Materials Literature
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Cobalt silicate was studied as a model catalyst to seek an understanding of why Co-MCM-41 catalyst is not active for single wall carbon nanotubes (SWNT) upon treatment at high temperature. Cobalt orthosilicate was formed during high-temperature pretreatment of Co-MCM-41 (at 900 °C) in an oxidizing environment. Cobalt…
This contribution documents with light micrographs the planktonic diatom flora in seven high arctic lakes on Store Koldewey, an island off Northeast Greenland. The lakes have maximum water depths between 6.1 and 72.0 m. Basic limnological analyses indicate that all lakes are cold, monomictic, clear, oligotrophic, and…
Specimens of 304 stainless steel with various martensite contents were prepared by a low temperature (−70°C) elongation method. Optical microscopy and transmission electron micrography were used to study the phase structure of the samples. A simulated occluded cell (OC) and electrochemical impedance spectroscopy were…
Abstract Microstructural analysis reveals many important details about the qualities and capabilities of high-performance ceramics. This article explains how to prepare ceramic samples for imaging and the imaging technologies normally used. It describes sectioning, mounting, grinding, and polishing as well as ceramogr…
An overview of the properties of carbon nanotubes is presented as a function of the structural characteristics and of the method of synthesis of these novel advanced materials. Emphasis is given to the catalytic decomposition of hydrocarbons over metal-supported catalysts and also the role of the support in obtaining…
We have studied the electronic structure of oxidized and reduced CeO2(111) surfaces using x-ray photoelectron spectroscopy (XPS). The 50 nm thick CeO2(111) film was grown on a YSZ(111) substrate using oxygen plasma assisted molecular beam epitaxy (OPA-MBE). This film has been characterized using in situ (RHEED) reflec…
INTRODUCTION: Aseptic loosening is considered to be the main problem of modern endoprothesis. Tumor necrosis factor alpha (TNFalpha) seems to be the initiator protein of particle disease. The aim of our study was to investigate the TNFalpha response of macrophage like cells (MLC) after stimulation with periprosthetic…
The characteristics of annular amplitude and phase filters are compared. The behavior of two-zone phase and amplitude filters as the inner zone is increased is studied in detail. Numerical simulations show that a phase filter can achieve a superresolution effect, a circular Dammann effect, and flat-topped intensity fo…
Abstract Previous attempts to use illite as a geothermometer have failed: no general relation between the mineral's chemical composition and temperature of crystallization has been found. Here, chemical compositions of 27 illite samples from five different geothermal fields (the data on four of which were drawn from t…
We report on the bulk and surface properties of dispersions consisting of nonstoichiometric polyelectrolyte complex (PEC) nanoparticles. PEC nanoparticles were prepared by mixing poly(l-lysine) (PLL) or poly(diallyldimethylammonium chloride) (PDADMAC) with poly(maleic acid-co-alpha-methylstyrene) (PMA-MS) or poly(male…
In this study, spandexes of three degrees of fineness are used as the core material with cotton fibers as the sheath to spin fine elastomeric yarns. We observe the cross sections of the core yarns and the migration of the spandex inside the core yarn concluding that producing a finer elastomeric yarn with a uniform st…
The influence of the support ionicity on the adsorption of H, CH x ( x = 2, 3), and O on supported Pt particles is investigated using density functional theory (DFT). The DFT calculations reveal that the importance of the 6s,p states for the Pt adsorbate bonding increases in the order Pt−O < Pt−CH 2 < Pt−CH 3 < Pt−H.…
The effects of temperature, frequency, and molarity on the dielectric behaviour and ac electrical conductivity have been studied for nanosized samples of MgAl 2 O 4 prepared by chemical co-precipitation technique. X-ray powder diffraction (XRD) study shows that the particle size is 8 nm and the system is orthorhombic.…
This work presents the design and test results of a charged-particle solid-state detector with ultrafast signal response based on polycrystalline chemical-vapor-deposition (pCVD) diamond as active detector material and a high-bandwidth RF amplifier. We tested the detector at the Indiana University Cyclotron Facility B…
We present measurements of the optical spectra on Na(0.7)CoO(2) single crystals. The optical conductivity shows two broad interband transition peaks at 1.6 eV and 3.1 eV, and a weak midinfrared peak at 0.4 eV. The intraband response of conducting carriers is different from that of a simple Drude metal. A peak at low b…
An improved synchrotron microradiography technique is being used to study dendrite growth and coarsening in Sn-13%Bi alloy in real time. The morphology of growing dendrites can be well resolved with reasonable image contrast. Dendrite arm remelting, coalescence, and fragmentation have been observed in a real alloy and…
The electronic properties, redox properties, protonation, and stability of five [alpha-PTi(2)W(10)O(40)](7)(-) isomers have been investigated employing density-functional theory (DFT) method. The results reveal that the stability of [alpha-1,2-PTi(2)W(10)O(40)](7)(-) and [alpha-1,6-PTi(2)W(10)O(40)](7)(-) is weaker an…
The paper presents new findings concerning the role of microstructural variations in the localised corrosion of a magnesium alloy AZ91. The alloy with prior solution treatment (T4 condition), when subjected to aging treatments (T6 condition), developed intermetallic β phase (Mg17 Al12), which is cathodic to the alloy…
Monodispersed nanosized yttrium aluminum garnet (YAG) powder was synthesized via a mixed‐solvent thermal method using stoichiometric amounts of inorganic aluminum and yttrium salts. Pure‐phase YAG crystalline powder was obtained at low temperature (290°C) and low pressure (10 MPa). The resulting products were characte…
In this study the inhibitive behaviour of benzotriazole, 5-methyl benzotriazole, 5-chloro benzotriazole and 5-nitro benzotriazole on the corrosion of pure aluminium in 0.1M HCl has been investigated by the potentiostatic polarisation technique. For this purpose, corrosion potentials Ecorr, corrosion rates icorr, anodi…