Materials Literature
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The relaxation processes in pure and copper-doped potassium tantalate niobate (KTN) were investigated by dielectric spectroscopy over a wide frequency and temperature range. In the copper-doped KTN above the ferroelectric phase transition temperature, a relaxation process was observed to behave according to the Vogel-…
In recent years, scientific and industrial interest has been focused on the preparation of organic/inorganic nanocomposites because of their unique hybrid properties correlated with the enormous interfacial adhesion region that is a characteristic of nanoparticles. The objective of the whole research was to improve po…
Abstract In this contribution we report on an XPS study of microporous and mesoporous titanosilicates, in particular microporous titanium silicalite TS‐1, ordered mesoporous Ti‐MCM‐41 and [Ti]‐MCM‐41 and amorphous mesoporous silica–titania (MST) catalysts. Our aim was to obtain both photoemission and x‐ray‐excited Aug…
Species of cyanobacteria in the genera Synechococcus and Synechocystis are known to be the catalysts of a phenomenon called "whitings", which is the formation and precipitation of fine-grained CaCO3 particles. Whitings occur when the cyanobacteria fix atmospheric CO2 through the formation of CaCO3 on their cell surfac…
Superelasticity is a property used in orthodontics to initiate tooth movement in the first stage of orthodontic treatment. It is the aim of all clinicians to accomplish biological tooth movement, which implies the use of low, continuous force and requires archwire with low stiffness. In this study, 15 nickel-titanium…
Abstract The molecular cluster model for homogeneous bubble nucleation was extended to predict the bubble nucleation events in elastomers, polymers and polymer solutions. For nucleation in elastomers and polymers, the strain energy overcome by a critical bubble during growth period was also considered. The calculation…
Principle and test experience of the Oxide Pyro-Process being developed at Research Institute of Atomic Reactors (RIAR, Russia) to process Fast Breeder Reactors spent MOX fuels were reviewed. Attention was paid to the thermodynamics and kinetics of fundamental chemical reactions and to the electrochemical properties o…
This report presents the clinical results three months after application of minocycline microspheres as an adjunct to mechanical treatment of incipient peri-implant infections compared to adjunctive treatment employing 1% chlorhexidine gel application. Sixteen patients in the minocycline group and 14 in the chlorhexid…
Antiferromagnetic resonance in single crystals of rhombohedral gadolinium ferroborate GdFe 3 (BO 3 ) 4 was studied. The frequency-field dependences of antiferromagnetic resonance over the frequency range 26–70 GHz and the temperature dependences of resonance parameters for magnetic fields oriented along the crystal ax…
Abstract Nine‐ and 27‐armed dendrimers with a peroxophosphotungstate core were synthesized by an ionic‐bonding approach and used as air‐stable, recoverable catalysts for oxidation reactions using hydrogen peroxide.
Abstract Highly porous, open‐cell polymers [poly(HIPE)] were prepared by polymerizing the monomers in the continuous phase (∼ 10%) of high internal phase emulsions (HIPE). This paper discusses using poly(HIPE) to remove bromoform from an aqueous solution through sorption, a combination of adsorption and absorption. Th…
(REE,Y) phosphates were synthesized in a 1 atm furnace by ß ux-growth methods involving Pb-free ß uxes. Microcrystalline (REE,Y) phosphate was precipitated from a solution of (REE,Y) chlorides or nitrates plus ammonium dihydrogen phosphate, and mixed with a M 2 CO 3 (M = Li or Na)-MoO 3 flux (75:25:2 molar ratio M 2 C…
A new, stepwise synthesis of calix[4]phyrins is described. It relies on the condensation of a ketone with pyrrole to form a dipyrromethane containing a quaternary carbon center that is subsequently condensed with an aromatic aldehyde. This methodology, in contrast to the previous rational approach described by this gr…
The structural gene for L-lactate dehydrogenase (LDH) (EC.1.1.1.27) from Clostridium thermocellum 27405 was cloned in Escherichia coli by screening the Lambda Zap II phage library of C. thermocellum genomic DNA. In one positive clone, an open reading frame of 948 base pairs corresponded to C. thermocellum ldh gene enc…
The competition to deliver ultra low emitting vehicles at a reasonable cost is driving the automotive industry to invest significant manpower and test lab resources in the design optimization of increasingly complex exhaust aftertreatment systems. Optimization can no longer be based on traditional approaches, which ar…
Abstract This report describes the thermal decomposition behavior and the formation to investigate the flame‐retardant mechanism of organic metal salt in polycarbonate. Moreover, the flame retardancy of the polycarbonate with the addition of various kinds of organic metal salt was evaluated, and the difference in flam…
A new route to the synthesis of 4-chloro-5-alkyl-phthalonitrile derivatives was shown by the displacement reaction of 4,5-dichloro-phthalonitrile and diethylmalonate, a CH -acidic precursor, in the presence of K 2 CO 3 . Cyclotetramerization of 1-chloro-3,4-dicyano-6-(1,1-dicarbethoxy-methyl)benzene and the metal salt…
Continuous carbon nanotube composite fibers having record energy‐to‐break (toughness) are reported. These fibers have been employed in the fabrication of lightweight fiber supercapacitors, which can be woven or sewn into fabrics and, therefore, be potentially considered as components for electronic textiles. Moreover,…
Abstract In this study an attempt was made to improve the rebound resilience and to decrease the density of ethylene‐vinyl acetate copolymer (EVA) foam. For this purpose, EVA was blended with natural rubber (NR), and EVA/NR blends were foamed at 155°C, 160°C, and 165°C. To investigate the correlation between crosslink…
Electrochemical and spectroelectrochemical studies are presented for nine copper corroles with electron-withdrawing or electron-donating substituents on the three meso-phenyl rings of the compounds or on the eight β-pyrrole positions of the macrocycle. Up to three reversible oxidations can be seen for each Cu (III) co…