Materials Literature
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On the basis of a literature review, an additional criterion of resolution of diffraction curves into crystalline peaks and amorphous component, in generally used Hindeleh-Johnson method of the polymers crystallinity degree (SK) determination, has been proposed. Besides two classical optimization methods by Powell and…
The coordination of diphenyl(phenylacetenyl)phosphine (DPAP, 1) to (X)Rh(III)TPP (X = I (2) or Me (3); TPP = tetraphenyl porphyrin) was studied in solution and in the solid state. The iodide is readily displaced by the phosphine, leading to the bis-phosphine complex [(DPAP)(2)Rh(TPP)](I) (4). The methylide on rhodium…
The cold roller straightening operation is the most critical process for the development of residual stress in rails during manufacturing. Knowledge of the residual stress in ‘as-manufactured’ rails is important for evaluation of the fatigue behaviour of rails during actual use. While experimental investigations have…
The lack of malolactic activity in H(+)-ATPase-deficient mutants of Oenococcus oeni selected previously was analyzed at the molecular level. Western blot experiments revealed a spot at 60 kDa corresponding to the malolactic enzyme only in the parental strain. Moreover, the mleA transcript encoding the malolactic enzym…
It has long been accepted that bacterial quinol-fumarate reductase (QFR) generally uses a low-redox-potential naphthoquinone, menaquinone (MK), as the electron donor, whereas mitochondrial QFR from facultative and anaerobic eukaryotes uses a low-redox-potential benzoquinone, rhodoquinone (RQ), as the substrate. In the…
A computer-based partial discharge detector has been used to measure AC corona pulses in air in a point-cup electrode system. The pulse height distribution was measured as a function of phase angle and pulse height for a range of voltages. The onset voltages for both positive and negative half-cycles are the same, and…
P-type PtSi/porous Si Schottky detectors exhibit efficiencies as large as 60% in 2 to 7 /spl mu/m spectral range. Such efficiencies are larger than theoretical limit for regular PtSi detectors, as predicted by the modified Fowler theory. In the porous detectors a thin PtSi layer covers the walls of the pores creating…
This work provides a crystal-chemical description of the trioctahedral sheet in 1M mica polytypes of C2/m symmetry. Some octahedral parameters were found to be related strictly to octahedral chemical composition, whereas others were related to the overall layer chemistry. As a general rule, the M1 site is more affecte…
Sum-frequency vibrational spectroscopy was employed to study surface glass transition of poly(vinyl alcohol) by monitoring the relaxation of rubbing-induced alignment of surface chains with increase of temperature. The observed chain relaxation is two-dimensional, parallel to the surface. The surface transition temper…
The surface and subsurface layers of cast iron articles upon electrolyte-plasma treatment (EPT) were studied for the first time by a combination of methods, including Rutherford backscattering, elastic recoil detection analysis, X-ray diffraction, optical metallography, and microhardness measurements. It was found tha…
As part of an ongoing research program on the effects of laundering on plain woven cotton fabrics, specimens of poplin and sheeting fabrics with and without a DMDHEU wrinkle resistant finish are laundered under regimes designed to evaluate the effect of five common home laundering variables: use of detergent, rinse cy…
Working insulators begin failing as airborne contaminants and moisture from natural wetting combine on insulator surfaces to cause a drop in surface resistivity. This enables current to conduct across the insulators, thereby changing the electrical activity exhibited by the insulators when clean. If the drop in surfac…
A brief account of transformations of internal structure of hydrogen bonds, and transformations involving the breaking and formation of hydrogen bonds is highlighted for a selected group of crystals. The main stress is laid on the short bistable –OH…O= hydrogen bonds, illustrating several general properties, often blu…
Abstract Long‐term monitoring (for 8000 exposure hours) of titanium and its implant alloys (Ti‐5Al‐4V, Ti‐6Al‐4Fe) interactions with Ringer's solutions of different pH‐values (2.5, 4.35, 6.98), simulating various conditions that can appear at the contact between implant and tissues was carried out in this paper. All d…
RAW 264.7 macrophages express nonmuscle myosin heavy chain II-A as the only significant nonmuscle myosin heavy chain isoform, with expression of nonmuscle myosin heavy chain II-B and II-C low or absent. Treatment of the cells with sodium butyrate, an inhibitor of histone deacetylase, led to the dose-dependent inductio…
Abstract The reaction of [Ru2II,III(O2CCMe3)4]BF4 with nitronyl nitroxide radicals (2,4,4,5,5-pentamethyl-4,5-dihydro-1H-imidazol-1-oxyl-3-N-oxide (nitme) and 2-ethyl-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-1-oxyl-3-N-oxide (nitet)) in CH2Cl2/hexane gave dimer and chain complexes [Ru2(O2CCMe3)4(L)2]BF4 and [{Ru2(O…
Abstract Clay minerals appear to change significantly under the influence of pasture development on poldered sediments in the Baie d'Authie area (Somme, France). Cores 40–90 cm deep from recent salt marsh sediments and poldered sediments developing grass pastures since 1737, 1575 and 1158 indicate that the natural min…
An electronic error compensator is proposed for instrument current transformers. It is specially intended for transformers used in high voltage networks at power frequency. In these transformers, the magnetizing current is the main cause of errors. The proposed system compensates this current, reducing the ratio and p…
We report surprising findings of spontaneous cross-linking of small-diameter zigzag single-walled carbon nanotubes, with no applied external pressure, using ab initio density functional theory. Sunstantial differences in the cross-linking reactivity of zigzag and armchair single-walled carbon nanotubes are revealed by…
Abstract The recycling of vulcanizates based on EPDM roofing membrane rubber using a new ultrasonic devulcanization reactor with a grooved barrel was carried out. This reactor provided continuous devulcanization at an output as high as 2.52 g/s. Die pressure and ultrasonic power consumption were measured as a function…