Materials Literature
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A coating approach for synthesizing 0.9Pb(Mg 1/3 Nb 2/3 )O 3 –0.1PbTiO 3 (0.9PMN–0.1PT) and PMN using a single calcination step was demonstrated. The pyrochlore phase was prevented by coating Mg(OH) 2 on Nb 2 O 5 particles. Coating of Mg(OH) 2 on Nb 2 O 5 was done by precipitating Mg(OH) 2 in an aqueous Nb 2 O 5 suspe…
A local strain of the pennate diatom Pinnularia cf. “ nobilis ” was investigated using cytochemistry and fluorescence and EM techniques. The regular perforation of the chloroplasts of P. “nobilis” and the lack of a typical diatom pyrenoid were confirmed at the ultrastructural level. Cavities and channels in the comple…
Abstract The crystal structure of sahlinite [Pb 14 (AsO 4 ) 2 O 9 Cl 4 ] from Lågban (Sweden) has been refined up to R = 0.071 using single-crystal diffraction data collected at the Elettra synchrotron facility. Sahlinite is monoclinic, space group C2/c, with a = 12.704(4), b = 22.576(5), c = 11.287(4) Å, β = 118.37(3…
Two unpromoted Mo/γ-Al 2 O 3 catalysts containing almost the same amount of Mo were prepared using equilibrium deposition filtration, EDF, for depositing Mo-oxo species on the alumina surface at two different pH values (3.9 and 6.3). On these samples the same amount of Co ions was deposited by dry impregnation and thu…
A Ni 0 (15 wt %)/Al 2 O 3 catalyst is prepared by impregnation using [Ni(en) 2 (H 2 O) 2 ](NO 3 ) 2 as precursor salt containing the chelating ligand ethylenediamine (en). Due to the low solubility of this salt and the high viscosity of its solution, large crystals of the salt deposit on the support, clogging the poro…
Different spliced yam properties (strength, bending, abrasion, and appearance) are merged into a single score, also known as the total score, which is then used to analyze the overall performance of the yarns. A regression model and neural network model are set up according to the total score to predict the performanc…
This article presents a very simple process to align macroscopic quantities of single-wall carbon nanotubes (SWNT), the alignment being controlled by x-ray diffraction. A pellet of SWNT is obtained by pressing a raw nanotube powder up to a pressure of 10 kbars. A detailed study of the most characteristic lines in the…
Abstract New water‐soluble peroxo complexes of niobium( V ) with polyaminocarboxylic acids (PAC) have been prepared and characterized by IR and NMR ( 1 H, 13 C, 15 N) spectroscopy, as well as by thermal analysis. The synthesis in presence of excess H 2 O 2 leads to the oxidation of the nitrogen atoms of the PAC ligand…
Asp142 in the homotetrameric ADP-glucose pyrophosphorylase (ADP-Glc PPase) enzyme from Escherichia coli was demonstrated to be involved in catalysis of this enzyme [Frueauf, J.B., Ballicora, M.A. and Preiss J. (2001) J. Biol. Chem., 276, 46319-46325]. The residue is highly conserved throughout the family of ADP-Glc PP…
High-purity WS 2 nanotubes were synthesized on a relatively large scale by thermal decomposition of amorphous/nano (NH 4 ) 2 WS 4 in a floating hydrogen and thiophene atmosphere at a heating temperature of 360−450 °C. Extensive investigations of WS 2 nanotubes by scanning electron microscopy, high-resolution transmiss…
Abstract The design and applications of photochromic crown compounds are reviewed here. Such compounds exhibit the possibility of distinct photochemical control of metal-ion complexation, based on the ionic interactions of their photoionized photochromic moieties. Crowned spirobenzopyran derivatives which the authors…
Abstract Chain‐folded lamellar crystals of nylon 12 14 have been grown from a dilute 1,4‐butanediol solution with the “self‐seeding” technique. The morphology and structure of nylon 12 14 lamellar crystals were studied by both transmission electron microscopy (TEM) and wide‐angle X‐ray diffraction (WAXD). Two kinds of…
In the decommissioning of a highly contaminated alpha environment, such as the one at Hanford's 233-S Plutonium Concentration Facility, one of the key elements of a successful radiological control program is an integrated safety approach. This approach begins with the job-planning phase where the scope of the work is…
Abstract Fluororubber vulcanizate powder (FVP) obtained from fluororubber based on tetrafluoroethylene/propylene/vinylidene fluoride terpolymer by mechanical grinding exists in a highly aggregated chain‐like structure. X‐ray photoelectron spectros‐copy (XPS) and infrared (IR) spectroscopy studies show that there are n…
The recycling of new and ten years old bumpers either painted or unpainted have been investigated. They were made by a polypropylene matrix and an ethylene-propylene rubber copolymer as dispersed phase. Mechanical testing carried out before reprocessing showed a dramatic loss in the tensile and impact properties of ag…
The microstructures and properties of Ti-Si alloys prepared by are-melting with non-consumable tungsten electrode in a water-cooled copper hearth under a purified argon atmosphere were studied in this paper. The results of XRD indicate that the Ti-Si as cast alloys are composed of α-Ti matrix and Ti5Si3intermetallics.…
Abstract Silicone resins have been used as binders for ceramic frit coatings and can withstand temperatures of 650°C to 1260°C. Conceptually, silicone resins can potentially be used as matrices for high temperature fiber‐reinforced composites. The mechanical and thermal properties of a commercially available silicone…
Five homologous series Ia-e, of the title compounds have been prepared and investigated for their mesophase behaviour in binary mixtures. Each series differs from the other by a substituent X, which changes between CH3O, CH3, Cl, CN, and NO2. The number of carbons in the terminal alkoxy group, within a homologous seri…
On the basis of the intensity-moment formalism, certain analytical relationships are obtained for both the angular domain and the size of a transverse region of the beam that ensure a power content of at least 75% of the total power. As an illustrative application, the analytical results are compared with the exact va…
Abstract As part of a wider research program related to polycarbonate embrittlement, the effects of heat‐aging on mechanical relaxation behavior have been studied by examining the relationship between secondary transitions and stress relaxation behavior. In this Part I, the differences in response between two molecula…