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Views Icon Views Article contents Figures & tables Video Audio Supplementary Data Peer Review Share Icon Share Twitter Facebook Reddit LinkedIn Tools Icon Tools Reprints and Permissions Cite Icon Cite Search Site Citation A. S. Glass, V. M. Bermudez; Infrared study of high pressure and high temperature coadsorption of…
The kinetics of polymerization of racemic and optically active mandelic acid were determined under a variety of conditions. The initial rate of monomer consumption in the reaction with racemic mandelic acid was approximately twice that for the single enantiomer for acid-catalyzed reactions in benzene solution. A signi…
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTSynthesis of 2-(2-hydroxyphenyl)-2H-benzotriazole monomers and studies of the surface photostabilization of the related copolymersF. A. Bottino, G. Di Pasquale, A. Pollicino, Antonino Recca, and D. T. ClarkCite this: Macromolecules 1990, 23, 10, 2662–2666Publication Date (Pr…
The combination of some additions and substitutions to sintered Nd-Fe-B magnets was investigated in order to obtain high coercivity and good thermal stability. Some additions (Al,Ga,Nb,W) and a substitution (Dy for Nd) give Nd-Fe-B-based sintered magnets high coercivities without a large remanence loss. Small differen…
The morphology, systematics and ecology of a new centric diatom—CycZotelZa cretica, from Lake Kournas in the island of Crete, Greece—are reported. The morphological variation and ultrastructure of the diatom are described as revealed by light and scanning electron microscopy. The species is characterised by a smooth f…
The Zr - free fluoride glass termed BIZYbT and based on the combination of Baryum, Indium, Zinc, Ytterbium and Thorium fluorides hasbeen optimized in orderto decrease thecriticalcoolingrate and make this glass suitablefor fiberdrawing. The lowest value of 5°C/mn has been obtained and is comparable to the classical ZBL…
Abstract Poly(2‐hydro‐2‐oxo‐1,3,2‐dioxaphosphorinane) was quantitatively chlorinated, and the resulting polymer was reacted with excess of imidazole, giving the highly reactive polyesteramide. This polymer, treated with N 1 ‐hydroxyethyluracil, gave polyphosphates with N 1 ‐oxoethyleneuracil in the side chains. The fi…
Abstract The progression of squamation and the formation of ctenii in developing juveniles of completely ambicolorate specimens of the Japanese flounder, Paralichthys olivaceus (Temmink et Schlegel), have been examined and compared with those of normally colored fish. The squamation developed with a similar pattern on…
Abstract Differential scanning calorimetry (DSC) has been utilized in several studies on polymerization kinetics, at different heating rates. However, there are several factors affecting the precision of kinetic parameters. In this work, the activation energy of urethane‐bond formation between 2,6‐tolylene diisocyanat…
A novel method of single-crystal growth from the melt is proposed. Single crystals are grown by directional solidification in vertical bottom-seeded crucibles. The heat is supplied to the melt by an axial submerged heater located close to the growth interface. The crucible is insulated radially. The portion of the mel…
Acoustic damping in polymers is shown to be dominated by the glass transition occurring in the amorphous portions of the polymer. Thus to tailor damping characteristics for a particular application requires an understanding of the relation between chemical composition and glass transition temperature. Glass transition…
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTInfluence of bromine doping on the electrical conductivity of carbonized poly(vinylidene chloride)Junichi. Ozaki, Iwao. Sunami, and Yoshiyuki. NishiyamaCite this: J. Phys. Chem. 1990, 94, 9, 3839–3843Publication Date (Print):May 1, 1990Publication History Published online1 M…
The susceptibility of Nd-Fe-B magnet powders to oxidation and corrosion is well known and presents problems in processing and in service. Although the oxidation of Nd-Fe-B magnet powders can lead to severe irreversible losses, such losses can be stemmed by the application of antidegradation coatings. The effects of ox…
Abstract Surface‐enhanced Raman scattering (SERS) was observed from thin films formed by 1,4‐ and 1,3‐dinitrobenzene (DNB) spin‐coated onto silver island films from dilute solutions. During laser irradiation of 1,4‐DNB films on silver substrates at relatively high laser powers, new bands appeared near 1152, 1350, 1412…
The effects of substitution of GeO2 for ZnO on the microstructure and magnetic properties of Mn-Zn ferrite have been studied. Results suggest that, to a very limited extent, by the substitution of Ge and a proper choice of sintering condition, good temperature coefficients can be obtained in a temperature range from 2…
Titanate ceramic waste forms were prepared using several combinations of calcination atmosphere (N 2 , N 2 ‐3.5% H 2 , H 2 ) and metallic redox buffers (Ni, Fe, Ti, Al) to examine the dependence of microstructure and durability upon oxygen activity. It was found that the microstructures and phase assemblages were most…
We present a simple mathematical model for the description of defect chaos in electrohydrodynamic convection. Our model can exhibit the transition from the Williams domain to the fluctuating Williams domain.
This document contains the accident sequence analyses of internally initiated events for the Zion Unit 1 Nuclear Power Plant. This is one of the five plant analyses conducted as part of the NUREG-1150 effort for the Nuclear Regulatory Commission. The work performed and described here is an extensive reanalysis of the…
This paper describes a novel route for the production of low‐oxygen‐containing fluorozirconate glasses. The process involves the use of a hitherto unknown solid‐state chemical reaction between ammonium bifluoride and specific anhydrous and hydrated metal fluoride salts. The products are defined as ammonium fluoride–me…
Data is presented which demonstrate that positron annihilation‐induced auger electron spectroscopy (PAES) can be used to eliminate secondary electrons in the energy range of Auger electrons. In PAES the core–hole excitations necessary for Auger electron spectroscopy (AES) are created by annihilation of core electrons…