Materials Literature
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We report on the fabrication of terminating-layer-controlled La0.6Sr0.4MnO3 (LSMO) thin films and in situ characterization of the films using photoemission spectroscopy. The terminating layer of the LSMO films was changed from B to A site by inserting one atomic layer of SrO between the LSMO film and a TiO2-terminated…
The temperature dependence of the spin polarization of half-metallic ferromagnets is investigated. A unitary spinor transformation shows that the corresponding spin mixing goes beyond finite-temperature smearing of the Fermi level, leading to a nonzero density of states in the gap of the insulating spin channel. As a…
High-quality epitaxial thin films of Co-doped anatase TiO2 (Co:TiO2) were grown epitaxially on SrTiO3 (001) substrates by using pulsed laser deposition with in-situ reflection high-energy electron diffraction. The oxygen partial pressure, PO2, during the growth was systematically varied. As PO2 decreased, the growth b…
Magnetic properties of IV–VI compound GeTe based diluted magnetic semiconductors with 3d transition metals from Ti to Ni have been investigated. Ferromagnetic order is observed for the Cr, Mn, and Fe doped GeTe films, whereas the Ti, V, Co, and Ni doped films are paramagnetic. The ferromagnetic order could give rise t…
Although the 3ω method was originally introduced to measure the thermal conductivity of bulk material and was later developed further to include thin-film materials, many thermal and geometrical parameters influence the 3ω signal. We show that several of these parameters can be determined simultaneously from a single…
Sm–Co nanoparticles with 7 nm mean diameter have been obtained by gas condensation in a cluster gun. By absorbing light from quartz halogen bulbs, the nanoparticles are annealed during their flight from the cluster gun to the substrate and are embedded in a carbon matrix by cosputtering. This in situ annealing results…
We report preliminary high-frequency electron paramagnetic resonance (EPR) investigations for several tetranuclear nickel complexes which exhibit single-molecule magnetism, including low-temperature (below ∼1 K) hysteresis loops and resonant magnetic quantum tunneling. The combination of a cavity perturbation techniqu…
The effect of mechanical milling on the luminescence properties of ZnO microcrystalline samples has been studied by means of cathodoluminescence in a scanning electron microscope. The samples consisted of pressed pellets of commercially available ZnO powder which were ball milled to investigate the possibility of nano…
Ni–Zn–Co ferrite films were deposited by the spin-spray ferrite plating from an aqueous solution. Film with optimized Zn and Co contents (i.e., Ni0.22Zn0.52Co0.03Fe2.23O4) exhibited the real permeability μr′ higher than 260 at frequencies up to 130 MHz, and the imaginary permeability μr″ higher than 100 in the extreme…
Asymmetric diblock copolymers with a spherical domain structure form islands or holes on the free surface of a thin film when the initial spun-cast film thickness does not match that of an integral number of layers of spheres plus a brush. When this film is cast on a substrate topologically patterned with rectangular,…
Nanosized ferrite spherical particles, ∼30 nm in diameter as revealed by scanning electron microscopy, were synthesized from an aqueous Fe(OH)2 suspension (pH=7.6–8.0) at 25 °C by oxidizing it with H2O2. The nanoparticles were of a spinel structure of an intermediate between Fe3O4 and γ-Fe2O3, as revealed by x-ray dif…
The evolution of stress in 50 nm FexPt1−x (x=0.41, 0.43, 0.49, 0.52, and 0.56) sputtered films was monitored in situ as a function of the temperature. In the as-deposited state, films have a disordered face-centered-cubic (fcc) structure with a strong (111) fiber texture and 685–978 MPa compressive stress. Below 200 °…
Plasma synthesis has previously been shown to be a viable route to producing nanocrystalline magnetite and Ni ferrite nanoparticles. In this work nanocrystalline powders of Mn and Mn–Zn ferrites have been synthesized using a 50 kW–3 MHz rf (radio frequency) induction plasma torch. We investigate these materials for so…
We have studied the effect of heat treatment on the magnetic properties and on the martensitic transition of the Ni50Mn30Al20 alloy. A mixed L21+B2 state is obtained in the as-prepared sample, while no L21 order is retained in the sample quenched from high temperature. For the two heat treatments, the samples order an…
We present the design and application of a movable collimated gas source of atomic and molecular species that allows the accurate determination of background-scattered electrons in beam–beam, low-energy electron scattering experiments. Our method provides a very simple solution for accurate background determination wi…
Abstract A new trifluoromethyl‐substituted bis(ether amine) monomer, 2,7‐bis(4‐amino‐2‐trifluoromethylphenoxy)naphthalene, was synthesized. It led to a series of novel fluorinated polyimides by thermal and chemical imidization routes when reacted with various commercially available aromatic tetracarboxylic dianhydride…
Highly Cr-doped II–VI diluted magnetic semiconductor (DMS) Zn1−xCrxTe films with a ferromagnetic long-range order have been grown. A phase diagram of Zn1−xCrxTe in relation to the growth temperature and Cr concentration was determined. Magnetic circular dichroism measurements revealed that a magnetically single phase…
Effects of the interstitial carbon atoms on the magnetic properties, especially on the magnetic entropy change, of the LaFe11.5Si1.5 compound, have been studied. X-ray diffraction patterns reveal a monotonous increase of the lattice constant with the concentration of carbon, while the cubic NaZn13-type structure remai…
Self-organized Co/Pt nanoparticulate arrays offer a novel approach to fabricating magnetic recording media with the potential for supporting Terabit/in.2 recording densities. Protein-derived Co/Pt nanoparticles are prepared within apoferritin from aqueous reactants, with synthesis conditions controlling grain size, st…
NiFe 2 O 4 ultrafine powder with high crystallinity has been prepared through a reverse microemulsion route. The composition in starting solution was optimized, and the resulting NiFe2O4 was formed at temperature of around 550–600 °C, which is much lower than that observed from the solid-state reaction. Magnetic inves…