Materials Literature
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Two series of experiments were done to investigate the effect of dislocations on grain growth in SrTiO 3 . In the first series, we observed the growth behavior of a single‐crystal plate toward a TiO 2 ‐excess SrTiO 3 powder compact, containing different dislocation densities on two equivalent {100} surfaces. The surfa…
The statistical kinematical X-ray diffraction theory is developed to describe reciprocal-space maps (RSMs) from deformed crystals with defects of the structure. The general solutions for coherent and diffuse components of the scattered intensity in reciprocal space are derived. As an example, the explicit expressions…
Abstract The gelators of organic solvents are classified into two categories on the basis of their basic intermolecular forces: hydrogen-bonded or nonhydrogen-bonded. To utilize these two interactions cooperatively for organogel formation we newly synthesized seven gelators (1—7) and two reference compounds (8 and 9)…
The deposition of metal nanoparticles (such as Ag, Cu, Au, Pd, and Pt) on boron-doped, polycrystalline diamond thin films grown on silicon substrates was investigated using Raman spectroscopy, scanning electron microscopy, X-ray photoelectron spectroscopy, and X-ray diffraction. Nanometer-size metal particles with pre…
The supramolecular structure of new hydrogen-bonded mesogens composed of dipyridyl and 4-(oligodimethylsiloxyl)alkoxybenzoic acids was investigated by X-ray diffraction and deuterium NMR. These H-bonded mesogens exhibit a cubic thermotropic liquid crystalline phase at a temperature below a smectic A phase. Moreover, a…
We present a neutron scattering study over a wide range of wave vectors of the structure of the fragile glass former triphenylphosphite, with an emphasis on the recently discovered, apparently amorphous, glacial phase. Direct evidence is given by small-angle scattering data that the glacial phase has a structural orga…
Experiments and thermodynamic calculations were performed to gain a better understanding of the CVD of Ti3SiC2. The computer program SOLGASMIX-PV was used to calculate deposition diagrams for the TiCl4–SiCl4–CCl4–H2 reagent system. The effects of hydrogen to reagent concentration ratio, temperature, and pressure were…
Resistance–temperature ( R – T ) characteristics were measured directly at single‐grain boundaries in 0.1‐mol%‐niobium‐doped barium titanate bicrystals that had been fabricated from polycrystalline sinters, to determine a geometrical grain‐boundary character dependence of the positive temperature coefficient of resist…
In this study, cotton fabrics are treated at different curing temperatures with different concentrations of 1,2,3,4-butanetetracarboxylic acid (BTCA) catalyzed with sodium hy pophosphite (SHP). Strength retention and wrinkle recovery angle (WRA) are tested, and the results show that high curing temperature and high BT…
CDP-2,3-di-O-geranylgeranyl-sn-glycerol synthase (CDP-archaeol synthase) activity was discovered in the membrane fraction of the methanoarchaeon Methanothermobacter thermoautotrophicus cells. It catalyzed the formation of CDP-2,3-di-O-geranylgeranyl-sn-glycerol from CTP and 2,3-di-O-geranylgeranyl-sn-glycero-1-phospha…
Using specially “designed” electrolytes, it is possible to obtain macropores even in highly doped n-type silicon (0.020–0.060 Ωcm) without illumination. Based on predictions of the “current-burst-model” [phys. stat. sol. (a) 182, 63 (2000), this issue], HF-containing electrolytes were systematically modified with stro…
The fine structure of the exciton ground level in a spherical nanocrystal of a zincblende or a wurtzite structure semiconductor was calculated with the inclusion of short-and long-range (nonanalytical), exchange-interaction components. The band-parameter dependence of the long-range exchange-interaction contribution t…
Strain-induced grain evolution in a 304 type austenitic stainless steel has been studied in multiple compression with the loading direction being changed in each pass. The tests were carried out to total strains above 6 at 873 K (0.5 T m) at a strain rate of about 10-3 s-1. Multiple deformation promotes the rapid form…
Temperature-dependent measurements of the photoluminescence (PL) intensity, PL lifetime, and infrared photocurrent, were performed on an erbium-implanted silicon p–n junction in order to investigate the energy transfer processes between the silicon electronic system and the Er 4f energy levels. The device features exc…
Microstructural changes caused by doping α‐Al 2 O 3 with small amounts of SiO 2 and TiO 2 added singly or together were investigated. When they were sintered at 1450°C for 120 min, singly doped samples developed equiaxed microstructures, but codoped material developed an anisotropic microstructure that contained plate…
The depolymerization of poly(ethylene terephthalate) (PET) by alcoholysis reaction is an easy operation and gives prospects for the valorization of wastes. PET waste was first depolymerized by glycolysis reaction at different molar ratios of diethylene glycol (DEG), in the presence of Mn acetate as a transesterificati…
The etching of various xerogel films has been studied in high-density fluorocarbon plasmas. The xerogel etch rate is in part enhanced by the porosity. In discharges resulting in low surface polymerization, such as CF4 or oxygen-rich fluorocarbon plasmas, an additional enhancement up to 60% is observed. When the polyme…
Exposure of metallic materials to carbonaceous gases can lead to (i) carburization, i.e. internal carbide formation causing embrittlement and failure especially at high temperatures of cracking tubes for olefine production, (ii) metal dusting, a disintegration of metals to a dust of carbon and fine metal particles, oc…
The pyridoxal 5'-phosphate (PLP)-dependent enzyme 1-aminocyclopropane-1-carboxylate deaminase (ACCD) catalyzes a reaction that involves a ring opening of cyclopropanoid amino acid, yielding alpha-ketobutyrate and ammonia. Unlike other PLP-dependent enzymes, this enzyme has no alpha-hydrogen atom in the substrate. Thus…
Epitaxial growth of thiophene/phenylene co-oligomers(e.g., see Figure) on uniaxially oriented poly(p-phenylene) (PPP) is reported. The emission properties of these co-oligomer thin films are investigated and compared to those of films grown on quartz. Color-tunable emission highly polarized along the direction of orie…