Materials Literature
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Liquid dewetting, physical confinement, and attractive capillary forces have been combined to assemble monodispersed spherical colloids into complex, zigzag aggregates characterized by well-defined internal structures and tightly controlled lengths.
We report the effect of the concentration of hydroxide ion adsorbed on indium tin oxide (ITO) in the electrodeposition of zinc oxide (ZnO) by potential modulation method. We found that by applying an optimal constant potential of −0.72 V, X-ray diffraction (XRD) peak intensity of crystalline phase indicating ZnO (100)…
Comparative investigations between the new lyocell fibers and the regular viscose and modal types were made in order to explain the reasons for the differences in the mechanical properties of the fibers. The purpose was a systematic analysis of structure characteristics and of influence of aqueous medium on the mechan…
The ligands cyanate and di-2-pyridyl ketone (dpk) are used to construct a tetranuclear cobalt(II) complex involving μ1,1-cyanate bridges: [Co4(dpk-OH)2(dpk-OMe)2(NCO)4], which shows a dicubane-type structure, with two missing vertices, and having ferromagnetic interactions.
The application of a mixed conduction model and a new contact electric impedance (CEI) technique to predict quantitatively the electronic and ionic transport properties of oxide films on iron in a nearly neutral tetraborate solution is discussed. The mixed-conduction model emphasizes the coupling between the ionic def…
The effects of tempering temperature on wear resistance and surface roughness of a high speed steel (HSS) roll manufactured by centrifugal casting method were investigated in this study. Hot-rolling simulation test was carried out using a high-temperature wear tester capable of controlling speed, load, and temperature…
Ternary complexes of formula [Gd–DO3A–L–(H2O)] (where L is a carboxylate-containing ligand) display exchange lifetimes of the metal-coordinated water that can be modulated as a function of L.
Hollow mesoporous silica fibers have been synthesized under acidic conditions in a two-phase static system. The fibers always have a circular internal architecture with hexagonally arranged channels running perpendicularly around the fiber axis. The inner radius of the hollow fibers is variable and the fibers are conn…
Age determination of plutonium particles is a highly important task in view of the pending cut-off treaty for nuclear weapons materials. By collecting particles from the vicinity or inside the nuclear facilities and determining their ages, it is possible to monitor the observance of the cut-off agreement. In this stud…
Mechanisms of a variety of charge and lattice ordered phases observed in halogen-bridged binuclear metal complexes are theoretically studied by applying the exact diagonalization and strong-coupling expansion methods to one- and two-band extended Peierls–Hubbard models. In R4[Pt2(pop)4I]nH2O [R = Na, K, NH4, (CH3(CH2)…
Silicon-based microelectromechanical system (MEMS) devices are made from single-crystal silicon, polycrystalline silicon (polysilicon) films obtained by low-pressure chemical vapour deposition and certain ceramic films. For high-temperature applications, SiC films are being developed to replace polysilicon films. Trib…
In this article, we present an experimental study of the formation of a Langmuir–Blodgett (LB) monolayer of alkanethiol-encapsulated gold particles. We developed a procedure for preparing the LB spreading suspension from an aqueous gold colloid, and we fabricated a large-scale densely packed monolayer of alkanethiol-e…
The structure and the composition of surface films formed by chemical conversion coating in Dow7 on pure magnesium and magnesium die cast AZ91D have been studied by XRD, XPS, SEM and TEM combined with ultramicrotomy to clarify the growth mechanism. The films are amorphous containing no definite crystallites detectable…
The interaction of ultraviolet laser light of wavelength 308 nm and a pulse length of 28 ns with 24 inorganic oxides was studied. The laser fluence was varied between 0.009 and 4 J cm−2. The visible result of the laser impulse could be divided into three categories. A number of oxides, CeO2, TiO2, Nb2O5, MoO3 and WO3,…
Polyaniline was doped with dodecylbenzenesulfonic acid (Pani · DBSA) in an agate mortar and used as a conductive additive in melt blends with styrene–butadiene–styrene (SBS) block copolymer. These blends exhibit relatively high levels of electrical conductivity at low-weight fractions of the polyaniline complex. The m…
The effect of convection on microstructure formation is examined experimentally and theoretically for the vertically upwards-directional solidification of Al–4.0 wt% Cu alloys. In this alloy system, the rejected solute is heavier than the solvent so that fluid flow occurs due to the presence of radial gradients in tem…
Description Fifty-seven papers provide a diverse and highly technical discussion of the influence of radiation on the microstructure and mechanical properties of structural materials. Nine sections cover: reactor pressure vessel (RPV) steels, austenitic and ferritic/martensitic alloys, proton and spallation neutron so…
Poly(lactic acid) (PLA) has potential for use in disposable and biodegradable plastics. Blending starch with PLAwould increase biodegradability and reduce costs. However, the brittleness of the starch/PLA blend is a major drawback formany applications. The objective of this study was to characterize thermal and mechan…
The preparation and characterization of the α-Keggin-type, novel tri-TiIV-1,2,3-substituted polyoxotungstates with heteroatoms P and Si are described. The molecular structure of K10H2[α,α-P2W18Ti6O77]·17H2O 1, obtained as a main product (30.4% yield) from the 1 ∶ 3 molar ratio reaction of tri-lacunary precursor Na9[A-…
Multi-walled carbon nanotubes, produced from catalytic decomposition of C2H2, were pre-oxidized by boiling nitric acid before being used as support media in a Co/carbon-nanotube monometallic catalyst system. The microstructures of nanotubes and the cobalt particles were examined by using high-resolution transmission e…