Materials Literature
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The isothermal crystallization of poly(L‐lactide) (PLLA) under steady‐shear flow was investigated in situ using an optical polarizing microscope with a hot shear stage. The steady–shear‐induced crystalline morphology of PLLA, to a great degree, depends on the crystallization temperature. There is a critical temperatur…
Four kinds of novel zigzag boron-carbon nanotubes with quasi-planar tetracoordinate carbons (2m, 0, i) (m = 3-6; i = 1-4) have been constructed, and their structures, stabilities, and bonding properties have been investigated by B3LYP calculations. The results show that the novel nanotubes (m, 0, i) have the character…
Abstract The thermal expansion behavior of a cyanate ester matrix reinforced by fumed silica nanoparticles with average primary particle diameters of 12 and 40 nm was investigated with thermomechanical analysis. All nanocomposites showed decreased coefficients of thermal expansion (CTEs) in comparison with the neat bi…
Nanosized β-SiC powder was prepared by combustion synthesis on a large scale, which was carried out in a N 2 atmosphere with silicon powder and carbon black as the reactants. Mechanical activation played an important role in enhancing the reactivity of the reactants, and a higher ball/charge weight ratio and a prolong…
Plate‐like Na 0.5 Bi 0.5 TiO 3 (NBT) particles with perovskite structure were synthesized by topochemical microcrystal conversion from plate‐like particles of layer‐structured Na 0.5 Bi 4.5 Ti 4 O 15 (NBIT) at 950°C in NaCl molten salt. As the precursors of NBT, plate‐like NBIT particles were first synthesized by molt…
The light efficiency of most well‐known nematic liquid crystal (LC) modes, such as twisted nematic and in‐plane switching, depends only on the cell retardation value, irrespective of the cell gap and dielectric anisotropy of the LC. Interestingly, the light efficiency of a homogenously aligned nematic LC cell driven b…
Multiwalled carbon nanocoils (CNCs) have been synthesized by a method of thermal chemical vapor deposition (CVD) using a codeposited thin film consisting of Fe and Sn as catalysts. It has been found that the multiwalled CNCs are thinner and have a higher crystallinity than conventional CNCs. The catalyst particles are…
Abstract Caliche in various forms, namely powdery, nodule, tube, fracture-infill, laminar crust, hard laminated crust (hardpan), and pisolitic crust, is widespread in the Mersin area in southern Turkey. It generally occurs within and/or over the reddish-brown mudstone of the Kuzgun Formation (Tortonian, Miocene) and a…
This paper presents a quadtree partitioning fractal image compression (QPFIC) method used for the partial discharge (PD) image remote recognition system. Self-similarity in PD images is the premise of fractal image compression and is described for the typical PD images acquired from defect model experiments in laborat…
The study of low-k TDDB line space scaling is important for assuring robust reliability for new technologies. Although spacing effects due to line edge roughness (LER) on low-k TDDB lifetime were reported previously (Chen et al., 2007; Lloyd et al., 2007; Kim et al., 2007), there has been a lack of an analytical model…
X‐ray diffraction measurements were carried out on nine members of the isothiocyanatobiphenyl homologous series (nBT) in their smectic E (SmE) phase, with the aim of estimating the layer thickness and deriving orthorhombic unit cell parameters for the SmE phase. The data obtained are discussed in relation to molecular…
The knowledge of the defect and impurity generation rates, as well as the defect spatial distribution, is the corner stone for the understanding of the evolution of material properties under irradiation. This knowledge is also an essential element for comprehensive experimental simulations of the behavior of irradiate…
The effect of the deformation temperature ensuring different mobility of dislocations on the change of stages of the structural state of single-crystal nickel has been studied. It has been shown that the deformation temperature affects the type of arising boundaries and the degree of deformation that corresponds to th…
High ultimate strength is required for polycrystalline oxide fibers used as reinforcements of all‐oxide ceramic matrix composites. In commercial alumina fibers high tensile strength (2–3 GPa) is achieved as a result of a submicrometer grain size. However, the fine‐grained fiber microstructure is prone to coarsening, w…
We developed a new surfactant for the dispersion of single-walled carbon nanotubes (SWNTs). The surfactant is an amphiphilic compound with a π-conjugative triphenylene skeleton. SWNTs were individually dispersed by the aid of the surfactant using a common low-power bath sonicator. Well-dispersed HiPco SWNTs in D 2 O s…
An experimental setup, including a cryostat and a temperature control system, has been constructed to meet the demands of measuring linear and nonlinear macroscopic relaxation properties of glass-forming liquids in the extremely viscous state approaching the glass transition. In order to be able to measure such freque…
The rates of fine structure relaxation in PbS, PbSe, and PbTe nanocrystals were measured on a femtosecond time scale as a function of temperature with no applied magnetic field by cross-polarized transient grating spectroscopy (CPTG) and circularly polarized pump-probe spectroscopy. The relaxation rates among exciton…
The room-temperature reaction between chromyl chloride and Sylopol 952 silicas pretreated at 200, 450, and 800 °C was investigated using IR, XANES, and EXAFS spectroscopy, as well as by DFT modeling. On the silicas pretreated at 200 and 450 °C, the structurally uniform sites formed by the reaction with one surface hyd…
A novel photosensitive polyimide, poly(4,4'-stilbenylene 4,4'-oxidiphthalimide) (ODPA-Stilbene PSPI) was newly synthesized. The most surprising feature of this PSPI is that the PSPI films irradiated with linear polarized ultraviolet light (LPUVL) can favorably induce a unidirectional alignment of liquid crystals (LCs)…
Polymer/clay nanocomposites have been under an extensive investigation for about 15 years. Traditional methods to modify the clay are usually limited to small organic cations, preferably containing long alkyl chain(s), which are exchanged with the inorganic cations in the clay gallery. This article provides a comprehe…