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Free energy of adsorption of water and calcium on the {10 1? 4} calcite surfaceElectronic supplementary information (ESI) available: free energy calculations. See http://www.rsc.org/suppdata/cc/b3/b311928a/

Sébastien Kerisit、Stephen C. Parker2003-12-19Chemical Communications

Molecular dynamics simulations of the calcite-water interface have shown that the free energy of adsorption of water is relatively small compared to the previously calculated enthalpy of adsorption implying a large entropy change and that the free energy profile of a calcium adsorbing on the surface correlates with th…

Calcium Carbonate Crystallization and InhibitionMinerals Flotation and Separation TechniquesCrystallization and Solubility Studies

Assembly of Nanoparticles using Surface‐Grafted Orthogonal Polymer Gradients

Rajendra R. Bhat、M. Tomlinson、Jan Genzer2003-12-19Macromolecular Rapid Communications

Abstract Summary: We report on preparing poly(2‐(dimethylamino)ethyl methacrylate) (PDMAEMA) gradient substrate, wherein molecular weight (MW) and grafting density ( σ ) of the surface‐anchored PDMAEMA chains vary continuously in two orthogonal directions. Such a specimen is used to control the assembly of charged gol…

Nanoparticle-Based Drug DeliveryGold and Silver Nanoparticles Synthesis and ApplicationsPolymer Surface Interaction Studies

Synthesis and characterization of large-pore vinyl-functionalized mesoporous silica SBA-15

Yanqin Wang、Bodo Zibrowius、Chia‐Min Yang 等 5 位作者2003-12-19Chemical Communications

Ordered mesoporous silicas SBA-15 with high loadings of pendant vinyl groups have been synthesized via co-condensation of tetraethoxysilane (TEOS) and triethoxyvinylsilane (TEVS) templated with a triblock copolymer.

Catalytic Processes in Materials ScienceMesoporous Materials and CatalysisPolyoxometalates: Synthesis and Applications

Synthesis and Spectroscopic and Electrochemical Studies of Novel Benzo‐ or 2,3‐Naphtho‐Fused Tetraazachlorins, Bacteriochlorins, and Isobacteriochlorins

Takamitsu Fukuda、Е. А. Макарова、E. A. LUK'YANETS 等 4 位作者2003-12-19Chemistry - A European Journal

Benzene- or 2,3-naphthalene-ring-expanded tetraazachlorins (TACs), tetraazabacteriochlorins (TABCs), and tetraazaisobacteriochlorins (TAiBCs) have been synthesized by using tetramethylsuccinonitrile as a source of hydrogenated sites. The derived compounds were characterized by using NMR spectroscopy, X-ray crystallogr…

Photosynthetic Processes and MechanismsPorphyrin and Phthalocyanine ChemistryPhotodynamic Therapy Research Studies

Synthesis of poly(para-phenylenevinylene) rotaxanes by aqueous Suzuki couplingElectronic supplementary information (ESI) available: details of analytical ultracentrifuge measurements; experimental synthetic procedures. See http://www.rsc.org/suppdata/cc/b3/b311762f/

Jun Terao、Andrew Tang、Jasper J. Michels 等 5 位作者2003-12-19Chemical Communications

PPV-based polyrotaxanes have been prepared by coupling vinyl boronic acids to aryl iodides in the presence of cyclodextrins, and the crystal structure of a [2]rotaxane of this type has been determined.

Supramolecular Chemistry and ComplexesPorphyrin and Phthalocyanine ChemistryLuminescence and Fluorescent Materials

Evolution of the microstructure during annealing of porous silicon multilayers

N. Ott、M. Nerding、G. Müller 等 5 位作者2003-12-19Journal of Applied Physics

We investigate the structural changes in porous silicon multilayers during annealing. Porous silicon multilayers play an important role in layer transfer technologies, where a thin crystalline silicon layer is separated from a wafer and transferred to a foreign substrate. High processing temperatures during epitaxial…

Silicon and Solar Cell TechnologiesSilicon Nanostructures and PhotoluminescenceNanowire Synthesis and Applications

48-Channel electron detector for photoemission spectroscopy and microscopy

Luca Gregoratti、A. Barinov、E. Benfatto 等 11 位作者2003-12-19Review of Scientific Instruments

