Materials Literature
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The preparation and properties of silver tripolyphosphate have been investigated. It has been found that silver tripolyphosphate dihydrate decomposes on heating, first into anhydrous silver tripolyphosphate forms I and II, and subsequently into crystalline silver pyrophosphate together with a glass containing ortho-,…
Three broad types of natural graphites are recognized: flake, vein, and amorphous. The compaction of graphite powders, representing these types, into coherent binderless artifacts at room temperature and pressures up to 125, 000 psi has been studied. The graphite powders were characterized as to their particle size di…
The chemical structures of the color reaction products (Ib and Ic) obtained from butyl-and p-tolyl-urea with diacetyl monoxime and glucuronolactone in phosphoric acid were elucidated by their physical properties. Ib develops immediately a red color in phosphoric acid and is thought to be one of the main reaction produ…
Tests are described on the adhesive strength of gold films deposited on glass substrate under tensile loads. Through a flat-topped rivet fixed by an adhesive onto the film the force to pull the film was transmitted normally to the substrate surface. This force was measured by a spring balance at two increasing rates o…
Magnesium ammonium phosphate hexahydrate MgNH4PO4,6H2O and magnesium hydrogen phosphate trihydrate MgHPO4,3H2O have been heated to temperatures up to 1220° and X-ray powder photographs taken of the products. Both substances decompose during the process and gradually change first into an amorphous phase and then into c…
Résultats de spectrométrie α pour 224Ac 27 raies, 223Ac 25 raies, 220Fr 15 raies, 219Fr 6 raies.
L'afghanite, nouvel alumino˗silicate de sodium, calcium et potassium, a été découverte dans la mine de lapis-lazuli de Sar-e-Sang, Badakhshan, Afghanistan. Hexagonale avec a = 12,77, c = 21,35 Å, V = 3015 ų, les groupes de symétrie possible étant P6₃/mmc, P6₃mc ou P[-6]2c. Z = 3 (Na,Ca,K)₁₂ (Si, Al)₁₆ O₃₄ (Cl, SO₄, C…
The electroreduction of 1,8-diaroylnaphthalenes, 2,2′-diaroylbiphenyls, and αω-diaroyl-propanes, -butanes, and -pentanes with 4-hydroxy- and 4-methoxy-substituents on the aryl group has been examined. Cyclic glycols are formed, together with other products, except in the case of the αω-diaroylpentanes which give linea…
Pure titanium metal was electrodeposited on a cathode by double fused salt electrolysis with the cell designed specifically for this work. Electrolysis was carried out in NaCl, NaCl-TiCl2-TiCl3 and NaCl-K2TiFx baths. The anode materials for the first stage electrolysis were Ti-C-O alloys or TiC prepared by carbon redu…
Nine carbon and low alloy cast steels cast in panel form, some machined and others unmachined, were exposed in marine and industrial atmospheres for periods of one-, three-, seven-, and 12-years and recorded as to weight loss information. The weight loss was converted to corrosion rate in terms of inches penetration p…
The dependence of the spherical aberration coefficient C s on object position z 0 and magnification M is studied using Glaser's bell-shaped field model. It is shown that C s may be written in the forms IMG1 where a i and b i are functions of the lens excitation k 2 . a i and b i are tabulated for a range of values of…
Stress relaxation at constant strains has been studied in crystals of copper and α-brasses containing 10, 20, or 30 at.-% zinc at 77,200, and 291° K after consecutive small plastic deformations. Close to the yield point the relaxation was generally within 1% of the applied stress, but at large deformations, notably wi…
Distributional results in the lower tail, and further percentage points in both tails, are given for the statistic WN2, or NωN2, used in testing for goodness of fit.
The complete structure of cubic hydroxystannates, CaSn (OH)₆ and ZnSn(OH)₆, of space group Pn₃, has been determined by neutron diffraction at 4° K (powder techniques), and with the study of the spectrum of CaSn (OD)₅,₄₅ (OH)₀,₅₅. The 24 hydrogen atoms of the unit cell form two sorts of hydrogen bonds with double well-…
18α-Olean-12-ene, which is in acid-catalysed equilibrium with olean-13(18)-ene (δ-amyrene), has been converted in several steps into olean-12-ene (β-amyrene). Transformation of this hydrocarbon into its 11α-hydroxyderivative and photolysis of the nitrite of the latter gave 11α-hydroxy-1-oximino-olean-12-ene. This oxim…
Thirty two tufted carpets, representing variations in fiber content, pile weight, and cut and loop-pile construction were studied for stress-strain behavior under cyclic loading to 12 lb/in. 2 on an Instron tensile tester. Results are presented conventionally in terms of compression, recovery, matting, and resilience.…
Abstract By measurement of peak areas in the dioxymethylene region of high‐resolution NMR spectra of partly formalized poly(vinyl alcohol), PVA, the relationship between tacticity of PVA, rate of formalization reaction, and stereochemical configuration of poly(vinyl formal) was studied. Formation of cis ‐formal at an…
Abstract The results of a study to characterize samples of single crystals of TlSe grown by the Bridgman‐Stockbarger and zone recrystallization techniques are given. The X‐ray diffraction patterns were indexed as a tetragonal lattice whose parameters were a = 8.02 Å and c = 7.00 Å. The absorption and transmission meas…
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTBase-catalyzed decomposition of peroxypivalic acid in aqueous solutionEdward Koubek and J. E. WelschCite this: J. Org. Chem. 1968, 33, 1, 445–446Publication Date (Print):January 1, 1968Publication History Published online1 May 2002Published inissue 1 January 1968https://pubs…
Abstract not Available.