of both substituted and unsubstituted frameworks, with and without the presence of extra-framework atoms, we sho…

Advanced Condensed Matter PhysicsZeolite Catalysis and SynthesisCrystal Structures and Properties

Ab Initio Investigation of Gadolinium Complexes with Polyamino Carboxylate Ligands and Force Fields Parametrization of Metal−Ligand Interactions

Ugo Cosentino、Giorgio Moro、Demetrio Pitea 等 7 位作者1998-05-22The Journal of Physical Chemistry A

The conformational properties of five gadolinium(III) complexes with polyamino carboxylate (PAC) ligands used as magnetic resonance imaging contrast agents have been investigated by ab initio and molecular mechanics (MM) methods. Ab initio calculations were performed using an effective core potential (ECP) that includ…

Lanthanide and Transition Metal ComplexesMagnetism in coordination complexesRadioactive element chemistry and processing

A statistical rate theory study of interface concentration during crystal growth or dissolution

Marcus Dejmek、C. A. Ward1998-05-22The Journal of Chemical Physics

The concentration at the interface of a growing or dissolving crystal has been previously found experimentally to be different from the equilibrium value; however, a method for predicting this concentration has not been available. We report an investigation that uses statistical rate theory to obtain the expression fo…

Crystallization and Solubility StudiesCalcium Carbonate Crystallization and InhibitionMinerals Flotation and Separation Techniques

Efficient introduction of alkene functionality into proteins in vivo

Jan C. M. van Hest、David A. Tirrell1998-05-22FEBS Letters

The methionine analogue 2-amino-5-hexenoic acid (homoallylglycine, Hag) can be utilized by Escherichia coli in the initiation and elongation steps of protein biosynthesis. Use of an E. coli methionine auxotroph and Hag-supplemented medium resulted in replacement of ca. 85% of the methionine residues in mouse dihydrofo…

Biochemical and Molecular ResearchEnzyme Structure and FunctionUbiquitin and proteasome pathways

Extended Moment Formation and Second Neighbor Coupling in Li$_2$CuO$_2$

Ruben Weht、W. E. Pickett1998-05-22arXiv

Comprised of ferromagnetic edge-sharing CuO$_2$ chains that order in antialigned fashion at T$_N$=9 K, Li$_2$CuO$_2$ is found from local spin density calculations to display several surprising characteristics: (1) the ordered moment/f.u. of 0.92 $μ_B$ is the largest for any low dimensional cuprate system, in agreement…

Materials Science

Origin of the anomaly in diffuse scattering from disordered Pt-V alloys

Igor Tsatskis1998-05-22arXiv

An explanation of the anomalous concentration dependence of diffuse scattering from the Pt-V alloy system (splitting of the (100) short-range order intensity peak with increasing Pt content) is proposed. The effect is attributed to the competition between the interaction and self-energy curvatures. A similar temperatu…

cond-mat.stat-mechMaterials Science

Polarized Wannier functions: ab-initio study of the dielectric properties of silicon and gallium arsenide

Pablo Fernández、Andrea Dal Corso、Alfonso Baldereschi1998-05-22arXiv

We present a first-principles calculation of the electronic properties of crystalline silicon and gallium arsenide in a uniform electric field. Polarized Wannier-like functions which are confined in a finite region are obtained by minimizing a total-energy functional which depends explicitly on the macroscopic polariz…

Materials Science

Molecular Dimensions for Adsorptives

Charles Edwin Webster、Russell S. Drago、Michael C. Zerner1998-05-22OpenAlex

Pore volumes, accessible surface areas, and the thermodynamics of adsorption are essential in the understanding of solid surface characteristics fundamental to catalyst and adsorbent screening and selection. The recently developed Multiple Equilibrium Analysis (MEA) provides a thorough characterization of the adsorpti…

Surface Chemistry and CatalysisAdsorption and biosorption for pollutant removalMesoporous Materials and Catalysis

Dynamic simulation of diblock copolymer microphase separation

Robert D. Groot、Timothy J. Madden1998-05-22OpenAlex

The dissipative particle dynamics (DPD) simulation method has been used to study mesophase formation of linear (AmBn) diblock copolymer melts. The polymers are represented by relatively short strings of soft spheres, connected by harmonic springs. These melts spontaneously form a mesocopically ordered structure, depen…

Material Dynamics and PropertiesAdvanced Polymer Synthesis and CharacterizationBlock Copolymer Self-Assembly

Fullerene Pipes

Jie Liu、Andrew G. Rinzler、Hongjie Dai 等 15 位作者1998-05-22OpenAlex

Single-wall fullerene nanotubes were converted from nearly endless, highly tangled ropes into short, open-ended pipes that behave as individual macromolecules. Raw nanotube material was purified in large batches, and the ropes were cut into 100- to 300-nanometer lengths. The resulting pieces formed a stable colloidal…

Fullerene Chemistry and ApplicationsCarbon Nanotubes in CompositesNanotechnology research and applications

The dependence of the fraction of material removed on the degree of penetration in single particle abrasion of ductile materials

