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Silsesquioxanes Derived from the Bulk Polycondensation of [3-(Methacryloxy)propyl]trimethoxysilane with Concentrated Formic Acid: Evolution of Molar Mass Distributions and Fraction of Intramolecular Cycles

Patricia Eisenberg、Rosa Erra‐Balsells、Yoko Ishikawa 等 6 位作者2002-01-16Macromolecules

The polycondensation of [3-(methacryloxy)propyl]trimethoxysilane was performed in bulk, using 98 wt % formic acid (molar ratio HCOOH/Si = 3 or 6), at 50 or 70 °C, for periods of time of up to 1 month. The resulting silsesquioxanes (SSOs) were characterized by 1 H NMR, FTIR, SEC, UV−MALDI−TOF MS (linear, reflector, and…

Silicone and Siloxane ChemistrySynthesis and properties of polymersAdvanced ceramic materials synthesis

Optical simulations of electron diffraction by carbon nanotubes

A. A. Lucas、F. Moreau、Ph. Lambin2002-01-16Reviews of Modern Physics

This colloquium discusses the atomic structure of carbon nanotubes as deduced from high-resolution electron microscopy and electron diffraction in transmission through a single nanotube. The principal features of the observed micrographs are interpreted in terms of the cylindrical, chiral geometry of the atomic distri…

Graphene research and applicationsFullerene Chemistry and ApplicationsCarbon Nanotubes in Composites

Structural and Optical Properties of NdAlO3 Nanocrystals Embedded in an Al2O3 Matrix

Sanjay Mathur、Michael Veith、Hao Shen 等 5 位作者2002-01-16Chemistry of Materials

Fabrication of an oxide−oxide nanocomposite, containing a homogeneous dispersion of NdAlO 3 nanocrystals in an Al 2 O 3 matrix, is achieved by employing a single molecular compound, [NdAl 3 (OPr i ) 12 (Pr i OH)], in the sol−gel process. X-ray diffraction patterns of the composite material show NdAlO 3 to be the only…

Luminescence Properties of Advanced MaterialsNuclear materials and radiation effectsGlass properties and applications

Kinetics of Gas Discharging in a Glass of Champagne: The Role of Nucleation Sites

Gérard Liger‐Belair、P. M. Adler、Cédric Voisin 等 5 位作者2002-01-16Langmuir

In this study, bubble production in a glass of champagne was used as a common tool to illustrate and better understand the nonclassical heterogeneous bubble nucleation from pre-existing gas cavities, referred as type IV nucleation in a recent review article (Jones et al. Adv. Colloid Interface Sci . 1999, 80, 27−50).…

nanoparticles nucleation surface interactionsPickering emulsions and particle stabilizationMinerals Flotation and Separation Techniques

Ultrafast Optical Switching from an Ionic to a Neutral State in Tetrathiafulvalene-p-Chloranil (TTF-CA) Observed in Femtosecond Reflection Spectroscopy

S. Iwai、Shōji Tanaka、K. Fujinuma 等 6 位作者2002-01-16Physical Review Letters

Ultrafast optical switching from an ionic ( I) to a neutral ( N) state in TTF-CA was observed in femtosecond reflection spectroscopy. Charge transfer excitation in the I phase produces N donor ( D0) acceptor ( A0) strings within 2 ps. These initial N states decay with a lifetime of 300 ps at 4 K, but rather multiply l…

Organic and Molecular Conductors ResearchElectron Spin Resonance StudiesMagnetism in coordination complexes

Geometric Approach to the Dynamic Glass Transition

Tomás S. Grigera、Andrea Cavagna、Irene Giardina 等 4 位作者2002-01-16Physical Review Letters

We numerically study the potential energy landscape of a fragile glassy system and find that the dynamic crossover corresponding to the glass transition is actually the effect of an underlying geometric transition caused by the vanishing of the instability index of saddle points of the potential energy. Furthermore, w…

Material Dynamics and PropertiesGlass properties and applicationsTheoretical and Computational Physics

Fundamentals of Carrier Transport, 2nd edn

Mark Lundstrom2002-01-16Measurement Science and Technology

This book presents an introduction to the theory of electronic transport in the solid state. The author starts with a reminder of the quantum theory of condensed matter and then concentrates on carrier transport itself. A wide range of subtopics is touched upon in different chapters, e.g. transport in bulk samples and…

Electron and X-Ray Spectroscopy TechniquesAdvanced Physical and Chemical Molecular Interactions

Reaction Mechanism Studies on Titanium Isopropoxide–Water Atomic Layer Deposition Process

Antti Rahtu、Mikko Ritala2002-01-16Chemical Vapor Deposition

Reaction mechanisms between titanium isopropoxide and deuterated water in the atomic layer deposition (ALD) of TiO2 at 150–350 °C were studied using a quartz crystal microbalance (QCM) and a quadrupole mass spectrometer (QMS). The temperature had no marked effect on the total amount of the main gaseous by-product (CH3…

Semiconductor materials and devicesCatalytic Processes in Materials ScienceElectronic and Structural Properties of Oxides

A Strategic Two-Stage Low-Temperature Thermal Processing Leading to Fully Dense and Fine-Grained Doped-ZnO Varistors

P. Durän、F. Capel、J. Tartaj 等 4 位作者2002-01-16Advanced Materials

Fully dense doped-ZnO varistors with sub- micrometer grain size (see Figure for a TEM image) can be fabricated by a strategic two-stage, one-cycle, thermal processing method at temperatures as low as 825 °C. The nonlinear coefficients α of such fully dense varistors are as high as 270, which is more than one order of…

