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Energy-filtering transmission electron microscopy in materials science

Ludwig Reimer、I. Fromm、Christoph Hülk 等 4 位作者1992-01-01Microscopy Microanalysis Microstructures

Energy-filtering transmission electron microscopy (EFTEM) with an imaging filter lens can combine the modes of electron spectroscopic imaging (ESI) and electron spectroscopic diffrac- tion (ESD), and different modes can be used to record an electron energy-loss spectrum (EELS). Therefore, an EFTEM can make full use of…

Electron and X-Ray Spectroscopy Techniquesnanoparticles nucleation surface interactionsAdvanced Materials Characterization Techniques

Monomer‐micelle equilibrium in the diffusion of surfactants in binary systems through collagen films

M. Teresa García、Isabel Ribosa、J. Sánchez Leal 等 4 位作者1992-01-01Journal of the American Oil Chemists Society

Three different binary systems (two anionic/nonionic and one anionic/amphoteric) were selected to study the behavior of these mixtures in their diffusion through a collagen film and the formation of micelle aggregates in such systems. The inhibition observed in the surfactant diffusion of anionic/nonionic and anionic/…

Surfactants and Colloidal SystemsPolymer Surface Interaction StudiesCollagen: Extraction and Characterization

An AMTEC vapor-vapor, series connected cell

M. L. Underwood、Roger M. Williams、Margaret A. Ryan 等 5 位作者1992-01-01AIP conference proceedings

The alkali metal thermal‐to‐electric converter (AMTEC) converts heat energy to electrical energy with efficiencies up to 3 to 4 times the state of the art static converters. However, the high current, low voltage output of a single module requires difficult series connecting of cells, and several life limiting concern…

Ferroelectric and Piezoelectric MaterialsAdvanced Battery Materials and TechnologiesThermal Expansion and Ionic Conductivity

The trapping of electrons in polystyrene

P.K. Watson、F.W. Schmidlin、R.V. La Donna1992-01-01IEEE Transactions on Electrical Insulation

The trapping of electrons in localized states in polystyrene has been studied by means of an electron beam technique. A 2.2-kV beam is used to inject a short pulse of charge into the free surface of a thin film of the polymer, and a second electron beam monitors the surface potential of the film. The surface potential…

Semiconductor materials and devicesHigh voltage insulation and dielectric phenomenaElectrostatic Discharge in Electronics

Tubular mesophases: a structural analysis

Jacques Malthête、Anne‐Marie Levelut、Jean‐Marie Lehn1992-01-01Journal of the Chemical Society Chemical Communications

The hitherto doubtful tubular mesomorphism of 1a has been confirmed by X-ray diffraction experiments on a mixture of the mesophase of 1a with the mesophase of its Br-substituted analogue 1b.

Liquid Crystal Research AdvancementsSupramolecular Self-Assembly in MaterialsMolecular spectroscopy and chirality

Boron nitride fibers processed from poly(borazinylamine) solutions

D. A. Lindquist、Jerzy F. Janik、Abhaya K. Datye 等 5 位作者1992-01-01Chemistry of Materials

ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTBoron nitride fibers processed from poly(borazinylamine) solutionsDavid A. Lindquist, Jerzy F. Janik, Abhaya K. Datye, Robert T. Paine, and J. Bruce RothmanCite this: Chem. Mater. 1992, 4, 1, 17–19Publication Date (Print):January 1, 1992Publication History Published online1…

Metal and Thin Film MechanicsBoron and Carbon Nanomaterials ResearchMXene and MAX Phase Materials

Formation of ferroelectric domains in a copolymer P(VDF–TrFE)

Hiroji Ohigashi、Nobuyuki Kagami、G. R. Li1992-01-01Journal of Applied Physics

The effects of reannealing on the depolarization and phase transition behaviors of poled ferroelectric copolymer film of P(VDF–TrFE) (75/25) are studied by using differential scanning calorimetry (DSC) and piezoelectric resonance techniques from a viewpoint of formation of ferroelectric domains. It is found that the D…

