Materials Literature
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The effects of irradiation up to 20 dpa on the Charpy impact properties of reduced-activation ferritic/martensitic steels (RAFs) were investigated. The ductile-brittle transition temperature (DBTT) of F82H-IEA shifted up to around 323K. TIG weldments of F82H showed a fairly small variation on their impact properties.…
A forced‐flow reactor has been designed for the synthesis of nanocrystalline AlN via in situ and ex situ nitridation of aluminum. Various reactor parameters, including evaporation temperature, microwave plasma generation, reactor pressure, gas flow rate, nitriding gas, carrier gas, and crucible purge, have been examin…
Abstract Diffusion measurements of metallic and semiconductor melts on earth show highly irreproducible results due to occurrence of unknown convection. Therefore we investigated the influence of different kinds of additional transports. Diffusion experiments with the shear cell technique and numerical simulations hav…
We present a way to fabricate microgrippers that can meet the industry's needs well, i.e., low cost and large tip deflection, etc. The microgripper is fabricated by bonding two identical micro NiTi-Si cantilever beams together with a silicon spacer in between. It can be actuated by electrical current directly. We have…
Detailed power loss distribution in induction machines is assessed using time-stepped finite-element analysis coupled to circuit equations of an inverter. Losses are examined for various load conditions. Iron losses are largely unexplored and so particular attention is paid to them here. The simulation has revealed th…
In experimental mass spectra of lead-sodium mixed clusters, an exceptionally abundant and stable ${\mathrm{Na}}_{6}\mathrm{Pb}$ cluster has been discovered [C. H. Yeretzian et al., Chem. Phys. Lett. 237, 334 (1995)]. By using first-principles calculations, several cluster assemblies based on the ${\mathrm{Na}}_{6}\mat…
Amphiboles were hydrothermally synthesized at 500 °C and 4 kbar in the system Li 2 O-Na 2 OFeO- Fe 2 O 3 -SiO 2 -H 2 O, with nominal compositions along the riebeckite [□Na 2 Fe 3 2+ Fe 2 3+ Si 8 O 22 (OH) 2 ]-ferri-clinoferroholmquistite [□Li 2 Fe 3 2+ Fe 2 3+ Si 8 O 22 (OH) 2 ] join, where the exchange vector is NaLi…
In this paper we report the effects of formulation on texture development for the “reactive‐templated grain growth” (RTGG) of Bi 1/2 (Na,K) 1/2 TiO 3 (BNKT). The solids formulation for BNKT was systematically varied by prereacting to well—defined alkali and bismuth titanates (Na 2 Ti 3 O 7 (N 2 T 3 ), K 2 Ti 2 O 5 (K…
Abstract Pitting of stainless steels in environments normally regarded as completely harmless is often attributed to microbial activity. In this paper, attention is drawn on one hand to the basic requirements for pitting of stainless steels to be possible, and on the other hand to various ways how microbial activity c…
Abstract The simultaneous biaxial deformation behavior of isotactic polypropylene films was investigated using a novel laboratory film stretcher. A detailed description of the apparatus and its measurement capabilities is presented. The effects of drawing temperature and ratio, strain rate, and deformation modes on th…
A new thiospinel CuCrZrS4 has been successfully synthesized by a solid-state chemical reaction. This CuCrZrS4 exhibits ferromagnetic properties below the Curie temperature at T c = 60 -2 K. The appearance of irreversible effect between field-cooled and zero-field-cooled magnetization is prominent below around 5 K in a…
The goal of this paper is to derive a micromechanics framework to study the kinetics of transformation due to interface migration in elastic-plastic materials. Both coherent and incoherent interfaces as well as interstitial and substitutional atomic diffusion are considered, and diffusional transformations are contras…
Porous CaZrO 3 /MgAl 2 O 4 composites were synthesized in air by pressureless reactive sintering of an equimolar mixture of dolomite (CaMg(CO 3 ) 2 ), monoclinic zirconia ( m ‐ZrO 2 ), and α‐alumina powders, with a 0.5 wt% lithium fluoride additive. The reaction behavior of the mixed powders (with/without LiF additive…
Abstract Eu 2 SnS 4 , Sr 2 SnS 4 , and Sr 2 GeSe 4 have been synthesized by heating the elements or binary precursors at 1073 K and their crystal structures were determined by single crystal methods. Eu 2 SnS 4 crystallizes with a new structure type ( Pnma , a = 11.187(2), b = 8.768(2), c = 7.538(2)Å, Z = 4), consisti…
The gene encoding a deoxyriboaldolase (DERA) was cloned from the chromosomal DNA of Klebsiella pneumoniae B-4-4. This gene contains an open reading frame consisting of 780 nucleotides encoding 259 amino acid residues. The predicted amino acid sequence exhibited 94.6% homology with the sequence of DERA from Escherichia…
The corrosion resistance and galvanic behavior of three stainless steels (SS), Alloy 33, and titanium were analyzed in commercial lithium bromide (LiBr) heavy brine solutions used in heating and refrigerating systems, with and without additives, using potentiodynamic anodic polarization measurements. Corrosion rates w…
Human osteoblast-like (bone-forming) cells were imaged using environmental scanning electron microscopy (ESEM). The cells were hydrated, unfrozen, and uncoated. Specimens were cooled to 3 degrees C and imaged in water vapor, with partial pressures varying from saturated conditions to a humidity of approximately 50%, r…
Abstract The hexacoordinate silicon(IV) complexes [NEt 4 ] 2 [Si(NCS) 6 ] ( 2 ), [K(18‐crown‐6)] 2 [Si(NCS) 6 ]·2CH 3 CN ( 3· 2CH 3 CN), and cis ‐[(acac) 2 Si(NCS) 2 ] ( cis ‐ 4 ; acac = acetylacetonato‐ O , O ) were synthesized, starting from Si(NCS) 4 ( 1 ). Compounds 1 , 2 , 3· 2CH 3 CN, and cis ‐ 4 were structural…
We have applied supercritical CO 2 drying technique to fabricate free-standing semiconductor nanotubes, in order to solve the problem of tube collapsing caused by the capillary forces in the final drying process. We have successfully fabricated damage-free single-turn nanotubes with ultra-thin walls (lesser than 3 nm)…
Abstract This is the first of two parts investigating the Flory‐Huggins interaction parameter, χ , as a function of composition and chain length. Part 1 encompasses experimental and theoretical work. The former comprises the synthesis of poly(dimethylsiloxane)s with different molar mass and the measurements of their s…