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Effect of pH of Medium on Hydrothermal Synthesis of Nanocrystalline Cerium(IV) Oxide Powders

Nanchun Wu、Er‐Wei Shi、Yanqing Zheng 等 4 位作者2002-10-01Journal of the American Ceramic Society

Well‐crystallized cerium(IV) oxide (CeO 2 ) powders with nanosizes without agglomeration have been synthesized by a hydrothermal method in an acidic medium by using cerium hydroxide gel as a precursor. The relationship between the grain size, the morphology of the CeO 2 crystallites, and the reaction conditions such a…

Catalytic Processes in Materials ScienceAdvanced Nanomaterials in CatalysisCopper-based nanomaterials and applications

Surface Characterization of CeO2/SiO2 and V2O5/CeO2/SiO2 Catalysts by Raman, XPS, and Other Techniques

Benjaram M. Reddy、Ataullah Khan、Yusuke Yamada 等 6 位作者2002-10-01The Journal of Physical Chemistry B

X-ray diffraction, Raman, and X-ray photoelectron spectroscopy were utilized to characterize CeO 2 /SiO 2 supports and V 2 O 5 /CeO 2 /SiO 2 catalysts calcined at different temperatures from 773 to 1073 K. The CeO 2 /SiO 2 support was obtained by an aqueous deposition precipitation method, and vanadium oxide was appli…

Radioactive element chemistry and processingCatalysis and Oxidation ReactionsCatalytic Processes in Materials Science

Viability of pHEMA Hydrogels as Coating in Human Synovial Joint Prosthesis

V.P. Bavaresco、C.A.C. Zavaglia、S.M. Malmonge 等 4 位作者2002-10-01Materials Research

In artificial joints, the bone part is usually substituted by a metallic component with high corrosion and strength resistance while the articular cartilage is replaced by a polymer. Use of thin layer of a compliant material acting as a bearing surface in human replacement joints has recently generated considerable in…

Influence of the Testing Gage Length on the Strength, Young's Modulus and Weibull Modulus of Carbon Fibres and Glass Fibres

Luiz Claudio Pardini、Luis Guilherme Borzani Manhani2002-10-01Materials Research

Carbon fibres and glass fibres are reinforcements for advanced composites and the fiber strength is the most influential factor on the strength of the composites. They are essentially brittle and fail with very little reduction in cross section. Composites made with these fibres are characterized by a high strength/de…

N2 and CO2 Adsorption by TMA- and HDP-Montmorillonites

C. Volzone、J.O. Rinaldi、J. Ortiga2002-10-01Materials Research

N2 and CO2 gases adsorption by tetramethylammonium(TMA)-montmorillonites and hexadecylpyridinium(HDP)-montmorillonites was carried out using volumetric equipment at 25 °C and 0.1 MPa. The addition of organic compounds to montmorillonites was 1 and 4 times the cation exchange capacity (CEC) of the montmorillonites and…

Clay minerals and soil interactionsMesoporous Materials and CatalysisMembrane Separation and Gas Transport

Evaluation of Adherence and Performance of Epoxyphenolic Coatings on Electrolytic Tinplates

Ε. Zumelzu、F. Rull2002-10-01Science and Engineering of Composite Materials

Article Evaluation of Adherence and Performance of Epoxyphenolic Coatings on Electrolytic Tinplates was published on October 1, 2002 in the journal Science and Engineering of Composite Materials (volume 10, issue 5).

Recycling and Waste Management TechniquesSynthesis and properties of polymersElectrophoretic Deposition in Materials Science

Calibration of a Commercial Kneader for Rheological Applications

Kealy Tim、Tiu Carlos2002-10-01Applied Rheology

In the case of some highly viscous fluids, or thick pastes (such as those exhibiting high yield stress and/or high plastic viscosity), neither rotational nor tube type viscometers are suitable for rheological characterisation. Due to their capacity for generating and maintaining high torque or high rates of rotation,…

Thermal Expansion and Oxidation of 3D C/SiC Composites with Different Coatings from Room Temperature to 1400°C

Laifei Cheng、Yongdong Xu、Litong Zhang 等 4 位作者2002-10-01Science and Engineering of Composite Materials

Article Thermal Expansion and Oxidation of 3D C/SiC Composites with Different Coatings from Room Temperature to 1400°C was published on October 1, 2002 in the journal Science and Engineering of Composite Materials (volume 10, issue 5).

Additive Manufacturing and 3D Printing TechnologiesAdvanced materials and compositesAdvanced ceramic materials synthesis

Thermodynamic Evaluation of Carbide Precipitates in 2.25Cr¾ 1.0Mo Steel for Determination of Service Degradation

Bojan A. Marinkovic、Roberto R. de Avillez、Simone Kessler Barros 等 4 位作者2002-10-01Materials Research

The 2.25Cr¾1.0Mo steel is widely used in petroleum refining units, for example, in pressure vessels, working under severe operational conditions. Due to the high temperatures of some processes, many phenomena such as precipitation of carbides and their coarsening occur during service, resulting in changes of material…

Numerical Studies of the Effect of Constitutive Model Parameters as Reflecting Polymer Molecular Structure on Extrudate Swell

Nithi-Uthai Nattapong、Manas-Zloczower Ica2002-10-01Applied Rheology

PolyFlow, a software package based on the finite element method was employed to simulate the extrudate swell for polybutadiene of various molecular weight (Mw) and molecular weight distribution (MWD). We calculated the relaxation spectra for the different samples and then inserted the spectra into a standard K-BKZ con…

Woodflour as Reinforcement of Polypropylene

José Cláudio Caraschi、Alcides Lopes Leão2002-10-01Materials Research

The effect of the filler content and size, as well as accelerated aging on the mechanical properties of polypropylene composites reinforced with woodflour (WF/PP) were evaluated. The composites were prepared by the extrusion of polypropylene with woodflour (Pinus elliotti) based on following ratios: 15, 25 and 40 wt%…

Polymer Foaming and CompositesNatural Fiber Reinforced CompositesPolymer Nanocomposites and Properties

Linear Viscoelastic Behavior of Bentonite-Water Suspensions

Bekkour Karim、Kherfellah Nadia2002-10-01Applied Rheology

Bentonite are extensively used materials in a wide range of applications. Creep and oscillatory shear experiments in the linear viscoelastic domain were carried out on bentonite-water suspensions at different solid fractions. It was found that bentonite dispersions exhibit important viscoelastic behavior which could b…

Synthesis of Titania-Silica Materials by Sol-Gel

R. F. S. Lenza、Wander L. Vasconcelos2002-10-01Materials Research

In this work TiO2-SiO2 glasses containing as much as 20 mol % of TiO2 were prepared via sol-gel process using titanium and silicon alkoxides, in the presence of chlorine, in the form of titanium tetrachloride or HCl. The gels were heat-treated until 800 °C. X-ray diffraction and Fourier transform infrared spectroscopy…

Glass properties and applicationsMesoporous Materials and CatalysisCatalysis and Oxidation Reactions

Effect of the Addition of Potassium or Lithium on the Columbite Precursor Microstructure

Alberto A. Cavalheiro、Maria A. Zaghete、Carlos O. Paiva-Santos 等 4 位作者2002-10-01Materials Research

Pechini method has been used to synthesize MN powders with stoichiometric control. By this method, K and Li-doped MN in the range from 0.1 to 5.0 mol% of dopants have been obtained at relatively lower temperatures than it is possible with the conventional mixture of oxides. The results from BET analysis indicated that…