Materials Literature
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We report neutron diffraction data on single crystal ${\mathrm{PrO}}_{2}$ which reveal a cooperative Jahn-Teller distortion at ${T}_{\mathrm{D}}=120\ifmmode\pm\else\textpm\fi{}2\phantom{\rule{0.2em}{0ex}}\mathrm{K}$. Below this temperature an internal distortion of the oxygen sublattice causes the unit cell of the cry…
Formation of colloids based on polyelectrolyte complexes (PECs) was mainly studied with synthetic polyelectrolytes. In this study, we describe the elaboration of positively charged PEC particles at a submicrometer level obtained by the complexation between two charged polysaccharides, chitosan as polycation and dextra…
The low-energy part of the vibration spectrum in KNbO$_3$ was studied by cold neutron inelastic scattering in the cubic phase. In addition to acoustic phonons, we observe strong diffuse scattering, which consists of two components. The first one is quasi-static and has a temperature-independent intensity. The second c…
We report initial NMR studies of gas dynamics in a particle bed fluidized by laser-polarized xenon (129Xe) gas. We have made preliminary measurements of two important characteristics: gas exchange between the bubble and emulsion phases; and the gas velocity distribution in the bed. We used T2* contrast to differentiat…
A general spin symmetry argument is proposed for spin currents in semiconductors. In particular, due to the symmetry with respect to spin polarization of the helicity eigenstates of the Luttinger Hamiltonian for a hole-doped semiconductor, the spin polarized flux from a single helicity eigenstate induced by an externa…
In this work we present measurements of permeability, effective porosity and tortuosity on a variety of rock samples using NMR/MRI of thermal and laser-polarized gas. Permeability and effective porosity are measured simultaneously using MRI to monitor the inflow of laser-polarized xenon into the rock core. Tortuosity…
Using a first-principles-based approach, we determine the ferroelectric pattern in PbZr$_{0.5}$Ti$_{0.5}$O$_3$ ultrathin film. It is found that vortex stripes are formed in the system and they are responsible for the 180$^\circ$ domains observed. When a local external field is exerted, the vortex stripe transforms int…
Mechanical properties of polyelectrolyte multilayer films were studied by nanoindentation using the atomic force microscope (AFM). Force-distance measurements using colloidal probe tips were systematically obtained for supported films of poly(L-lysine) and hyaluronan that are suited to bio-application. Both native and…
The structural evolution and crystallization dynamics of poly( l -lactide) (PLLA) during isothermal cold-crystallization process are studied by infrared (IR) spectroscopy and two-dimensional correlation analysis. In the C O stretching region, the band shift to a higher wavenumber taking place during the crystallizatio…
Thermal decomposition of the molecular single-source precursor (PPh 3 ) 2 CuIn(SEt) 4 in the presence of hexanethiol in dioctylphthalate forms colloidal CuInS 2 at 200 °C. The colloidal solution displays size-dependent quantum confinement behavior in the absorption and photoluminescence spectra. The average size of th…
Preface. List of Contributors. Polymer Brushes: On the Way to Tailor-Made Surfaces (Jurgen Ruhe). 1 Growth of Polymer Molecules at Surfaces: Introductory Remarks. 2 Coatings: First Principles to High-Tech Applications. 3 Surface-Coating Techniques. 4 Surface-Attached Polymers. 5 Polymer Brushes: General Features. 6 Th…
We report on the use of dopamine (DA) as a robust molecular anchor to link functional molecules to the iron oxide shell of magnetic nanoparticles. Using nitrilotriacetic acid (NTA) as the functional molecule, we created a system with an M/Fe2O3-DA-NTA (M = Co or SmCo5.2) nanostructure, which possesses high stability a…
Abstract The hydrothermal ageing of wood‐flour‐filled PVC produced by dry‐blending in a high‐speed mixer in the presence of a plasticizer and other processing additives was carried out to investigate its thermal behaviour, and the results obtained were compared with those for the unfilled material. The dry‐blended com…
This investigation was carried out in order to evaluate ammonium hydrogen fluoride (AHF) and cupric chloride (CC) as components of a metal etchant. The surface of cast titanium-aluminum-niobium (Ti-6Al-7Nb) was air-abraded with alumina, etched for 10 s, and rinsed with water. A phosphate or a thiophosphate primer was…
Abstract In attempt to improve the properties of polyanhydrides based on aliphatic anhydrides, we synthesized novel polyanhydrides containing amide groups in the main chains. In this work, N , N ′‐bis( L ‐alanine)‐sebacoylamide (BSAM) was prepared from natural amino acid and sebacic acid (SA) and characterized by IR a…
Abstract In this paper, the isothermal crystallization of nylon 6 in the presence of Kevlar 129 fiber was investigated by polarized optical microscopy (POM). The formation of a transcrystalline domain was found to be mainly controlled by crystallization conditions, such as the temperature of the isothermal crystalliza…
Abstract Random crystalline–amorphous copolymers containing ethylene and butene segments, yielded from dilute‐solution, and self‐assembled to one‐dimensional, needle‐shaped aggregates, can modify wax crystal structures through the cocrystallization of the copolymer and wax molecules into hairy platelets. These copolym…
Abstract A series of optically active poly(ester imide)s (PEsI's) has been synthesized by the polycondensation reactions of new axially asymmetric dianhydrides, that is, ( R )‐2,2′‐bis(3,4‐dicarboxybenzoyloxy)‐1,1′‐binaphthyl dianhydride and ( S )‐2,2′‐bis(3,4‐dicarboxybenzoyloxy)‐1,1′‐binaphthyl dianhydride, and vari…
This study presents the status and results from an effort to design, fabricate, and test an adaptive jet engine chevron concept based upon embedding shape memory alloy (SMA) actuators in a composite laminate, termed a SMA hybrid composite (SMAHC). The approach for fabricating the adaptive SMAHC chevrons involves embed…
Abstract A novel template-free solvothermal route was successfully designed to fabricate single-crystal vertically aligned CdS nanowire array, and its field emission property for the first time, was studied. The relatively high emission current density and low turn-on field make the CdS nanowire array one of the promi…