Thin-Film Transistor TechnologiesTransition Metal Oxide NanomaterialsZnO doping and properties

Electromigration-Induced Propagation of Nonlinear Surface Waves

R. Mark Bradley2002-01-16arXiv

Due to the effects of surface electromigration, waves can propagate over the free surface of a current-carrying metallic or semiconducting film of thickness h_0. In this paper, waves of finite amplitude, and slow modulations of these waves, are studied. Periodic wave trains of finite amplitude are found, as well as th…

Materials Sciencenlin.PS

Nonlinear transmission and light localization in photonic crystal waveguides

Sergei F. Mingaleev、Yuri S. Kivshar2002-01-16arXiv

We study the light transmission in two-dimensional photonic crystal waveguides with embedded nonlinear defects. First, we derive the effective discrete equations with long-range interaction for describing the waveguide modes, and demonstrate that they provide a highly accurate generalization of the familiar tight-bind…

cond-mat.dis-nnMaterials Science

Advanced memory effects in the aging of a polymer glass

L. Bellon、S. Ciliberto、C. Laroche2002-01-16arXiv

A new kind of memory effect on low frequency dielectric measurements on plexiglass (PMMA) is described. These measurements show that cooling and heating the sample at constant rate give an hysteretic dependence on temperature of the dielectric constant $ε$. A temporary stop of cooling produces a downward relaxation of…

Materials Sciencecond-mat.stat-mech

Spiral cracks in drying precipitates

Z. Neda、K. -t. Leung、L. Jozsa 等 4 位作者2002-01-16arXiv

We investigate the formation of spiral crack patterns during the desiccation of thin layers of precipitates in contact with a substrate. This symmetry-breaking fracturing mode is found to arise naturally not from torsion forces, but from a propagating stress front induced by the fold-up of the fragments. We model thei…

Materials ScienceSoft Condensed Matter

A Model for Granular Texture with Steric Exclusion

H. Troadec、F. Radjai、S. Roux 等 4 位作者2002-01-16arXiv

We propose a new method to characterize the geometrical texture of a granular packing at the particle scale including the steric hindrance effect. This method is based on the assumption of a maximum disorder (entropy) compatible both with strain-induced anisotropy of the contact network and steric exclusions. We show…

Materials Science

Nonuniqueness and derivative discontinuities in density-functional theories for current-carrying and superconducting systems

K. Capelle、G. Vignale2002-01-16arXiv

Current-carrying and superconducting systems can be treated within density-functional theory if suitable additional density variables (the current density and the superconducting order parameter, respectively) are included in the density-functional formalism. Here we show that the corresponding conjugate potentials (v…

Materials ScienceSuperconductivityStrongly Correlated Electrons

Vibrational properties of amorphous silicon from tight-binding O(N) calculation

Parthapratim Biswas2002-01-16arXiv

We present an O(N) algorithm to study the vibrational properties of amorphous silicon within the framework of tight-binding approach. The dynamical matrix elements have been evaluated numerically in the harmonic approximation exploiting the short-range nature of the density matrix to calculate the vibrational density…

Materials Sciencecond-mat.dis-nn

In-plane Hall effect in c-axis-oriented MgB2 thin films

W. N. Kang、Hyeong-Jin Kim、Eun-Mi Choi 等 7 位作者2002-01-16arXiv

We have measured the longitudinal resistivity and the Hall resistivity in the ab-plane of highly c-axis-oriented MgB2 thin films. In the normal state, the Hall coefficient (R_H) behaves as R_H ~ T with increasing temperature (T) up to 130 K and then deviates from that linear T-dependence at higher temperatures. The T^…

SuperconductivityMaterials Science

Why ferromagnetic semiconductors?

Tomasz Dietl2002-01-16arXiv

Rapid development of information technologies originates from the exponential increase in the density of information that can be processed, stored, and transfer by the unit area of relevant devices. There is, however, a growing amount of evidences that the progress achieved in this way approaches its limits. Various n…

Materials ScienceStrongly Correlated Electrons

High-Performance Polypropylene-Clay Nanocomposites by In-situ Polymerization with Metallocene/Clay Catalysts

Taolin Sun、Juan M. Garcés2002-01-16Advanced Materials

A novel in-situ polymerization approach has been used to manufacture polyolefin–clay nanocomposites (see Figure) with amazingly enhanced performance. The nanocomposites demonstrate reduced thermal expansion coefficients, improved melt flow strengths, increased heat-distortion temperatures, and lowered gas diffusion co…

biodegradable polymer synthesis and propertiesPolymer crystallization and propertiesPolymer Nanocomposites and Properties

Atom Transfer Radical Polymerization from Cellulose Fibers at Ambient Temperature

Anna Carlmark、Eva Malmström2002-01-16OpenAlex

Cellulose fibers have been successfully grafted with poly(methyl acrylate) using atom transfer radical polymerization, mediated by Me6-TREN and Cu(I)Br at ambient temperature. The initially hydrophilic cellulose was first modified by reacting the hydrozyl groups with 2-bromoisobutyryl bromide whereupon methyl acrylate…

Surface Modification and SuperhydrophobicityElectrospun Nanofibers in Biomedical ApplicationsAdvanced Cellulose Research Studies