Materials Literature
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A novel class of allyl compounds based on epoxy resins was synthesized and characterized. The synthesis of these allyl compounds was carried out by reacting corresponding epoxy resin with 2-allyl-4-methylphenol. The copolymers of 4,4′-bismaleimi-dodiphenyl methane with the allyl compounds were prepared and their prope…
The wetting behavior of single‐crystalline magnesia (MgO) by fayalite‐type slag melts has been studied by the sessile‐drop technique, which incorporates high‐temperature X‐ray radiography. The experiments have been performed under oxygen partial pressures of 106 and 104 Pa at a temperature of 1473 K. The mass ratios o…
Copper has been proposed as a possible replacement for aluminum as the primary microelectronics metallization material. As the feature sizes of ultralarge scale integration (ULSI) technologies reach sub-0.25 μm in dimension, new metallization processes must be developed to properly fill the extreme topographies. This…
ZnO thin films have been grown on glass substrates using the spray pyrolysis technique. The depositions were carried out in the range of substrate temperatures from 400 to 500 °C. Highly c-axis oriented ZnO films, having a strong (002) X-ray diffraction line, are obtained at lower temperatures (400 to 420 °C). Film su…
Anomalous dispersion of X-ray diffraction at wavelengths near the X-ray K-absorption edge of sulfur at wavelengths around 5 A has been applied to single crystals of trypsin obtained from an ammonium sulfate solution. The multiwavelength anomalous-dispersion method based on 775 unique reflections (+183 Bijvoet mates) m…
Small amounts of polytetrafluoroethylene (PTFE) are shown to modify the combustion behaviour of Acrylonitrile–Butadiene–Styrene terpolymers (ABS) fire retarded with a bromine/antimony synergistic system. PTFE makes ignition more difficult and decreases the rate of flame propagation in the early stage of combustion. Th…
(La,Sr)CoO3/Pb(Zr,Ti)O3/(La,Sr)CoO3 (LSCO) heterostructures have been grown on LaAlO3 substrates by pulsed laser deposition (PLD) to investigate asymmetric polarization switching of Pb(Zr,Ti)O3 (PZT) thin films with different electrode configuration. P-V hysteresis loop of LSCO/PZT/LSCO was symmetric. However, LaCoO3…
Abstract Starch, totally biodegradable polysaccharide biosynthesized by numerous plants, is one of the most abundant renewable resources known to man. Composed mostly from linear amylose and highly branched amylopectin, the starch, in its granular form, is a crystalline material. When mixed with limited amount of wate…
Abstract Crystallization and supramolecular aggregation of 1,4,7,10,13‐pentaoxacyclopentadecane‐2‐ylmethyl 3,4‐bis[4‐(dodecyl‐1‐oxy)benzyloxy]‐5‐(11‐methacryloyloxyundecyl‐1‐oxy)benzoate ( 1 ) and its complexes with sodium triflate are described in solutions of the methacrylate monomers. Formation of a gel was observe…
Abstract The influence of structural recovery or physical aging on the craze initiation of amorphous polystyrene and a styrene‐acrylonitrile copolymer has been examined in two states of stress/deformation and at different temperatures. Studies of craze initiation in equibiaxial creep were performed using a “bubble” in…
Abstract The titled new salts were synthesized by exchanging the unknown counter anion of [Sb(pc)Cl2]+ salt (pc2− = phthalocyaninate, C32H16N82−), which was the first product of the reaction of phthalonitrile with antimony(III) trichloride, with perchlorate, tetrafluoroborate, and hexafluorophosphate. Elemental analyt…
Abstract There is a growing demand for rigid vinyl foam as a wood replacement in window frames, blinds, trimming and other applications. While rigid vinyl foam has existed for many years, additional understanding of its processability and required conditions for good quality extruded profile would be helpful. This pap…
In this paper we propose a fitting procedure to describe the bandpass effect on all x radiation that passes through a focusing graphite monochromator used on the diffracted beam. The proposed bandpass function is: M (2θ)=1/(1+ K mon 1 s K mon 2 ), with s =(2 sin θ)/λ, where K mon 1 and K mon 2 are constants which have…
Electrical resistance measurements and x-ray-diffraction experiments have been carried out under high pressure for \ensuremath{\alpha}-monoclinic and amorphous and trigonal Se. \ensuremath{\alpha}-monoclinic Se showed a transition to the metallic state at 12 GPa, which was considerably lower than 23 GPa of trigonal Se…
Expansion of a mesh skin graft depends on factors pertaining to the graft itself as well as on parameters of the meshing device. With regard to the graft, we examine the efficiency of graft handling and thickness of the skin graft. With regard to the parameters of the meshing apparatus, which determine the expansion r…
The intensity of Raman modes of four different silicate garnets in the energy range 1.9–2.7 eV was investigated. In the case of almandine (Fe3Al2Si3O12) and pyrope (Mg3Al2Si3O12) no change in intensities was observed in this energy region and in uvarovite (Ca3Cr2Si3O12) a weak resonance maximum was observed between 2.…
ArF excimer laser photolysis of gas phase tetramethyltin was used to deposit thin organotin films on Si. In situ Auger electron spectroscopy and x-ray photoelectron spectroscopy (XPS) film analysis, showed the presence of C and Sn, which, according to C 1s and Sn 3d5/2 peak deconvolution, were organized in highly bran…
Three existing multislice formulations (MS) that are claimed to be applicable for large beam tilt are introduced in a unified form and the validity of these formulations for large beam tilt is evaluated. It is shown that one formula, which is called MSSBT (the MS for small beam tilt), is valid only for tilt angles les…
This paper deals with the problem of carpet resilience which depends on pile yarn properties and carpet construction characteristics. Up to now, resilience could only be measured on the carpet itself. New methods are being developed to assess the resilience properties of pile yarns directly before carpet manufacturing…
This study compared the relative effectiveness of TLD crystals LiF:Mg,Ti (TLD-100) and LiF:Mg,Cu,P (TLD-700H) for clinical dosimetry, focusing on reproducibility, linearity, and energy response. Experimental results indicated that TLD-700H was superior to TLD-100 with regard to reproducibility, lack of supralinearity,…