Materials Literature
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Two new amide chloride phases, with approximate stoichiometries Li7(NH2)6Cl and Li6Mg0.5(NH2)6Cl, have been identified by powder X-ray diffraction, and their hydrogen storage properties studied. Both phases released hydrogen on reaction with LiH at a lower temperature than observed for lithium amide, and ammonia relea…
Abstract Abstract. In the crystal structure of the clathrate‐I K 8 Li x Ge 44– x /4 □ 2–3 x /4 , the K atoms fill the polyhedral cages of a host framework formed by Li and Ge atoms. The phase has been obtained in two forms, at elevated temperatures with space group Pm $\bar{3}$ n , and at low temperatures with a 2 a 0…
The effects of addition of synthesized organic-suspension silver nanoparticles on the crystallization and thermal stability of poly(3-hydroxybutyrate-co-3-hydroxyvalerate) (PHBV) were studied by transmission electron microscopy (TEM), differential scanning calorimetry (DSC), wide-angle X-ray diffraction (XRD), UV-Vis…
The present work is aimed at studying the fracture behavior of a hydroxyl-terminated polybutadiene solid rocket propellant. A fracture mechanics method based on the integral was adopted to evaluate the material’s resistance against crack initiation and propagation with the auxiliary of a high-speed microscopic camera…
In this research, we studied the preparation of nanochitosan from the addition of potassium persulfate as an initiator for monomer polymerization and monocarboxylic acid—namely acetic acid, lactic acid, and formic acid—to a chitosan solution. To obtain the dried form of chitosan nanoparticles, we investigated the effe…
Inspired by a Newton's cradle device and interested in the development of redox-controllable bimetallic molecular switches, a mixed-valence thallium(III)/thallium(I) bis-strap porphyrin complex, with Tl(III) bound out of the plane of the N core and Tl(I) hung to a strap on the opposite side, was formed by the addition…
We study the linear and nonlinear acoustic response of SrTiO3 across its ferroelastic transition at Ta=105 K by time domain Brillouin scattering. Above Ta we observe that for a strain amplitude of ∼0.18% the sound velocity for compressive strain exceeds the tensile strain velocity by 3%. Below Ta we find a giant slowi…
Rice husk is a potential source for renewable energy and silica. To extract the maximum amount of silica, usually the rice husk is treated with strong acids that burn the organic part leaving behind a black residue. In this research, sulfuric acid is used as an oxidizing agent. Efforts are focused to find out more abo…
Nitrogen doping in carbon nanotube (CNT) fibers using pyrolyzed ionic liquid induced interfacial hydrogen bonding between individual CNTs, enhancing mechanical properties and electrical conductivity simultaneously. In particular, the nitrogen doped CNT fiber using the ionic liquid BMI-I exhibited about 104%, 714%, and…
ABSTRACT A robust and coarse surface mesh was fabricated by introducing a hydrogel coating with interpenetrating polymer network (IPN) structure on stainless steel mesh. The IPN hydrogel was prepared by crosslinking polymerization of acrylic acid (AA) followed by condensation reaction of polyvinyl alcohol (PVA) and gl…
In this study, complex optical parameters such as absorption, extinction coefficient, refractive index, optical conductivity and real and imaginary dielectric constants of V2O5–P2O5–B2O3–Dy2O3 glass systems were studied. The conformation of the glassy phase in a sample was accomplished by X-ray diffraction analysis, a…
We report the growth of multi-walled carbon nanotube forests employing an active-active bimetallic Fe-Co catalyst. Using this catalyst system, we observe a synergistic effect by which—in comparison to pure Fe or Co—the height of the forests increases significantly. The homogeneity in the as-grown nanotubes is also imp…
A 'powder-poling' technique was developed to study electric field induced structural transformations in ferroelectrics exhibiting a morphotropic phase boundary (MPB). The technique was employed on soft PZT exhibiting a large longitudinal piezoelectric response (d(33) ∼ 650 pC N(-1)). It was found that electric poling…
Considering the boom in the market for wood plastic composite (WPC) products due to their relatively high specific strength properties, low maintenance costs, and wide range of applications, many authors have studied the performance of these composites prepared by reactive extrusion with different compatibilizers and…
Highly cation-ordered (100) and (110)-oriented PbSc0.5Ta0.5O3 (PST) films were deposited on buffered Si (100) substrates using pulsed laser deposition. Switching of crystal orientation from (100) to (110) was achieved by replacing the Si (100)/ZrO2:Y2O3 (100)/CeO2 (100)/LaNiO3 (100)/PST (100) heterostructure with Si (…
Among the widely studied superconducting iron-pnictide compounds belonging to the Ln1111 family (with Ln a lanthanide), a systematic investigation of the crossover region between the superconducting and the antiferromagnetic phase for the Ln = Nd case has been missing. We fill this gap by focusing on the intermediate…
In this work, NiO thin films have synthesized by pulsed laser deposition on glass substrates with different substrate temperature (100, 200, 300)°C, using Q-switching Nd:YAG laser. Structure and optical properties have carried out by using FTIR, AFM and UV- Vis spectroscopy. FTIR spectraconformed of NiO bonding an…
Colloidal quantum dots (QDs) with a ZnO core were synthesized with subsequent surface passivation by MgO. The photo-enhancement effect of the near band-edge photoluminescence (PL) in ZnO nanocrystals, dispersed in ethanol, is investigated by observing changes in the optical properties after ultraviolet (UV) exposure.…
The effects of die geometry on the deformation behavior of aluminum 6061 alloy tube in a novel severe plastic deformation (SPD) process called tube channel pressing (TCP) were studied using the Abaqus 6.10 software. Using the optimized die geometry, 1 to 3 passes of TCP is imposed not only to validate the simulation r…
Abstract Magnetic resonance imaging (MRI) is an imaging modality adequate for in vivo studies. Therefore, many scientists are interested in the development of MRI probes capable of detecting enzyme activities in vivo. 19F MRI is useful for monitoring particular biosignals, cells, and target tissues, due to the absence…