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Microstructural and Chemical Characterisation of Metal Particles Nanostructures

Asunci oacute n Fern aacute ndez、T.C. Rojas2003-01-01MATERIALS TRANSACTIONS

In order to achieve a full characterisation of metal particles nanostructures at the microstructural level, we show in this overview the use of different techniques: i) High resolution transmission electron microscopy (TEM) or energy filtered TEM (EFTEM) associated to energy dispersive X-Ray analysis (EDX) and electro…

Gold and Silver Nanoparticles Synthesis and ApplicationsQuantum Dots Synthesis And PropertiesElectron and X-Ray Spectroscopy Techniques

Miscibility of PVC with chlorinated PE and chlorinated PVC

Jan‐Chan Huang2003-01-01International Journal of Polymeric Materials

Miscibility of PVC with chlorinated PE and chlorinated PVC was reviewed. The miscible region of chlorine content ranged from 44 wt% to 65 wt%, which was not symmetric to the chlorine content of PVC, 56.7 wt%. Two group contribution methods were used to calculate solubility parameters of polymers. The results of solubi…

Polymer Science and PVC

Heat-Treatment on Black-Passivated ZnNi Alloys

C. Müller、M. Sarret、Elisa Rubio-García2003-01-01Journal of The Electrochemical Society

Zinc-nickel alloys obtained from an alkaline bath were passivated with a black, silver-free, chromate conversion coating (CCC). The attack of the chromate solution on the coatings changed most of their characteristics. The CCC modified the composition, thickness, structure, roughness, and stress level of the alloys. S…

ZnO doping and propertiesCorrosion Behavior and InhibitionAnodic Oxide Films and Nanostructures

Thermal-hydraulic model of the helium-cooled pebble bed test blanket module for ITER FEAT

K. Kleefeldt2003-01-01Repository KITopen (Karlsruhe Institute of Technology)

Im Rahmen des Europaeischen Fusionprogrammes werden derzeit verschiedene test blanket module (TBM) entwickelt, die in ITER, dem ''International Thermonuclear Experimental Reactor'', erprobt werden sollen. Das vom Forschungszentrum Karlsruhe GmbH vorbereitete TBM spiegelt ein mit Helium gekuehltes Feststoff-Blanket (en…

Fusion materials and technologiesNuclear reactor physics and engineeringNuclear Materials and Properties

Principle and application of spark plasma sintering technology

Feng Hai2003-01-01Materials Science and Technology

The basic principles, system constituents and typical sintering technique of spark plasma sintering (SPS), a new advanced sintering technique used for materials consolidation. SPS were discussed to further study its advantages. Nanomaterials synthesis, functional gradient materials (FGMs) and high density fine grain…

Advanced ceramic materials synthesisAdvanced materials and compositesMaterials Engineering and Processing

Development of Isotropic Bonded Magnets with (BH)max of 120 kJ/m3

Shinya Sakurada、A. Tsutai、Tomohisa Arai2003-01-01Journal of the Japan Society of Powder and Powder Metallurgy

We have developed isotropic magnet powder with the composition of (Sm, Zr)(Fe, Co)zB0.1Nx (z=9-10) prepared by rapid quenching, annealing, and nitrogenation. The presence of both zirconium and cobalt make it possible to realize a nearly single phase of the TbCu7 structure with a c/a ratio as high as 0.87. These powder…

Magnetic and transport properties of perovskites and related materialsHydrogen Storage and MaterialsMagnetic Properties of Alloys

Spectroscopic properties and thermal stability of a new erbium-doped bismuth-based glass

Jianhu Yang、Dai Shi-Xun、Wen Lei 等 7 位作者2003-01-01Acta Physica Sinica

The absorption spectra,emission spectra and thermal stability of Er3+-doped (85-x)Bi2O3-(10+x)B2O3-5Na2O(x=0,5,10,15,20,25 mol%)glasses were investigated in this work.The Ωt(t=2,4,6)(Ω2=(352—386)×10-20cm2,Ω4=(138—152)×10-20cm2,Ω6=(093—117)×10-20cm2)parameters were calculated by Judd-Ofelt theory.The stimulated e…

Luminescence Properties of Advanced MaterialsGlass properties and applicationsSolid State Laser Technologies

RIETVELD REFINEMENT OF 2-THETA SPLIT RANGES - A METHOD FOR REDUCING ANALYSIS TIME

Karin Laursen、Tim W. White2003-01-01OpenAlex

This paper presents a method of reducing the X-ray diffraction data collection tim e, while maintaining high data quality, suitable for Rietveld refinement. The approach taken here is that phases in general show peak broadening as well as a loss of intensity with increasing 2-theta. Thus, by splitting the full analyze…

Cultural Heritage Materials AnalysisX-ray Spectroscopy and Fluorescence AnalysisX-ray Diffraction in Crystallography

The biodegradation of poly-b-(hydroxybutyrate), poly-b-(hydroxybutyrate-co-b-valerate) and poly(e-caprolactone) in compost derived from municipal solid waste

Laboratrio de Pol、Rodovia D. Pedro2003-01-01OpenAlex

Understanding the behavior of polymeric materials, particularly their biodegradation, is fundamental for solving problems in the management of environmental residues. In this work, we used a monitoring system based on an aerobic biodegradation technique known as the Sturm test to investigate the biodegradation of poly…

biodegradable polymer synthesis and propertiesElectrospun Nanofibers in Biomedical ApplicationsMicroplastics and Plastic Pollution