Jiaren Jiang、R.D. Arnell1998-05-21Journal of Physics D Applied Physics

The relationship between the fraction of material removed and the degree of penetration often observed in the literature during single-particle grooving tests on metals is examined in terms of low cycle fatigue. It is shown that the fraction of material removed is closely related to the low cycle fatigue behaviour of…

Surface Treatment and Residual StressErosion and Abrasive MachiningMetal Alloys Wear and Properties

Electron Microscopy Study of a New Cation Deficient Perovskite-like Oxide: Ba3MoNbO8.5

E. Garcı́a-González、M. Parras、J.M. González-Calbet1998-05-21Chemistry of Materials

A new ordering scheme in cationic-deficient perovskite-like phases of the Ba n (Mo,Nb) n - δ O 3 n - x system has been described for the composition Ba 3 MoNbO 8.5, which has an oxygen stoichiometry between those of the 9R polytype and the palmierite structure. An electron diffraction and high-resolution electron micr…

Advanced Condensed Matter PhysicsMagnetic and transport properties of perovskites and related materialsFerroelectric and Piezoelectric Materials

New Chemical and Electrochemical Synthesis of the [Mn4IVO6(bpy)6]4+ Cluster. Electrochemical Interconversion with Corresponding Bi- and Mononuclear Complexes

Marie‐Noëlle Collomb、Alain Deronzier、Alexis Piron 等 5 位作者1998-05-21Journal of the American Chemical Society

A new chemical and electrochemical synthesis of the linear tetranuclear manganese complex, [Mn 4 IV O 6 (bpy) 6 ] 4+ (bpy = 2,2‘-bipyridine) ( 4 ) is described. This complex can be synthesized by a two-electron oxidation of an aqueous solution of the mononuclear [Mn II (bpy) 3 ] 2+ ( 1 ) one. The aqueous solutions wer…

Porphyrin and Phthalocyanine ChemistryMagnetism in coordination complexesMetal-Catalyzed Oxygenation Mechanisms

A Vapochromic Photodiode

Yoshihito Kunugi、Larry L. Miller、Kent R. Mann 等 4 位作者1998-05-21Chemistry of Materials

A sandwich composed from indium−tin oxide, an electrodeposited hole transport layer, a layer of a stacked platinum complex, and an aluminum electrode acted as a photodiode. Exposure of the sandwich to organic vapors changed the color of the platinum complex and changed the action spectrum of the photodiode.

Luminescence and Fluorescent MaterialsPhotochromic and Fluorescence ChemistryPorphyrin and Phthalocyanine Chemistry

Improved capping layers for suppression of ambient ageing in porous silicon

T Giaddui、L.G. Earwaker、K.S. Forcey 等 5 位作者1998-05-21Journal of Physics D Applied Physics

Accelerator-based nuclear techniques were used to study the ageing of as-prepared and aluminium-capped porous silicon samples with a porosity of 55% and with two different morphologies (microporous and mesoporous). Aluminium surface capping layers with thicknesses in the range 0.1-0.5 m were applied by rf sputtering.…

Silicon Nanostructures and PhotoluminescenceNanowire Synthesis and ApplicationsSemiconductor materials and devices

Dynamics and Microstructure Formation during Nucleation of Lysozyme Solutions

Yannis Georgalis、Patrick Umbach、Dikeos Mario Soumpasis 等 4 位作者1998-05-21Journal of the American Chemical Society

The liquid−liquid coexistence region of aqueous lysozyme−NaCl solutions was examined by time-resolved small-angle static light scattering and light microscopy. At the initial stages of the reaction scattered intensities peaked at finite scattering vectors as expected for globular domains growing under the influence of…

Material Dynamics and Propertiesnanoparticles nucleation surface interactionsCrystallization and Solubility Studies

Chemisorbed Oxygen on Au(111) Produced by a Novel Route: Reaction in Condensed Films of NO2 + H2O

Wang Jiang、M. Voß、H. Busse 等 4 位作者1998-05-21The Journal of Physical Chemistry B

We report a facile, low-temperature reaction between condensed-phase NO 2 and H 2 O that leads ultimately to the formation of a large concentration (θ 0 = 0.42 monolayers) of adsorbed oxygen adatoms on a Au(111) surface. This reaction represents a novel route to generate surface oxygen on Au that can be utilized in fu…

Catalytic Processes in Materials ScienceAdvanced Chemical Physics StudiesGas Sensing Nanomaterials and Sensors

A Solvothermal Elemental Reaction To Produce Nanocrystalline ZnSe

Yadong Li、Yi Ding、Yitai Qian 等 5 位作者1998-05-21Inorganic Chemistry

A solvothermal elemental reaction to nanocrystalline zinc selenide was proposed. The coordinating ability of the solvent was found to play an important role on the nucleation and growth of the nanocrystalline ZnSe.

Chalcogenide Semiconductor Thin FilmsLaser-Ablation Synthesis of NanoparticlesQuantum Dots Synthesis And Properties

Silos

Chris Brown、Jørgen Nielsen1998-05-21OpenAlex

Bringing together the leading European expertise in behaviour and design of silos, this important new book is an essential reference source for all concerned with current problems and developments in silo technology. Silos are used in an enormous range of industries and the handling characteristics of many industrial…

Recycling and Waste Management TechniquesGraphite, nuclear technology, radiation studies