Materials Literature
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We have performed numerical calculations to study the generation of arbitrary temperature profiles with high spatial resolution on the surface of a solid. The characteristics of steady-state distributions and time-dependent heating and cooling cycles are examined, as well as their dependence on material properties and…
Electrochemical potentiodynamic polarizations, electrochemical corrosion potential (ECP) measurements and slow strain rate tensile (SSRT) tests were conducted to investigate the intergranular stress corrosion cracking (IGSCC) characteristics of Type 304 stainless steels treated with inhibitive chemicals in simulated b…
Pt/SiO 2 nanosized particles have been synthesized using a reverse micelle technique combined with metal alkoxide hydrolysis and condensation. The size of the particles and the thickness of the coating can be controlled by manipulating the relative rates of the hydrolysis and condensation reactions of tetraethoxysilan…
Arsenic pentachloride has a trigonal bipyramidal structure in the solid state with As-Cleq = 210.6, 211.9 pm, As-Clax= 220.7 pm, space group Pmmn, a = 706.2 (1); b = 760.3 (2), c = 623.3 (1) pm. Antimony pentachloride exists in two modifications: above −54.1 °C it is also trigonal bipyramidal with Sb-Cleq = 227.0 and…
The goals of the Storage and Delivery System (SDS) of the ITER Tritium Fuel Processing Plant are 1) safe storage of tritium-deuterium (DT) mixtures in reservoirs and in metal tritide beds with in-bed accountancy, 2) supply of various DT mixtures with DT and T2 flow rates up to 200 and 100 Pam3s−1 and of pure gases (He…
Thermal-responsive shape-memory polyurethane consists of two phases, a thermally reversible phase for maintaining a transient shape and fixed phase structure for recovering the original shape. The use of shape memory polyurethane in clothing is a novel concept. The aim of this paper is to introduce the application of…
Abstract A bonding model, valid for alimited group of borates, is formulated which allows the ratio of triangularly to tetrahedrally coordinated B atoms to be calculated from the chemical formula. The anion complex, which is formed by covalently bound atoms, has non-directed ionic bonds with the surrounding cations. T…
The first experimental investigation of a normal-incidence Mo-Y multilayer-coated diffraction grating operating at a 9-nm wavelength is reported. The substrate is a replica of a concave holographic ion-etched blazed grating with 2,400 grooves/mm and a 2-m radius of curvature. The measured peak efficiency in the -3 ord…
Single‐phase glasses containing 37.5 mol% Y 2 O 3 , 7 mol% La 2 O 3 , and 1 mol% Pr, Ho, Nd, Er, Sm, Tm, Eu, or Yb oxide substituted for part of the Y 2 O 3 were synthesized by containerless melting. The spectral transmission and absorption cross sections of the glasses were determined at wavelengths from 360 to 3300…
The synthesis and liquid crystalline properties of a new series of amides (series 2a-f,3a-d and 4a-d) incorporating pyridine and 1,3,4-thiadiazole rings are reported. No homologues of the series 2 show mesomorphic properties. In the series 3 only the highest homologues (3d) displays an enantiotropic SmA mesophase; the…
Corrosion of mild steel under aerobic conditions in the presence of a monoculture of aerobic bacteria (Pseudomonas fragi K [P. fragi K]) has been studied in a continuous flow system using electrochemical impedance spectroscopy (EIS). P. fragi K grown in Luria-Bertani (LB) medium causes a 10- to 20-fold decrease in the…
A series of peroxy oligomers has been synthesized on the basis of pyromellitic dianhydride and tetrachloroanhydride of pyromellitic acid by condensation with polyethylene glycols and tert-butylhydroperoxide. The resulting oligoesters contain two types of functional groups: carboxylic—which can participate in ionic rea…
The chemical exfoliation characteristics of phlogopite samples taken from Sivas - Yıldızeli-Karakoç (Turkey) ore were investigated. H2SO4, HCl, HNO3, H3PO4 and H2O2 solutions at varying concentrations were tested for chemical exfoliation and the best reagent for this purpose was determined to be hydrogen peroxide. In…
The role of liquid phase in the enhancement of the PTCR (positive temperature coefficient of resistance) effect in (Ba 0.7 Sr 0.3 )TiO 3 (BST) with the addition of AST (4Al 2 O 3 · 9SiO 2 · 3TiO 2 ) is investigated in this paper. The AST–BST samples were characterized with optical microscopy, transmission electron mic…
The thermal conductivity, thermal expansion, mechanical properties at low strain rates and dynamic mechanical properties of a collection of crosslinked closed cell polyethylene foams manufactured by a high pressure nitrogen solution process have been studied as a function of the cell size. The main mechanisms that inf…
The project consisted of two phases. In the Phase I study, the relative corrosiveness of the two salts [magnesium chloride (MgCl2) and sodium chloride (NaCl)] were examined by SAE J2334 test and ASTM B117 test. In the Phase II study, SAE J2334 test and NACE TM-01-69 test (as modified by the Pacific North States) were…
The crystal structure of the title complex, [Cd(tsac)2(py)3], has been determined by single crystal X-ray diffractometry. It crystallizes in the monoclinic space group C2/c with Z = 8.The Cd 2+ cation is at the center of a square- bipyramidal environment, equatorially coordinated to two thiosaccharinate anions through…
Gallium oxide films 20 Å in thickness were deposited onto GaAs substrates in ultra high vacuum (UHV) via e-beam evaporation from a monolithic high-purity source. The substrates were prepared by molecular-beam epitaxy and transferred to the oxide film deposition site in a wholly UHV environment. The Ga2O3−x films were…
Abstract Conventional sulfur-cured, gum natural rubber vulcanizates of various crosslink densities were prepared. Dumbbell test pieces with and without edge precuts were tested in uniaxial tension. Relative strengths of the different vulcanizates depended on cut size. Lightly crosslinked specimens exhibited an abrupt…
Because of the diversity of their compositions and structures, and the treatments needed to render them active, heterogeneous catalysts present a major challenge in structural characterisation. Electron microscopy provides textural and structural information at the scale of the individual particle. We have been able t…