Materials Literature
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Phosphate glass (Pglass)/polymer hybrids are a unique material class that promises to help fulfill the growing need for new advanced materials. Rheological investigations into Pglass/polyamide 12 hybrids have shown a strong dependence on temperature and composition. Strong negative deviations from the log-additivity r…
The electron–photon coincidence technique has been used as the most sensitive tool for investigating inelastic collisions of atoms with electrons and heavy particles and led to new insights into collision dynamics theory. However, for purely geometrical reasons, due to finite sizes of the electron energy analysers and…
Abstract Localized Electrochemical Impedance Spectroscopy (LEIS) was used to study corrosion initiation of a cold-rolled steel panel covered by electrodeposited coating (Ecoat). LEIS technique, developed from the conventional electrochemical impedance spectroscopy (EIS) that usually measures the impedance over an area…
The effects of temperature (50-80°C), reaction time (up to 15h) as well as type and concentration of oxidizing agent (NaOCl, air O2, H2O2) on the course of oxidative polymerization of 4-[(pyridin-2-yl-imino)methyl]phenol (4-PIMP) in aqueous alkaline medium, and on the yield of the oligomers formed (O-4-PIMP) were inve…
Recently, it becomes possible to fabricate bulk metals having ultrafine grained or nanocrystalline structures of which grain size is in nano-meter dimensions. One of the promising ways to realize bulk nanostructured metals is severe plastic deformation (SPD) above logarithmic equivalent strain of 4. We have developed…
The behavior of a fire retardant in polypropylene is studied in order to improve the understanding of its activity in terms of its chemical behavior. The effect of a N-alkoxy hindered amine light stabilizer upon the fire performance of this system is also considered. The authors relate fire performance (UL 94, OI, NOI…
The structure and properties of quasicrystals are discussed. The short-and long-range atomic orders and the effect of these factors on the physical characteristics are considered. It is noted that investigations of the physical properties of quasicrystals at temperatures above room temperature should be performed. Pro…
In this paper, we report the funtionalization of multiwalled carbon nanotubes (MWCNTs) with Ni3S2 using a solvent-thermal approach. The nanocomposites synthesized without ammonia show that the MWCNTs' outer surface was uniformly coated with a Ni3S2 film appearing like centipede-shaped objects when characterized by sca…
Abstract The effect of polyvinylidene fluoride (PVDF) on the crystallization behavior of polyoxymethylene (POM) was investigated using polarized light microscopy, wide angle X‐ray diffraction, and differential scanning calorimetry. From these results, it is seen that with the addition of PVDF, the spherulitic size of…
A chemical route to decorate MWCNTs by titanium nanoparticles has been developed. MWCNTs, grown by catalytic decomposition of propane, have been used to prepare intercalated K-MWCNTs, which are then reacted with Ti(IV) isopropoxide. The amount of Ti present in the nanostructure is 8.7 wt%. Several techniques have been…
Detailed and consistent crystal field analysis of the LiGa 5 O 8 :Cr 3+ absorption spectrum is performed in the present paper by using the exchange charge model of crystal field. We calculate the crystal field parameters from the crystal structure date and diagonalize the crystal field Hamiltonian to obtain the energy…
1. Symmetry in Crystals: Fundamentals 2. Point Groups and Lattice Types 3. Space-Group Symmetry 4. X-ray Diffraction Techniques 5. The Structure Factor and the Electron Density 6. The Patterson Function 7. Structure-Factor Statistics 8. Direct Methods 9. Atomic Displacement Parameters 10. Refinement of Structural Para…
Abstract The nonisothermal crystallization kinetics of poly(vinylidene fluoride) (PVDF) in PVDF/dibutyl phthalate (DBP)/di(2‐ethylhexyl)phthalate (DEHP) blends via thermally induced phase separation were investigated through differential scanning calorimetry measurements. The Ozawa approach failed to describe the crys…
Abstract Growth mechanisms of carbon nanotubes are investigated and compared for both high‐ and low‐temperature synthesis methods through experiments utilizing time‐resolved, in situ imaging and spectroscopy. High‐speed videography and pyrometry measured the timeframes for growth for single‐wall carbon nanotubes (SWNT…
In this paper, a summary of some of the recent research efforts in our laboratory on chemical interactions at noble metal nanoparticle surfaces is presented. The article is divided into five sections, detailing with (i) interactions of simple halocarbons with gold and silver nanoparticle surfaces at room temperature b…
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Liquid‐crystalline (LC) monomers, which were functionalized with a cinnamoyl group on their extremity, were synthesized and irradiated with UV light in their LC phases. In the presence of a triplet sensitizer, most LC monomers were converted into the corresponding dimers, which were produced by the cycloaddition react…
A 1.7-fold enhancement in the spontaneous emission intensity of dye chromophore loaded in a printable polymer is achieved by coupling the dye emission to surface plasmons of metallic nanoparticles. The nanocomposite material, embossed into arrays of wires by nanoimprint lithography process, shows good imprint properti…
The use of silicon based light emitting diodes may completely solve the problem of low compatibility of optoelectronics elements and silicon chip. At present time the most suitable kinds of Si-LEDs are monocrystal and porous silicon avalanche LEDs. They have advantages such as long operation lifetime (> 10000 hours),…
Doping of the ZnGeAs2 semiconductor with manganese has produced compositions with spontaneous magnetization and high Curie temperatures of up to 367 K for the composition 3.5 wt% Mn. Their magnetic properties are characteristic of spin glasses at temperatures T < T S and magnetic fields H < 11 kOe. In stronger fields,…