Materials Literature
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Abstract The polymerization of metal salts of N ‐chloroacetyl‐ β ‐alanine and N ‐chloroacetyl‐4‐aminobutyric acid was investigated. The former gives a mixture of polymer and a seven‐membered cyclic compound constituted of glycolic and β ‐alanine units, and its reaction proceeds in the solid state. However, liquefactio…
Abstract Due to a nanotechnology boom in science and technology, the metal nanoclusters or nanoparticles stabilized by polymers and organic ligands have achieved much attention recently all over the world. We have studied on the preparation of polymer‐stabilized metal nanoclusters by chemical methods, and applied them…
Abstract The formation of inclusion complexes of well‐known 1,4‐dihydropyridine calcium antagonists, such as nifedipine (NF) and nicardipine (NC), with β‐cyclodextrin (βCD) was investigated by differential pulse polarography (DPP) and UV‐vis spectrophotometry. The equimolar variation method indicated the formation of…
We present a method for synthesizing insulator-coated carbon nanotubes by pulsed laser deposition. Isolated multi-walled carbon nanotubes (MWNTs) were coated with an SiO x thin layer in a multishell form. The product showed that a stoichiometric SiO 2 thin layer was uniformly wrapped around a MWNT, and reflected the s…
Substantial amounts of self-boiling, Al-rich, hyperalkaline, and saline high-level waste fluids (HLWF) were deposited to the vadose zone at the Hanford Site, in Washington State. The objective of this study was to investigate the effects of similar fluids on the extent of dissolution and precipitation in the sediments…
The effect of yarn hairiness on energy consumption when rotating a ring-spun yarn package is investigated theoretically and experimentally. A theoretical model is developed to calculate the energy required to rotate hair fibers, based on hair length and number as well as package speed and size. A single spindle test r…
A 2 cm long and 0.8 cm thick, single graphite crystal embedded in quartz, feldspar, and orthopyroxene of a granulite-facies metamorphic rock from southern India exhibits unique homogeneity in δ 13 C values along layers parallel to the (0001) surface and smooth unidirectional variation of about 1‰ along the c-crystallo…
Abstract N ‐(2‐Hydroxypropyl)methacrylamide (HPMA) copolymer‐linked nitroxides were synthesized as macromolecular contrast agents for MR imaging. Molar relaxivities of HPMA copolymer‐linked nitroxides increased linearly in proportion to the number of nitroxides attached per gram of copolymer. HPMA copolymer‐linked nit…
We propose a new magnetic force control device, composed of a giant magnetostrictive material (Terfenol-D) and a piezoelectric material (PZT), for coilless magnetic force control. The device uses the inverse magnetostrictive effect, whereby the variation of magnetization of a Terfenol-D rod controlled by PZT is conver…
Abstract Acrylonitrile-butadiene-styrene terpolymer (ABS) is one of the engineering plastics most frequently used as outer casings for computer equipment such as monitors, keyboards and other similar components. In an attempt to recycle, blends of scrap computer plastics (SCP) based on ABS with nitrile rubber (NBR) we…
This paper reports an analysis of the influence of polyester and yarn type on the abrasion resistance of 50/50 wool/polyester blended woven fabrics. Recently developed polyester fibers put into the blend and two-strand Sirospun yams are compared with 2.5 denier standard polyester and two-fold ring yarns. Mass losses o…
Abstract A large distribution coefficient and large sorption capacity were observed during selenate adsorption by cation (Fe3+, Cu2+, and H+)-anchored diamino-functionalized MCM-41. Moreover, these synthetic adsorption media showed excellent selectivity for selenate sorption in the presence of other anions. In a pure…
The mechanical, structural, and dyeing properties of solvent-spun lyocell fibers in a plain weave fabric are studied before and after industrial treatments of mechanical fibrillation and enzymatic defibrillation. Stress-strain relationships, surface morphology, crystallinity, and dye uptake are assessed for each of th…
Three Ru2(5+) diruthenium complexes, (4,0) Ru2(2-CH3ap)4Cl, (3,1) Ru2(2-Fap)4Cl, and (3,1) Ru2(2,4,6-F3ap)4Cl where ap is the 2-anilinopyridinate anion, were examined as to their electrochemical and spectroelectrochemical properties in five different nonaqueous solvents (CH2Cl2, THF, PhCN, DMF, and DMSO). Each compoun…
We have used deposited polymeric nanofibers as nonlithographic templates for the fabrication of semiconductor nanostructures. We deposited oriented poly(methyl methacrylate) (PMMA) fibers, with diameters ranging from 85 to 350 nm, on the surface of various substrates using a microfabricated electrospinning source. By…
Abstract The reinforcing effect of up to 6 parts per hundred rubber by weight (phr) bis- (3-triethoxysilylpropyl) tetrasulfide (TESPT), a bifunctional organosilane, on the crosslink density, bound rubber, and technical properties of some conventional accelerator/sulfur compounds of natural rubber, containing 30 phr pr…
Alacranite from the type locality (Uzon caldera, Kamchatka, Russian Federation) was submitted for structural analysis. A single crystal was selected and the following lattice parameters were determined: a = 9.942(4), b = 9.601(2), c = 9.178(3) Å, β = 101.94(3)°, V = 857.1 (5) Å 3 . The crystal structure was solved in…
The sliding interface of a flyer/target system is subject to immense forces caused by dynamic loads and impact of the flyer with the target. In addition, tremendous heating caused by aerodynamic and frictional effects is produced at the interface. The buildup of the temperature caused by external heat sources is impor…
Gray-scale electron beam lithography has been used to create high-efficiency (63%, output normalized) blazed gratings suitable for use at extreme ultraviolet (EUV) wavelengths (i.e., 13.4 nm). The total blaze height at these wavelengths is ≈7 nm. The surface topography was generated in a single processing step in hydr…
The interactions of two pyridoxal-5-phosphate (PLP)-dependent enzymes, alanine aminotransferase (ALT) and glutamate decarboxylase (GAD), with pyridoxal kinase (PK) were studied by fluorescence polarization as well as surface plasmon resonance techniques. The results demonstrated that PK can specifically bind to ALT an…