Materials Literature
按标题、摘要、年份、主题和来源检索公开元数据。结果保留作者、摘要、分类与原始来源链接。
A novel plasma beam source for the deposition of DLC films is described. Wide ranges of ion energy (130-250 eV) and C/sub 2/H/sub 2//N/sub 2/ flow conditions have been used to investigate the effect of N doping an the structure and properties of DLC films. The resulting films are characterized by their chemical compos…
Two series of alicyclic polyimides composed of cis- and trans-dicyclohexyl-3,3′,4,4′-tetracarboxylic dianhydrides (DCDAs) and aromatic diamines were prepared. All cis-polymers could be readily prepared both in a one-step method and a two-step method. However, a two-step method is preferably applied in the preparation…
Highly ordered nanoporous Co membranes were fabricated by a two-step replication from the honeycomb structure of porous anodic alumina. These metal membranes are confirmed to have two substructures: first, the Co membrane consists of very fine quantum-sized particles with diameters of about 2–5 nm; second, the very fi…
This work reports survey and core level x-ray photoemission spectra obtained from the surface of a barium sulfate powder. The high purity (99.998%) barium sulfate specimen was commercially obtained from Alfa/AESARS. The XPS spectra were acquired with a Kratos Axis 165 instrument using monochromatic Al Kα radiation. Th…
Nach Guinier-Simon-Untersuchungen ist Kaliumtrifluormethylsulfonat dimorph, mittels DSC wird eine Umwandlungstemperatur von –33 °C und eine Umwandlungsenthalpie von 0.93 ± 0.03 kJ/mol ermittelt. Im Beugungsexperiment erstreckt sich die Phasenumwandlung in die Tieftemperaturmodifikation über einen Temperaturbereich von…
For the insulation diagnosis of gas-insulated switchgear (GIS), it is necessary to detect partial discharge (PD) under noisy conditions and to specify the direction of electromagnetic wave radiation due to PD. We propose the "phase gate control method" for discriminating the electromagnetic waves caused by PD in SF6 g…
A simple thermomechanical model is applied to evaluate the influence of the nonuniformity of ZnO varistor disks used in surge arresters on their energy-handling capability. Puncture is the dominating failure mode for slightly nonuniform disks, but cracking becomes more likely as the degree of nonuniformities increases…
Young’s modulus and Poisson’s ratio of SiC ceramics at temperatures >1400°C were obtained using a laser ultrasonics method that included a Fabry‐Pérot interferometer (LUFP). At temperatures <1000°C, Young’s modulus and Poisson’s ratio measured using the LUFP method agreed well with those measured using standard…
Amounts of trace elements with large activation cross section in concrete materials were measured to offer the basic data for developing of low activation concrete. From the measurements, the quantities of the activated radioactivities in biological shielding concrete were measured and evaluated for the clearance leve…
2-methyl benzoazole and 2-mercapto benzoazole derivatives were investigated as corrosion inhibitors for Type 304 (UNS S30400) stainless steel in 2 M sulfuric acid (H2SO4) solution using weight loss, gasometry, and alternating current (AC) impedance techniques. Effect of immersion time and temperature were studied. The…
We have studied the relative rates of oxidative corrosion of U–Nb alloys containing 2–8 wt. % Nb, using x-ray photoelectron spectroscopy and depth profiling by sputtered neutrals mass spectroscopy. The alloys have been characterized after exposure to dry and humidified air (up to 50% relative humidity) at temperatures…
We characterize the local Li structure in the low-temperature phase of LixC60 with 6⩽x⩽15 using single and multiple-quantum Li7 nuclear magnetic resonance spectroscopy. We find clear evidence for Li cluster intercalated structures in all compositions. The inferred cluster sizes are significantly smaller than those sug…
XPS spectra are reported for a well-ordered Ni2P (0001) surface. These are the first reported photoemission spectra for this transition metal phosphide in single crystal form. Ion bombardment and annealing produces an ordered surface.
Abstract Rietveld refinement and the final model for pure κ -alumina are presented. The starting model was obtained through total energy calculations based on first principles. The resulting geometry parameters are within intervals of expected values for octahedral and tetrahedral coordina-tions. This result thus serv…
Abstract Measurements of the contact angle for water, glycerol, formamide, ethylene glycol, and diiodomethane on polymethyl methacrylate covered by adsorptive bovine serum albumin (BSA) films were made. Adsorption was performed from solutions in the concentration range 0–100 g/L. From the obtained contact angles the L…
Abstract In‐depth imaging of subsurface structures in scanning electron microscopy (SEM) is usually obtained by detecting backscattered electrons (BSE). For a layer‐by‐layer imaging in BSE microtomography, it is preferable to use an energy filtering of BSE. A simple approach is used to estimate the contrast by using b…
Solid state thin film batteries with MoO 3- x films as their cathode active material exhibit good battery performance. The chemical composition of the MoO 3- x thin film has been difficult to determine by chemical analysis, because of the difficulty in weighing ultra light samples located on massive substrates. To sur…
The beamline BL43IR at SPring-8 has been constructed as a beamline exclusively dedicated to the infrared spectroscopy. The beamline was designed to make use of infrared synchrotron radiation emitted from a bending magnet of 39.3 m bending radius with the acceptance angle of 36.5(H)×12.6(V) mrad2 and to cover a very wi…
Ultrafine Ni/sub 0.63/Zn/sub 0.17/Cu/sub 0.2/Fe/sub 2/O/sub 4/ powders and thin films were fabricated by a sol-gel method and their magnetic and structural properties were investigated with thermogravimetric and differential thermal analysis (TG-DTA), X-ray diffractometer (XRD), transmission electron microscope (TEM),…
Magnetic properties of new intermetallics FeVSn and CoVSn are reported. Both materials belong to the group of semi-Heusler compounds, with lattice parameters of 0.593 and 0.598 nm respectively in a cubic MgAgAs structure. X-ray investigations indicate partial atomic ordering in both cases. Ferromagnetic order was obse…