Liquid Crystal Research AdvancementsPolymer Nanocomposites and PropertiesNonlinear Optical Materials Research

Visible luminescence from porous silicon and siloxene

H. D. Fuchs、M. Stutzmann、Martin S. Brandt 等 6 位作者1992-01-01Physica Scripta

Infrared transmission and Raman spectra of siloxene (Si 6 O 3 H 6 ) and porous Si have been analyzed in terms of the structural composition. Siloxene consists of Si 6 -rings interconnected by oxygen and terminated by hydrogen, and corrugated Si(111)-planes saturated by OH and H. The pronounced photoluminescence of sil…

Carbon Nanotubes in CompositesSilicon Nanostructures and PhotoluminescenceNanowire Synthesis and Applications

Special issue "Magnesium and magnesium alloys". Precipitation structures of Mg-Y alloys.

Tatsuo Sato、Isao Takahashi、Hiroyasu Tezuka 等 4 位作者1992-01-01Journal of Japan Institute of Light Metals

Precipitation process and microstructures of both Mg-5%Y and Mg-10%Y (in mass%) alloys were investigated using hardness measurement, optical microscopy and transmission electron microscopy. In a Mg-5%Y alloy hardness increased slightly by about HV 10 with aging time at temperatures between 423 and 523K. In a Mg-10%Y a…

Metal and Thin Film MechanicsMagnesium Alloys: Properties and ApplicationsHydrogen Storage and Materials

Intramolecular NH ? S hydrogen bond in o-acylamino substituted benzenethiolate iron(II) and cobalt(II) complexes

Norikazu Ueyama、Taka‐aki Okamura、Akira Nakamura1992-01-01Journal of the Chemical Society Chemical Communications

The crystal structures of (NEt4)2[FeII(o-pabt)4](o-pabt =o-pivaloylaminobenzenethiolato) and (NEt4)2[CoII(o-pabt)4] show the presence of NH ⋯ S hydrogen bonds which contribute to the positive shift of redox potential and the through-bonding isotropic-contact shift.

Metal complexes synthesis and propertiesMagnetism in coordination complexesMetal-Catalyzed Oxygenation Mechanisms

Electron-beam-enhanced flow and instability in amorphous silica fibres and tips

P. M. Ajayan、Sumio Iijima1992-01-01Philosophical Magazine Letters

Amorphous silica structures which are a few nanometres in width and tens of nanometres in length are seen to become unstable under intense electron irradiation against plastic deformation, necking and failure. Similarly irradiated atomistically sharp tips, which are observed to be stable in crystalline materials, unde…

High-pressure geophysics and materialsGlass properties and applicationsIon-surface interactions and analysis

Ionic conductivity and dielectric properties of vanadium pentoxide xerogels

Jean‐Claude Badot、No�l Baffier1992-01-01Journal of Materials Chemistry

The electrical transport properties of cation-exchanged MxV2O5·yH2O (M = Al, Li, Zn, Ni, Na, Ag, H3O, K, Ba and Cs) xerogels have been studied in a broad frequency range 1 KHz–10 GHz between 190 and 300 K. In the low-frequency domain (1–100 kHz), the ionic conductivity has been obtained by the a.c. admittance method w…

Gas Sensing Nanomaterials and SensorsAdvanced Condensed Matter PhysicsSolid-state spectroscopy and crystallography

Tailoring Process Control

Sueo Kawabata、Kodo Ito、Masako Niwa1992-01-01Journal of the Textile Institute

The KESF system, which was developed for the objective measurement of fabric handle, provided precise measurements of fabric mechanical properties in the low-load range, which was enough to apply them to tailoring process control. The joint research of the present authors began in 1975 with the accumulation of a datab…

Textile materials and evaluationsColor Science and ApplicationsIndustrial Vision Systems and Defect Detection

Recent Studies on the Precise Crystal-Structural Analyses of Martensitic Transformations