We show that it is possible to use a multichannel electron detector in a zone plate based photoemission spectromicroscopy in a snap shot mode to reduce the total acquisition time for a given counting time by 50% relative to the standard scanning mode while preserving the feature of the spectra. We describe the result…

Advancements in Photolithography TechniquesX-ray Spectroscopy and Fluorescence AnalysisElectron and X-Ray Spectroscopy Techniques

Bioinspiriertes Molekulardesign von lichtsammelnden Multiporphyrinsystemen

Myung‐Seok Choi、Tomoko Yamazaki、Iwao Yamazaki 等 4 位作者2003-12-19Angewandte Chemie

Abstract Jüngste Fortschritte bei Grundlagenstudien zu Multiporphyrinsystemen geben Aufschluss über die maßgeblichen Strukturparameter für das Molekulardesign von künstlichen Lichtsammelantennen, die die radähnlichen Antennenkomplexe photosynthetischer Purpurbakterien imitieren. “Kovalente” und “nichtkovalente” Ansätz…

Photosynthetic Processes and MechanismsSupramolecular Chemistry and ComplexesPorphyrin and Phthalocyanine Chemistry

A Unique Binaphthyl Strapped Iron–Porphyrin Catalyst for the Enantioselective Epoxidation of Terminal Olefins

Éric Rose、Qizhi Ren、Bruno Andrioletti2003-12-19Chemistry - A European Journal

A new chiral binaphthyl-strapped iron-porphyrin 4 b that exhibits unprecedented catalytic activity toward the enantioselective epoxidation of terminal olefins was synthesized. Typical enantiomeric excesses (ee) of 90 % were measured with a maximum of 97 % for the epoxidation of styrene, whereas the turnover numbers (T…

Porphyrin and Phthalocyanine ChemistryMetalloenzymes and iron-sulfur proteinsMetal-Catalyzed Oxygenation Mechanisms

Influence of Nafion Content in Electrodes on Performance of Carbon Supercapacitors

Francesco Lufrano、P. Staiti、Maurizio Minutoli2003-12-19Journal of The Electrochemical Society

The effects of Nafion loading in electrodes on the performance of supercapacitors have been investigated in this work. Electrodes based on carbon material were prepared with Nafion loading varying from 10 to 50 wt %, and the optimal loading was investigated by electrochemical impedance spectroscopy. The capacitors wit…

Supercapacitor Materials and FabricationFuel Cells and Related MaterialsAdvanced battery technologies research

Grain Boundary Space Charge Effect in Zirconia

Xin Guo、Yong Ding2003-12-19Journal of The Electrochemical Society

According to the space charge concept, oxygen vacancies are depleted in the grain boundary space charge layers of acceptor-doped whereas electrons are expected to accumulate in the space charge layers if present, leading to significant changes in the grain boundary electrical properties. In this work, electrons were i…

Advancements in Solid Oxide Fuel CellsSemiconductor materials and devicesElectronic and Structural Properties of Oxides

Nanostructural zinc oxide and its electrical and optical properties

Chunxiang Xu、Xiao Wei Sun、B. J. Chen 等 6 位作者2003-12-19Journal of Applied Physics

Nanostructural zinc oxide fibers have been fabricated by a simple vapor transport method of heating the mixture of zinc oxide, gallium oxide, and carbon powders in air. The zinc oxide nanofibers showed cauliflower-like, disordered, vertically and horizontally aligned morphologies in different temperature regions. The…

ZnO doping and propertiesGas Sensing Nanomaterials and SensorsGa2O3 and related materials

Heteroepitaxial growth behavior of Mn-doped ZnO thin films on Al2O3 (0001) by pulsed laser deposition

Sang Sub Kim、Jongun Moon、Byung‐Teak Lee 等 5 位作者2003-12-19Journal of Applied Physics

Heteroepitaxial growth behavior of Mn-doped ZnO thin films (Zn1−xMnxO) on Al2O3 (0001) substrates by pulsed laser deposition was investigated particularly as a function of Mn content (0.00⩽x⩽0.35) using synchrotron x-ray scattering and atomic force microscopy. The undoped ZnO film was grown epitaxially with a 30° rota…

ZnO doping and propertiesCopper-based nanomaterials and applicationsGa2O3 and related materials

Characterization of Oxide Films Formed on Mg-Based WE43 Alloy Using AC/DC Anodization in Silicate Solutions

