Materials Literature
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The dealloying of β-brass in 0.5 M aqueous NaCl was studied by electrochemical techniques at different temperatures in the range 278 K ≤ T ≤ 318 K, complemented with in situ scanning tunneling microscopy (STM) imaging. In the potential region where the electrodissolution of zinc and the formation of vacancies and copp…
Critical settings and their effects on the properties of open-end cover spun yams produced by a novel system are explained. The yams are constructed from open-end rotor spun (OER) yarns and textured polyester yarns combined within the yarn formation zone of the rotor during the open-end rotor spinning process. The end…
The antiferroelectric liquid crystal (AFLC) under investigation possesses different helical polar phases. Measurements of pyroelectric response of these phases as a function of temperature and bias field have elucidated the ability of this method for investigating the nature of antiferroelectric phases and phase trans…
Grain-boundary grooving has been studied on polished surfaces of polycrystalline tungsten annealed at 1350°C. Atomic force microscopy images were taken in the same area for each groove after different annealing times. Secondary oscillations next to the main groove maxima (predicted for grooving by surface diffusion) w…
Typical measurements of macromolecular crystal mosaicity are dominated by the characteristics of the X-ray beam and as a result the mosaicity value given during data processing can be an artifact of the instrumentation rather than the sample. For physical characterization of crystals, an experimental system and softwa…
Peripheral modification of the porphyrazine macrocycle is an important synthetic approach to β-substituted porphyrazine derivatives, especially those which cannot be obtained via direct template cyclotetramerization of maleodinitriles and other similar synthons. The paper presents the last results of the systematical…
Some properties of rare earth orthophosphates have been determined by means of synthesis, X-ray diffraction, infrared absorption spectra, and Raman spectra measurements. The results are: (1) a synthesis of new compounds GdPO4.2H2O weinschenkite type, (2) the salt readily lost its water and changed from the weinschenki…
We study the spectral width as a function of the external momentum for the dynamical structure factor of a disordered harmonic solid, considered as a toy model for supercooled liquids and glasses. In the contexts of both the single-link coherent potential approximation and a single-defect approximation, two different…
Recently published Monte Carlo simulation studies have demonstrated that carbon nanotubes could be a new adsorbent material for the storage of gases such as hydrogen. This engineering application suitable for the use of hydrogen in fuel cells has motivated much experimental and theoretical work, including the present…
Polymalatase from Physarum polycephalum calalysed the hydrolysis of beta-poly[L-malate] and of the synthetic compounds beta-di(L-malate), beta-tetra(L-malate), beta-tetra(L-malate) beta-propylester, and L-malate beta-methylester. Cyclic beta-tri(L-malate), cyclic beta-tetra(L-malate), and D-malate beta-methylester wer…
In-situ gas-phase Fourier transform infrared spectroscopy (FTIR) studies of thermally activated processes occurring in the metal–organic chemical vapor deposition (MOCVD) of La(hfac)3·diglyme provide evidence that the precursor can be evaporated from the melt up to 130 °C without side decomposition processes. In contr…
Abstract Polypropylene (PP) blends, commercially known as “impact polypropylene copolymers” (IPC), are produced by a sequential gas phase polymerization process. The final product is a complex mixture of polypropylene (PP) and a range of ethylenepropylene copolymers (EPC) with different ethylene contents. In the prese…
Partial modification of the nonionic polymer poly(N-2-hydroxy-propylmethacrylamide) by cinnamate produces stimuli-responsive copolymers. The hydrophobic character of the cinnamate chromophore induces not only a lower critical solution temperature (LCST) in water, but renders additionally the polymers photoresponsive.…
This contribution is concerned with the exceptionally strong influence of smectic mesophase formation on the optically induced orientation and on the surface relief grating formation in a liquid crystalline melamine derivative containing azobenzene groups. We demonstrate that the strong amplification of optically indu…
Reaction of sodium azide with manganese(II) and diethylnicotinamide (DENA) leads to the two-dimensional system trans-[Mn(DENA)2(N3)2]n. The compound crystallises in the P2/c (monoclinic) group. Structural determination shows layers of manganese atoms bridged by means of single µ1,3-azido bridges. The polymeric structu…
We studied various types of surface treatments for magnesium alloys that involved the application of chromium or manganese by measuring their corrosion potential using X-ray diffraction, X-ray photoelectron spectroscopy, auger electron spectroscopy, and microscopic examination. The chromium-conversion coating is compo…
This paper theoretically analyzes the hydrodynamic shape stability problem for sonoluminescing bubbles. We present a semianalytical approach to describe the evolution of shape perturbations in the strongly nonlinear regime of violent collapse. The proposed approximation estimating the damping rate produced by liquid v…
Formability on cylindrical deep drawing and mechanical properties at relatively low temperature was investigated for a commercially rolled AZ31 magnesium. A small punch radius, which ratio to thickness was 2.5, was adoped intentionally. At room temperature, brittle fracture occurred near the flat portion of punch shou…
SAN containing 20 wt % of reactive SAN-X has been melt blended with EPDM containing 50 wt % of EP chains grafted by maleic anhydride (EP- g -MA). Two types of reactive groups (X) have been attached to SAN (2 mol % of X), i.e., a primary amine and a precursor of it at the processing temperature, i.e., a carbamate. The…
The electronic situation of boron atom frameworks in boron-rich solids is not easy to understand. Attempts to describe such compounds according to known bonding theories such as the Lipscomb or Zintl−Klemm approaches, are not completely unambiguous. To gain further insight and to create a solid experimental basis for…