Ken rsquo ichi Shimizu、Tsugio Tadaki1992-01-01Materials Transactions JIM

Recent studies on the martensitic transformations by precise crystal-structural analyses have been reviewed. Crystal structures of the B19′ and ζ′2 martensites in Ti–Ni and Au–Cd alloys, respectively, which had been controversial for a long time because of their complexity, and the γ′1 and γ′2 martensites in Cu–Al–Ni…

Microstructure and Mechanical Properties of SteelsShape Memory Alloy TransformationsMagnetic Properties and Applications

Reactive Wetting of Ceramics by Liquid Metals

Hideo Nakae、Hidetoshi Fujii、Kenji Sato1992-01-01Materials Transactions JIM

In order to establish a method for estimation of the wetting of ceramics accompanied by interfacial reaction, the authors’ previous work has been rearranged. The wetting was estimated using meniscography and an improved sessile drop method both of which were devised to measure the wetting from the initial contact. Usi…

Surface Modification and SuperhydrophobicityNanomaterials and Printing TechnologiesAdhesion, Friction, and Surface Interactions

Contact angle equilibrium: the intrinsic contact angle

Abraham Marmur1992-01-01Journal of Adhesion Science and Technology

The conceptual and mathematical difficulties associated with contact angle equilibrium are reviewed and analyzed. The main discussion is centered around the theory of the intrinsic contact angle and its dependence on the three-phase mutual interactions in the vicinity of the contact line. Rigorous thermodynamic deriva…

Material Dynamics and PropertiesMinerals Flotation and Separation Techniquesnanoparticles nucleation surface interactions

Stefan Problem with Surface Tension as a Limit of the Phase Field Model

П. И. Плотников、V. N. Starovoîtov1992-01-01Birkhäuser Basel eBooks

The quasistationary phase field model equations depending on the small parameter are considered. It is proved that these equations possess a family of the solutions, which converge to the solutions of the Stefan problem with surface tension as the small parameter tends to zero.

Solidification and crystal growth phenomenaAdvanced Mathematical Modeling in EngineeringDifferential Equations and Numerical Methods

Materials under Irradiation

A. Dunlop、F. Rullier-Albenque、C. Jaouen 等 5 位作者1992-01-01Trans Tech Publications Ltd. eBooks

The purpose of this book is to provide a state-of-the-art picture of the field of radiation damage. It covers various topics extending from theoretical understanding of energy deposition and defect creation to industrial and nuclear applications.

Nuclear Materials and Properties

Fabrication of Silicon Nitride Based Composites by Impregnation with Perhydropolysilazane

Kiyoshi Sato、Tadashi Suzuki、O. Funayama 等 4 位作者1992-01-01Journal of the Ceramic Society of Japan

A low viscosity perhydropolysilazane which is converted to Si-N ceramics with a 70-90wt% yield by pyrolyzing at temperatures above 800°C, was used as a matrix precursor. The preform of SiCw/Si-N composites was prepared by slip casting, and impregnated with the polysilazane. The impregnated specimen was cured at 100°-3…

Advanced ceramic materials synthesisAdvanced Surface Polishing TechniquesSilicone and Siloxane Chemistry

Localization and characterization of acid phosphatase activity in Bonamia ostreae (Ascetospora), an intrafemocytic protozoan parasite of the flat oyster Ostrea edulis (Bivalvia)

D Hervio、Dominique Chagot、Paul J. Godin 等 5 位作者1992-01-01Diseases of Aquatic Organisms

Acid phosphatase activity was cytochemically detected at the ultrastructural level in the protozoan Bonamla ostreae, an intrahemocytic parasite of the flat oyster Ostrea edulis. Lead nitrate was used as capture agent for phosphate liberated during the hydrolysis of the substrate (cytidine 5' monophosphate). Lead phosp…

Marine Bivalve and Aquaculture StudiesCalcium Carbonate Crystallization and Inhibition