Viola Birss、Shen Xia、R. Yue 等 4 位作者2003-12-19Journal of The Electrochemical Society

The characteristics of the oxide film formed on a Mg-based WE43 alloy using ac/dc anodization techniques in an alkaline silicate solution have been investigated using scanning electron microscopy and Rutherford back-scattering spectroscopy, and the corrosion resistance of these films has been determined using the ac i…

Corrosion Behavior and InhibitionConcrete Corrosion and DurabilityAnodic Oxide Films and Nanostructures

Stress effects in sol-gel derived ferroelectric thin films

L. Lian、N. R. Sottos2003-12-19Journal of Applied Physics

Residual stress development during processing of sol-gel derived ferroelectric thin films influences electromechanical properties and performance. The present work investigates the effects of stress on field-induced polarization switching in ferroelectric Pb(Zr0.52Ti0.48)O3 (PZT) (52/48) thin films. Film response is m…

Ferroelectric and Piezoelectric MaterialsAcoustic Wave Resonator TechnologiesDielectric materials and actuators

Combinatorial Electrochemical Synthesis and Screening of Mesoporous ZnO for Photocatalysis

Thomas F. Jaramillo、Sung‐Hyeon Baeck、Alan Kleiman‐Shwarsctein 等 4 位作者2003-12-19Macromolecular Rapid Communications

Abstract Summary: Automated electrochemical synthesis was used to create combinatorial libraries of mesoporous materials using tri‐block copolymers as structure directing agents (SDA). An example library of 56 ZnO samples was synthesized, varying concentrations (0–15 wt.‐%) of poly(ethylene oxide)‐block‐poly(propylene…

Advanced Photocatalysis TechniquesMesoporous Materials and CatalysisPolyoxometalates: Synthesis and Applications

Stacking of Molecules Possessing a Fullerene Apex and a Cup-Shaped Cavity Connected by a Silicon Connection

Yutaka Matsuo、Ayako Muramatsu、Ryo Hamasaki 等 6 位作者2003-12-19Journal of the American Chemical Society

Hexagonal or tetragonal packing of columnar stacks in crystals and liquid crystals has been observed for a series of molecules possessing a fullerene apex and an aromatic cone that are connected with a Si-C connection. The columnar stacking of the new shuttlecock molecules is constitutionally stable but conformational…

Carbon Nanotubes in CompositesGraphene research and applicationsFullerene Chemistry and Applications

Continuous synthesis of CdSe–ZnS composite nanoparticles in a microfluidic reactor

Hongzhi Wang、Xianying Li、Masato Uehara 等 8 位作者2003-12-19Chemical Communications

ZnS-coated CdSe composite particles have been continuously synthesized in a microfluidic reactor. By using this system, CdSe particles and a ZnS coating can be produced in sequence, and the particle size and layer thickness can be directly adjusted by the residence time. It demonstrated that the continuous synthesis i…

Gold and Silver Nanoparticles Synthesis and ApplicationsQuantum Dots Synthesis And PropertiesInnovative Microfluidic and Catalytic Techniques Innovation

A Chiroptical Molecular Switch with Distinct Chiral and Photochromic Entities and Its Application in Optical Switching of a Cholesteric Liquid Crystal

Richard A. van Delden、Tommaso Mecca、Carlo Rosini 等 4 位作者2003-12-19Chemistry - A European Journal

Two new structurally related photoswitches are described, in which azobenzene photochromism is combined with the chirality of a 2,2'-dihydroxy-1,1'-binaphthyl unit. In system 1 the chiral binaphthyl moiety is bridged by a methylene tether, locking the biaryl chirality while in system 2 the biaryl core is unbridged and…

Porphyrin and Phthalocyanine ChemistryPhotochromic and Fluorescence ChemistryMolecular spectroscopy and chirality

Monolithic Integration of Carbon Nanotube Devices with Silicon MOS Technology

Yu‐Chih Tseng、Peiqi Xuan、Ali Javey 等 7 位作者2003-12-19Nano Letters

An integrated circuit combining single-walled carbon nanotube (SWNT) devices with n-channel metal oxide semiconductor (NMOS) field effect transistors was fabricated. SWNTs were grown, using chemical vapor deposition, from catalyst islands located on an NMOS decoder circuit. Massive arrays of nanotube devices, each add…

Carbon Nanotubes in CompositesMechanical and Optical ResonatorsNanotechnology research and applications