Materials Literature
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A new synthesis pathway for MCM-48 is developed using fumed silica as the silicate source and a Gemini surfactant (GEM 16-12-16) as the surface directing agent. Different synthesis parameters have been optimized in order to obtain a highly ordered mesostructure. The determining factor in the stabilization of the final…
Er 3+ and Yb3+ ions codoped calcium aluminum germanate glass has been synthesized by solid-state reaction. An intense infrared emission at 1534 nm, which corresponds to the minimum losses of silica based fibers used in optical communications, and visible emissions at 416, 490, 525, 548, and 660 nm, corresponding to th…
As an evaluation test method for surface insulation degradation of organic insulating materials, the tracking test method is described in IEC Publ.112 as a safe and reliable evaluation. This publication has now been applied to the material selection. Due to the fact that the experimental values of the comparative trac…
MtaN (Multidrug Transporter Activation, N terminus) is a constitutive, transcriptionally active 109-residue truncation mutant, which contains only the N-terminal DNA-binding and dimerization domains of MerR family member Mta. The 2.75 A resolution crystal structure of apo-MtaN reveals a winged helix-turn-helix protein…
Nanopores in alumina membranes can serve as reaction vessels for the generation of nanosized gold particles. In addition, they enable a quasi one-dimensional arrangement of nanoparticles, the optical properties of which can easily be investigated due to their transparency in the visible and near ultraviolet (UV) regio…
We have developed a three-dimensional Monte Carlo simulator for thin film growth and applied it to understand the morphologies of thin films prepared by dynamic oblique deposition with a special emphasis on an effective surface area. Columnar shapes zigzag, helix, and cylinder are successfully reproduced, and the pack…
Abstract New types of phase transitions occurring in molecule-based materials have recently drawn great attention, in which electrons are directly involved. In this paper are given calorimetric investigations aimed at the elucidation of the mechanisms governing such phase transitions as (i) spin crossover phenomena oc…
The 20 MHz water relaxivity (r(1)) of gadolinium(III) complexes formed with two fatty acid analogues of 1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrakis(methylene phosphonate) were shown to increase substantially in the presence of albumin. The r(1) values of Gd(C(8)-DOTP)(5-) and Gd(C(11)-DOTP)(5-) in water were simi…
In traditional alloy development, experimental investigations with many different alloy compositions are performed. The selection criteria for multicomponent alloying elements and their compositions become diffuse in a traditional approach. Computational thermochemistry as used in the Calphad approach can provide a cl…
Layered double hydroxides are antitype 2/1 clay minerals that can be synthesized rapidly under laboratory conditions. Due to their high anion exchange capacities, layered double hydroxides have been investigated as potential adsorbents for removal of anionic contaminants from aqueous systems. In this study, uncalcined…
We present ab initio density-functional calculations for the electronic structure of the dilute magnetic semiconductors ${\mathrm{Mn}}_{x}{\mathrm{Ga}}_{1\ensuremath{-}x}\mathrm{As}$ and ${\mathrm{Mn}}_{x}{\mathrm{In}}_{1\ensuremath{-}x}\mathrm{As}$ with a realistic $x=0.063.$ We find that the introduction of Mn pertu…
Abstract PVC‐clay nanocomposites were prepared by melt blending of the polymer with an organically modified clay, both in the presence and in the absence of di(2‐ethylhexyl) phthalate (DOP). The clay can serve as a plasticizer for PVC in the absence of DOP. The nanocomposites were characterized by using X‐ray diffract…
The Affiliate Plan, established by the IEEE Board of Directors, enables individuals who are not members of the IEEE, but who have an interest in the field of plasma science, to join the IEEE Nuclear and Plasma Sciences Society. Admission as an affiliate requires only membership in a professional society listed below.…
Work has been performed to investigate the effect of inhibitor charge and pH, in the range 3.9 to 6.5, on the efficiency of various tertiary and quaternary amines. Results have revealed that for such adsorption type inhibitors performance at a given pH depends critically upon the charge of the adsorbing species. At pH…
A synthesis has been developed for 2,3,7,8,12,13-hexakis[2-(2-methoxyethoxy)ethoxy]-tricycloquinazoline (TCQ6EO2M) in which the ethylenoxy side chains are introduced before elaboration of the heterocylic core. This discogen gives a hexagonal columnar phase (Colh) between 77 and 233°C. n-Doping using potassium metal is…
Spectroscopic and thermal analysis indicates that tellurite glasses doped with B2O3 and GeO2 are promising candidate host materials for wide-band erbium doped fiber amplifier (EDFA) with a high 980 nm pump efficiency. In this study, we measured the thermal stabilities and the emission cross-sections for Er3+: 4I13/2 →…
A structurally‐related model for the viscosity of silicate melts developed by the present authors has been extended to melts containing alumina. In the binary Al 2 O 3 ‐SiO 2 system, viscosity was modelled by treating Al 2 O 3 as a metal oxide, i.e., as a network modifier based on the similarities in the general behav…
Phosphate solubility and reactions were investigated in each of three horizon samples from six cultivated soils representing Spodosols, Alfisols and Entisols, with pH ranging from 4.6 to 7.7. Soils were incubated for 30 days near field capacity moisture content without P application or with 44.5 mg P kg−1 soil applied…
A novel cryostat was developed for in situ neutron scattering studies on vapor-deposited amorphous samples. By the use of this cryostat, vapor-deposited amorphous ice was prepared at ca. 8 K. The neutron scattering spectra of the as-deposited sample and those annealed at ca. 120 K, 160 K, and 250 K were measured at 50…
Abstract Plane-wave pseudopotential total energy calculations have been applied to investigate the structure and energetics of the Cs/K exchange into interlayer sites in muscovite mica. Novel muscovite structures were designed to isolate the effects of 2:1 layer charge, cation size/interlayer site shape, and tetrahedr…