Seeded Batch Cooling Crystallization of Adipic Acid from Ethanol Solution

Norihito Doki、Masaaki Yokota、Hiroaki Nakamura 等 5 位作者2003-01-01JOURNAL OF CHEMICAL ENGINEERING OF JAPAN

Adipic acid was crystallized by cooling in a batch crystallizer. At low seed loadings, the product crystal size distribution (CSD) was bi-modal because of enormous secondary nucleation. However, at high seed loadings, it became uni-modal, where the crystallization was dominated by seed growth with practically no secon…

Fermentation and Sensory AnalysisCrystallization and Solubility StudiesFood Chemistry and Fat Analysis

Chemical Reaction between Tantalum and Gallium under High Pressure

Yasuo Fujinaga、Yoshihiro Murakami2003-01-01MATERIALS TRANSACTIONS

Tantalum in contact with gallium is compressed up to 7 GPa and heated. When the temperature keeps above 50°C of the melting temperature of gallium, the lattice constant of tantalum is approximately constant. The lattice expansion begins to increase with raising the temperature from above 300°C. The expansion becomes a…

Metal and Thin Film MechanicsIntermetallics and Advanced Alloy PropertiesMetallurgical and Alloy Processes

Evaluation of corrosion resistance of two engineering alloys in molten salts by electrochemical techniques

A. Martínez‐Villafañe、Facundo Almeraya-Calderón、Citlalli Gaona-Tiburcio 等 5 位作者2003-01-01Materials and Corrosion

Abstract The electrochemical behaviour of two steels typically used in power boilers has been studied in the temperature range from 540°C to 680°C. Two environments were used: a) a synthetic salt mixture of 80% V 2 O 5 − 20% Na 2 SO 4 and b) oil ash collected from a high temperature reheater. Corrosion rates obtained…

Corrosion Behavior and InhibitionHydrogen embrittlement and corrosion behaviors in metalsMetallurgical Processes and Thermodynamics

Production of Crystalline Boric Acid through the Reaction of Colemanite Particles with Propionic Acid

Bahman ZareNezhad2003-01-01Developments in Chemical Engineering and Mineral Processing

Abstract A new process for boric acid production is developed. In this process the crystalline boric acid particles are directly produced in a one‐stage crystallizer through the reaction of colemanite particles with propionic acid. Each porous colemanite particle is comprised of spherical solid grains. It is found tha…

Zeolite Catalysis and SynthesisMesoporous Materials and CatalysisClay minerals and soil interactions

Influence of Shot Peening on Surface Durability of Plasma Case-Hardened Sintered Powder Metal Gears

Akira Yoshida、Yuji OHUE、Masanori SEKI2003-01-01OpenAlex

In order to investigate the influence of shot peening on the surface durability of sintered powder metal gears, the plasma case-hardened sintered powder metal rollers and gears shotpeened with different condition were fatigue-tested under a sliding-rolling contact condition. The hardness, the compressive residual stre…

Metal and Thin Film MechanicsTribology and Lubrication EngineeringMetal Alloys Wear and Properties

Surface Treatments for Lyotropic Liquid Crystals Alignment

Ivan H. Bechtold、Maria Letícia Vega、E. A. Oliveira 等 4 位作者2003-01-01Molecular Crystals and Liquid Crystals

For nematic lyotropic liquid crystals it has been experimentally observed that in nontreated glass cells the director in the surface layer can be reoriented by a magnetic field in any direction parallel to the surface, and the final state is stable. In this paper we will focus on the equilibrium configuration of the d…

Liquid Crystal Research AdvancementsTheoretical and Computational PhysicsAdvanced Thermodynamics and Statistical Mechanics

Effects of the Type of Alcoholic Solvent on the Formation of SiO2 Wet Gels in Sol-Gel Process.

Morinao FUKUOKA、Akio Makishima2003-01-01Journal of the Ceramic Society of Japan

The effect of the type of alcoholic solvent on the formation of SiO2 gels in the sol-gel process has been studied by observing the gelation time in a tightly closed system. A large difference in the rate of gelation was found among fifteen kinds of alcohols used as the solvent. The gelation time decreased with increas…

Gas Sensing Nanomaterials and SensorsMesoporous Materials and CatalysisAnalytical Chemistry and Sensors

THERMAL PLASMA DESTRUCTION OF OZONE-DEPLETING SUBSTANCES: TECHNOLOGIES AND CHEMICAL EQUILIBRIUM, CHEMICAL KINETIC AND FLUID DYNAMIC MODELLING

Anthony B. Murphy2003-01-01High Temperature Material Processes An International Quarterly of High-Technology Plasma Processes

Plasma technologies for the destruction of ozone-depleting substances are reviewed. Particular attention is paid to the PLASCON process, based on an argon plasma produced by a dc plasma torch, which is used to destroy halons and chlorofluorocarbons in Australia and the UK. Three different approaches to modelling the d…

Catalytic Processes in Materials ScienceIndustrial Gas Emission Control

Hybrid ceramic-polymer coating used to protect metallic surfaces against corrosion

Miriam Estévez、S. Vargas、V. M. Castaño 等 5 位作者2003-01-01International Journal of Polymeric Materials

A new hybrid ceramic-polymer coating was designed to provide a chemical barrier to protect metallic substrates against corrosion. This material is completely hydrophobic, protecting the coated surface from chemical attack from its environment. A good adhesion between the organic and inorganic phases was achieved, prod…

Corrosion Behavior and InhibitionSilicone and Siloxane ChemistryMaterial Properties and Applications